RU95120604A - LIGHT- AND HEAT-STABILIZING MIXTURE FOR POLYPROPYLENE FIBER, NOT HAVING A GREAT IMPACT ON COLOR CHANGE - Google Patents
LIGHT- AND HEAT-STABILIZING MIXTURE FOR POLYPROPYLENE FIBER, NOT HAVING A GREAT IMPACT ON COLOR CHANGEInfo
- Publication number
- RU95120604A RU95120604A RU95120604/04A RU95120604A RU95120604A RU 95120604 A RU95120604 A RU 95120604A RU 95120604/04 A RU95120604/04 A RU 95120604/04A RU 95120604 A RU95120604 A RU 95120604A RU 95120604 A RU95120604 A RU 95120604A
- Authority
- RU
- Russia
- Prior art keywords
- amino
- bis
- tetramethylpiperidin
- mixture
- stabilized
- Prior art date
Links
- -1 POLYPROPYLENE Polymers 0.000 title claims 25
- 239000000203 mixture Substances 0.000 title claims 12
- 239000004743 Polypropylene Substances 0.000 title claims 8
- 229920001155 polypropylene Polymers 0.000 title claims 8
- 239000000835 fiber Substances 0.000 claims 19
- 238000006068 polycondensation reaction Methods 0.000 claims 11
- 239000003381 stabilizer Substances 0.000 claims 10
- 150000001412 amines Chemical class 0.000 claims 9
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims 8
- YZXTWMQYSSMUFH-UHFFFAOYSA-N 4-[6-(1-amino-2,2,6,6-tetramethylpiperidin-4-yl)hexyl]-2,2,6,6-tetramethylpiperidin-1-amine Chemical compound C1C(C)(C)N(N)C(C)(C)CC1CCCCCCC1CC(C)(C)N(N)C(C)(C)C1 YZXTWMQYSSMUFH-UHFFFAOYSA-N 0.000 claims 7
- STEYNUVPFMIUOY-UHFFFAOYSA-N 1-(2-hydroxyethyl)-2,2,6,6-tetramethylpiperidin-4-ol Chemical compound CC1(C)CC(O)CC(C)(C)N1CCO STEYNUVPFMIUOY-UHFFFAOYSA-N 0.000 claims 4
- 239000007789 gas Substances 0.000 claims 4
- 230000003647 oxidation Effects 0.000 claims 4
- 238000007254 oxidation reaction Methods 0.000 claims 4
- 239000001384 succinic acid Substances 0.000 claims 4
- UQAMDAUJTXFNAD-UHFFFAOYSA-N 4-(4,6-dichloro-1,3,5-triazin-2-yl)morpholine Chemical compound ClC1=NC(Cl)=NC(N2CCOCC2)=N1 UQAMDAUJTXFNAD-UHFFFAOYSA-N 0.000 claims 3
- 241000790917 Dioxys <bee> Species 0.000 claims 3
- 238000004061 bleaching Methods 0.000 claims 3
- 125000004956 cyclohexylene group Chemical group 0.000 claims 3
- LRBPFPZTIZSOGG-UHFFFAOYSA-N dimethyl 2-methylpropanedioate Chemical compound COC(=O)C(C)C(=O)OC LRBPFPZTIZSOGG-UHFFFAOYSA-N 0.000 claims 3
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims 3
- 125000005373 siloxane group Chemical group [SiH2](O*)* 0.000 claims 3
- ULINDIVVCBSIPZ-UHFFFAOYSA-N (2,4-ditert-butylphenyl) phosphite Chemical compound CC(C)(C)C1=CC=C(OP([O-])[O-])C(C(C)(C)C)=C1 ULINDIVVCBSIPZ-UHFFFAOYSA-N 0.000 claims 2
- HPFWYRKGZUGGPB-UHFFFAOYSA-N 4,6-dichloro-N-(2,4,4-trimethylpentan-2-yl)-1,3,5-triazin-2-amine Chemical compound CC(C)(C)CC(C)(C)NC1=NC(Cl)=NC(Cl)=N1 HPFWYRKGZUGGPB-UHFFFAOYSA-N 0.000 claims 2
