SE128380C1 - - Google Patents

Info

Publication number

SE128380C1

SE128380C1 SE128380DA SE128380C1 SE 128380 C1 SE128380 C1 SE 128380C1 SE 128380D A SE128380D A SE 128380DA SE 128380 C1 SE128380 C1 SE 128380C1

Authority

SE

Sweden

Prior art keywords

dinitrotoluol

amino

nitrobenzoic acid

equal parts

heated

Prior art date

1950-01-01

Links

• Espacenet
• Global Dossier
• Discuss

• RMBFBMJGBANMMK-UHFFFAOYSA-N 2,4-dinitrotoluene Chemical compound CC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O RMBFBMJGBANMMK-UHFFFAOYSA-N 0.000 claims description 7
• UEALKTCRMBVTFN-UHFFFAOYSA-N 4-nitroanthranilic acid Chemical compound NC1=CC([N+]([O-])=O)=CC=C1C(O)=O UEALKTCRMBVTFN-UHFFFAOYSA-N 0.000 claims description 7
• KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 6
• KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 6
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
• 238000010438 heat treatment Methods 0.000 claims description 3
• 239000003085 diluting agent Substances 0.000 claims description 2
• 238000010924 continuous production Methods 0.000 claims 1
• 239000011872 intimate mixture Substances 0.000 claims 1
• 238000010992 reflux Methods 0.000 claims 1
• 150000003839 salts Chemical class 0.000 claims 1
• 238000002360 preparation method Methods 0.000 description 5
• 239000007795 chemical reaction product Substances 0.000 description 3
• 238000006243 chemical reaction Methods 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• 239000007858 starting material Substances 0.000 description 2
• UYJXRRSPUVSSMN-UHFFFAOYSA-P ammonium sulfide Chemical compound [NH4+].[NH4+].[S-2] UYJXRRSPUVSSMN-UHFFFAOYSA-P 0.000 description 1
• 239000002246 antineoplastic agent Substances 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 239000006227 byproduct Substances 0.000 description 1
• 239000003795 chemical substances by application Substances 0.000 description 1
• 229940127089 cytotoxic agent Drugs 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• YMHUULKGTGEHHQ-UHFFFAOYSA-N n-(2-methyl-5-nitrophenyl)acetamide Chemical compound CC(=O)NC1=CC([N+]([O-])=O)=CC=C1C YMHUULKGTGEHHQ-UHFFFAOYSA-N 0.000 description 1
• 230000007935 neutral effect Effects 0.000 description 1
• 230000003647 oxidation Effects 0.000 description 1
• 238000007254 oxidation reaction Methods 0.000 description 1
• 239000012286 potassium permanganate Substances 0.000 description 1
• 239000004071 soot Substances 0.000 description 1
• 239000004094 surface-active agent Substances 0.000 description 1
• 201000008827 tuberculosis Diseases 0.000 description 1