SE8301537L - METHOD AND APPARATUS FOR SULFUR ACID PREPARATION - Google Patents

METHOD AND APPARATUS FOR SULFUR ACID PREPARATION

Info

Publication number
SE8301537L
SE8301537L SE8301537A SE8301537A SE8301537L SE 8301537 L SE8301537 L SE 8301537L SE 8301537 A SE8301537 A SE 8301537A SE 8301537 A SE8301537 A SE 8301537A SE 8301537 L SE8301537 L SE 8301537L
Authority
SE
Sweden
Prior art keywords
h2so4
tower
vapour
steam
sulfuric acid
Prior art date
Application number
SE8301537A
Other languages
Unknown language ( )
Swedish (sv)
Other versions
SE8301537D0 (en
Inventor
P C S Schoubye
Original Assignee
Haldor Topsoe As
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Haldor Topsoe As filed Critical Haldor Topsoe As
Publication of SE8301537D0 publication Critical patent/SE8301537D0/en
Publication of SE8301537L publication Critical patent/SE8301537L/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C01B17/80—Apparatus
    • C01B17/806—Absorbers; Heat exchangers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

In the preparation of sulfuric acid, a 240-330 DEG C hot gas stream containing SO3 and H2SO4-vapour in a total amount of up to 10% b.v. and up to 50% b.v. of steam, the ratio steam/SO3 being at least 1:1, is passed upwards through a plurality of externally cooled, vertical, acid resistant tubes (7) in a heat exchange tower for condensing sulfuric acid. The tubes are cooled with air introduced through an inlet opening (12) in the upper part of the tower and discharged through one or more exit openings in the lower half of the tower. By regulating cooling air velocities and levels from the bottom of the tower of discharging the cooling air the cooling is regulated so as to determine the discharge temperature T4 DEG C by the formula T4>125+6 alpha + beta +0.2(T1-Td> (where alpha is the %b.v. content of SO3+H2SO4-vapour in the feed gas, beta its % b.v. content of steam, T1 its temperature in DEG C and Td its dew point for H2SO4-vapour in DEG C). Sulfuric acid is condensed on the inner tube walls as a film of liquid flowing downwards and in contact with the hot feed gas is concentrated to 93-98% H2SO4. <IMAGE>
SE8301537A 1982-03-25 1983-03-21 METHOD AND APPARATUS FOR SULFUR ACID PREPARATION SE8301537L (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DK136182A DK155723C (en) 1982-03-25 1982-03-25 METHOD AND APPARATUS FOR Sulfuric Acid Preparation

Publications (2)

Publication Number Publication Date
SE8301537D0 SE8301537D0 (en) 1983-03-21
SE8301537L true SE8301537L (en) 1983-09-26

Family

ID=8104014

Family Applications (1)

Application Number Title Priority Date Filing Date
SE8301537A SE8301537L (en) 1982-03-25 1983-03-21 METHOD AND APPARATUS FOR SULFUR ACID PREPARATION

Country Status (7)

Country Link
JP (1) JPS5918103A (en)
CA (1) CA1205614A (en)
DE (1) DE3310779A1 (en)
DK (1) DK155723C (en)
FR (1) FR2523948A1 (en)
GB (1) GB2117368B (en)
SE (1) SE8301537L (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DK168702B1 (en) * 1988-06-02 1994-05-24 Topsoe Haldor As Process for preparing sulfuric acid and apparatus for use in the practice of the process
DK168701B1 (en) * 1988-06-09 1994-05-24 Topsoe Haldor As Process for condensing sulfuric acid vapors in the production of sulfuric acid
CN103547348B (en) * 2011-04-06 2015-07-22 赫多特普索化工设备公司 Process for production of sulphuric acid
EA027599B1 (en) * 2011-06-15 2017-08-31 Хальдор Топсёэ А/С High flow capacity condenser tube for sulphuric acid condensation
CN102320579B (en) * 2011-07-01 2013-04-24 上海科洋科技发展有限公司 Technical method for preparing sulfuric acid from hydrogen sulfide
EP2561921B1 (en) 2011-08-23 2017-03-22 Haldor Topsøe A/S Process for removal of NOx and SO2 in flue gas boilers
CN109692490A (en) * 2019-01-28 2019-04-30 何文旭 Corrosion-resistant falling film evaporator, dilute sulfuric acid concentration systems and its technique and application
CN111495124B (en) * 2020-05-11 2024-04-02 贵州兰鑫石墨机电设备制造有限公司 Comprehensive absorption system for preparing hydrogen chloride from graphite

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE607216C (en) * 1932-11-20 1934-12-19 Metallgesellschaft Ag Production of sulfuric acid by condensation
GB429267A (en) * 1933-03-11 1935-05-20 Metallgesellschaft Ag Process of and apparatus for the recovery of sulphuric acid by condensation
FR1020504A (en) * 1949-06-29 1953-02-06 Nouvelle Soc Induschimie D Etu Method and apparatus for the absorption of sulfur trioxide
CA1079481A (en) * 1973-04-23 1980-06-17 Ralph M. Parsons Company (The) Process and apparatus for prevention of corrosion in a multiple contact-multiple absorption sulfuric acid manufacturing operation
US4360057A (en) * 1979-06-18 1982-11-23 Westinghouse Electric Corp. High temperature abrasive resistant heat exchanger
DK145457C (en) * 1980-03-25 1983-04-18 Haldor Topsoe As PROCEDURE FOR THE PRODUCTION OF SULFURIC ACID, BY THE QUANTITY OF SULFURIC ACID IN THE EXHAUST GAS CONTROLLED BY TEMPERATURE CONTROL

Also Published As

Publication number Publication date
GB2117368B (en) 1985-09-11
DE3310779A1 (en) 1983-09-29
SE8301537D0 (en) 1983-03-21
GB8308081D0 (en) 1983-05-05
JPS5918103A (en) 1984-01-30
FR2523948A1 (en) 1983-09-30
DK155723B (en) 1989-05-08
CA1205614A (en) 1986-06-10
DK136182A (en) 1983-09-26
GB2117368A (en) 1983-10-12
DK155723C (en) 1989-10-09

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