- NPYDPROENPLGBR-UHFFFAOYSA-N 4,6-dichloro-N-cyclohexyl-1,3,5-triazin-2-amine Chemical compound ClC1=NC(Cl)=NC(NC2CCCCC2)=N1 NPYDPROENPLGBR-UHFFFAOYSA-N 0.000 claims 2
- ITUWQZXQRZLLCR-UHFFFAOYSA-N N,N-dioctadecylhydroxylamine Chemical compound CCCCCCCCCCCCCCCCCCN(O)CCCCCCCCCCCCCCCCCC ITUWQZXQRZLLCR-UHFFFAOYSA-N 0.000 claims 2
- AQSJGOWTSHOLKH-UHFFFAOYSA-N Phosphite Chemical compound [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- ZEFSGHVBJCEKAZ-UHFFFAOYSA-N bis(2,4-ditert-butyl-6-methylphenyl) ethyl phosphite Chemical compound CC=1C=C(C(C)(C)C)C=C(C(C)(C)C)C=1OP(OCC)OC1=C(C)C=C(C(C)(C)C)C=C1C(C)(C)C ZEFSGHVBJCEKAZ-UHFFFAOYSA-N 0.000 claims 2
- LROMFDHROPKFSO-UHFFFAOYSA-N dioxidophosphane Chemical compound [O-]P[O-] LROMFDHROPKFSO-UHFFFAOYSA-N 0.000 claims 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 2
- 238000005562 fading Methods 0.000 claims 2
- AVXURJPOCDRRFD-UHFFFAOYSA-N hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims 2
- 239000002530 phenolic antioxidant Substances 0.000 claims 2
- 230000002035 prolonged Effects 0.000 claims 2
- 238000011105 stabilization Methods 0.000 claims 2
- RXFCIXRFAJRBSG-UHFFFAOYSA-N 3,2,3-tetramine Chemical compound NCCCNCCNCCCN RXFCIXRFAJRBSG-UHFFFAOYSA-N 0.000 claims 1
- IFVTZJHWGZSXFD-UHFFFAOYSA-N Biphenylene Chemical group C1=CC=C2C3=CC=CC=C3C2=C1 IFVTZJHWGZSXFD-UHFFFAOYSA-N 0.000 claims 1
- 238000002845 discoloration Methods 0.000 claims 1
Claims (16)
а) смешанного амина, выбранного из группы, состоящей из продукта поликонденсации 4,4'-гексаметилен-бис(амино-2,2,6,6-тетраметилпиперидина) и 2,4-дихлор-6-трет-октиламино-с-триазина; продукта поликонденсации 1-(2-гидроксиэтил)-2,2,6,6-тетраметил-4-гидроксипиперидина и янтарной кислоты; N,N',N'', N'''-тетракис[4,6-бис(бутил-(2,2,6,6-тетраметилпиперидин-4-ил)-амино)-с-триазин-2-ил] -1,10-диамино-4,7-диазадекана; продукта поликонденсации 4,4'-гексаметилен-бис (амино-2,2,6,6-тетраметилпиперидина) и 2,4-дихлоро-6-морфолино-с-триазина; поли[метил-3-(2,2,6,6-тетраметилпиперидин-4-илокси) пропил] силоксана; бис(2,2,6,6-тетраметилпиперидин-4-ил) циклогексилендиоксидиметилмалоната; 1,3,5-три{ N-циклогексил-N-[2(2,2,6,6-тетраметилпиперазин-3-он-4-ил) этил] амино-с-триазина; продукта поликонденсации 4,4'-гексаметилен-бис(амино-2,2,6,6-тетраметилпиперидина) и 2,4-дихлоро-6-циклогексиламино-с-триазина; и поли{ N-[4,6-би(бутил-2,2,6,6-тетраметилпиперидин-4-ил)амино)-с-триазин-2-ил] -1,4,7-триазанонан} -N''-[4,6-бис(бутил-2,2,6,6-тетраметилпиперидин-4-ил)амино)-с-триазин-2-ил]амина;
б) фосфита или фосфонита, выбранного из группы, состоящей из три(2,4-ди-третбутилфенил)фосфита; 3,9-ди(2,4-ди-трет-бутилфенил)-2,4,8,10-тетраокса-3,9-дифосфа[5,5]андекана; 2,2',2''-нитрило-три[этил(3,3',5,5'-тетра-трет-бутил-1,1' бифенил-2,2'диил)фосфита; этил бис(2,4-ди-трет-бутил-6-метилфенил) фосфита; и тетракис(2,4-дитрет-бутилфенил)4,4'-бис(дифенилен) фосфонита; и
