SE8301537D0 - A PROCESS AND APPARATUS FOR THE PREPARATION OF SULFURIC ACID - Google Patents
A PROCESS AND APPARATUS FOR THE PREPARATION OF SULFURIC ACIDInfo
- Publication number
- SE8301537D0 SE8301537D0 SE8301537A SE8301537A SE8301537D0 SE 8301537 D0 SE8301537 D0 SE 8301537D0 SE 8301537 A SE8301537 A SE 8301537A SE 8301537 A SE8301537 A SE 8301537A SE 8301537 D0 SE8301537 D0 SE 8301537D0
- Authority
- SE
- Sweden
- Prior art keywords
- h2so4
- tower
- sulfuric acid
- vapour
- steam
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/74—Preparation
- C01B17/76—Preparation by contact processes
- C01B17/80—Apparatus
- C01B17/806—Absorbers; Heat exchangers
Abstract
In the preparation of sulfuric acid, a 240-330 DEG C hot gas stream containing SO3 and H2SO4-vapour in a total amount of up to 10% b.v. and up to 50% b.v. of steam, the ratio steam/SO3 being at least 1:1, is passed upwards through a plurality of externally cooled, vertical, acid resistant tubes (7) in a heat exchange tower for condensing sulfuric acid. The tubes are cooled with air introduced through an inlet opening (12) in the upper part of the tower and discharged through one or more exit openings in the lower half of the tower. By regulating cooling air velocities and levels from the bottom of the tower of discharging the cooling air the cooling is regulated so as to determine the discharge temperature T4 DEG C by the formula T4>125+6 alpha + beta +0.2(T1-Td> (where alpha is the %b.v. content of SO3+H2SO4-vapour in the feed gas, beta its % b.v. content of steam, T1 its temperature in DEG C and Td its dew point for H2SO4-vapour in DEG C). Sulfuric acid is condensed on the inner tube walls as a film of liquid flowing downwards and in contact with the hot feed gas is concentrated to 93-98% H2SO4. <IMAGE>
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DK136182A DK155723C (en) | 1982-03-25 | 1982-03-25 | METHOD AND APPARATUS FOR Sulfuric Acid Preparation |
Publications (2)
Publication Number | Publication Date |
---|---|
SE8301537D0 true SE8301537D0 (en) | 1983-03-21 |
SE8301537L SE8301537L (en) | 1983-09-26 |
Family
ID=8104014
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SE8301537A SE8301537L (en) | 1982-03-25 | 1983-03-21 | METHOD AND APPARATUS FOR SULFUR ACID PREPARATION |
Country Status (7)
Country | Link |
---|---|
JP (1) | JPS5918103A (en) |
CA (1) | CA1205614A (en) |
DE (1) | DE3310779A1 (en) |
DK (1) | DK155723C (en) |
FR (1) | FR2523948A1 (en) |
GB (1) | GB2117368B (en) |
SE (1) | SE8301537L (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109692490A (en) * | 2019-01-28 | 2019-04-30 | 何文旭 | Corrosion-resistant falling film evaporator, dilute sulfuric acid concentration systems and its technique and application |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DK168702B1 (en) * | 1988-06-02 | 1994-05-24 | Topsoe Haldor As | Process for preparing sulfuric acid and apparatus for use in the practice of the process |
DK168701B1 (en) * | 1988-06-09 | 1994-05-24 | Topsoe Haldor As | Process for condensing sulfuric acid vapors in the production of sulfuric acid |
MX2013011484A (en) * | 2011-04-06 | 2013-11-04 | Haldor Topsoe As | Process for production of sulphuric acid. |
WO2012171824A1 (en) * | 2011-06-15 | 2012-12-20 | Haldor Topsøe A/S | High flow capacity condenser tube for sulphuric acid condensation |
CN102320579B (en) * | 2011-07-01 | 2013-04-24 | 上海科洋科技发展有限公司 | Technical method for preparing sulfuric acid from hydrogen sulfide |
EP2561921B1 (en) | 2011-08-23 | 2017-03-22 | Haldor Topsøe A/S | Process for removal of NOx and SO2 in flue gas boilers |
CN111495124B (en) * | 2020-05-11 | 2024-04-02 | 贵州兰鑫石墨机电设备制造有限公司 | Comprehensive absorption system for preparing hydrogen chloride from graphite |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE607216C (en) * | 1932-11-20 | 1934-12-19 | Metallgesellschaft Ag | Production of sulfuric acid by condensation |
GB429267A (en) * | 1933-03-11 | 1935-05-20 | Metallgesellschaft Ag | Process of and apparatus for the recovery of sulphuric acid by condensation |
FR1020504A (en) * | 1949-06-29 | 1953-02-06 | Nouvelle Soc Induschimie D Etu | Method and apparatus for the absorption of sulfur trioxide |
CA1079481A (en) * | 1973-04-23 | 1980-06-17 | Ralph M. Parsons Company (The) | Process and apparatus for prevention of corrosion in a multiple contact-multiple absorption sulfuric acid manufacturing operation |
US4360057A (en) * | 1979-06-18 | 1982-11-23 | Westinghouse Electric Corp. | High temperature abrasive resistant heat exchanger |
DK145457C (en) * | 1980-03-25 | 1983-04-18 | Haldor Topsoe As | PROCEDURE FOR THE PRODUCTION OF SULFURIC ACID, BY THE QUANTITY OF SULFURIC ACID IN THE EXHAUST GAS CONTROLLED BY TEMPERATURE CONTROL |
-
1982
- 1982-03-25 DK DK136182A patent/DK155723C/en not_active IP Right Cessation
-
1983
- 1983-03-21 SE SE8301537A patent/SE8301537L/en not_active Application Discontinuation
- 1983-03-23 FR FR8304732A patent/FR2523948A1/en active Pending
- 1983-03-24 DE DE19833310779 patent/DE3310779A1/en not_active Ceased
- 1983-03-24 GB GB08308081A patent/GB2117368B/en not_active Expired
- 1983-03-25 JP JP58049077A patent/JPS5918103A/en active Pending
- 1983-03-25 CA CA000424458A patent/CA1205614A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109692490A (en) * | 2019-01-28 | 2019-04-30 | 何文旭 | Corrosion-resistant falling film evaporator, dilute sulfuric acid concentration systems and its technique and application |
Also Published As
Publication number | Publication date |
---|---|
GB8308081D0 (en) | 1983-05-05 |
SE8301537L (en) | 1983-09-26 |
DK136182A (en) | 1983-09-26 |
GB2117368B (en) | 1985-09-11 |
DK155723B (en) | 1989-05-08 |
FR2523948A1 (en) | 1983-09-30 |
DE3310779A1 (en) | 1983-09-29 |
GB2117368A (en) | 1983-10-12 |
DK155723C (en) | 1989-10-09 |
CA1205614A (en) | 1986-06-10 |
JPS5918103A (en) | 1984-01-30 |
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Legal Events
Date | Code | Title | Description |
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NAV | Patent application has lapsed |
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