в) гидроксиламина, выбранного из группы, состоящей из N,N-диоктадецилгидроксиламина; N,N-диалкилгидроксиламина с формулой T1T2NOH, где T1 и T2 - смесь алкилов из гидрогенизированного жирного амина; и N,N-диалкилгидроксиламина, полученного прямым окислением N,N-ди(гидрогенизированный жир)амина; причем компоненты смешиваются в соотношении (а) : (б) : (в): от 1 : 1 : 1 до 100 : 2 : 1.1. Stabilized polypropylene fiber that does not contain phenolic antioxidants or essentially does not contain them and has increased light resistance, increased heat resistance during prolonged exposure and increased resistance to gas bleaching, stabilized with a mixture
a) a mixed amine selected from the group consisting of 4,4'-hexamethylene bis (amino-2,2,6,6-tetramethylpiperidine) polycondensation product and 2,4-dichloro-6-tert-octylamino-s-triazine ; the polycondensation product of 1- (2-hydroxyethyl) -2,2,6,6-tetramethyl-4-hydroxypiperidine and succinic acid; N, N ', N'',N''' - tetrakis [4,6-bis (butyl- (2,2,6,6-tetramethylpiperidin-4-yl) amino) -c-triazin-2-yl ] -1,10-diamino-4,7-diazadecane; the polycondensation product of 4,4'-hexamethylene bis (amino-2,2,6,6-tetramethylpiperidine) and 2,4-dichloro-6-morpholino-s-triazine; poly [methyl-3- (2,2,6,6-tetramethylpiperidin-4-yloxy) propyl] siloxane; bis (2,2,6,6-tetramethylpiperidin-4-yl) cyclohexylene dioxy dimethyl methyl malonate; 1,3,5-tri {N-cyclohexyl-N- [2 (2,2,6,6-tetramethylpiperazin-3-one-4-yl) ethyl] amino-s-triazine; the polycondensation product of 4,4'-hexamethylene bis (amino-2,2,6,6-tetramethylpiperidine) and 2,4-dichloro-6-cyclohexylamino-s-triazine; and poly {N- [4,6-bi (butyl-2,2,6,6-tetramethylpiperidin-4-yl) amino) -c-triazin-2-yl] -1,4,7-triazanonan} -N '' - [4,6-bis (butyl-2,2,6,6-tetramethylpiperidin-4-yl) amino) -c-triazin-2-yl] amine;
b) a phosphite or phosphonite selected from the group consisting of three (2,4-di-tert-butylphenyl) phosphite; 3,9-di (2,4-di-tert-butylphenyl) -2,4,8,10-tetraoxa-3,9-diphospha [5.5] andecane; 2,2 ', 2''- nitrilo-tri [ethyl (3,3', 5,5'-tetra-tert-butyl-1,1 'biphenyl-2,2'diyl) phosphite; ethyl bis (2,4-di-tert-butyl-6-methylphenyl) phosphite; and tetrakis (2,4-ditret-butylphenyl) 4,4'-bis (diphenylene) phosphonite; and
c) hydroxylamine selected from the group consisting of N, N-dioctadecylhydroxylamine; N, N-dialkylhydroxylamine with the formula T 1 T 2 NOH, where T 1 and T 2 are a mixture of alkyls from a hydrogenated fatty amine; and N, N-dialkylhydroxylamine obtained by direct oxidation of an N, N-di (hydrogenated fat) amine; moreover, the components are mixed in the ratio (a): (b): (c): from 1: 1: 1 to 100: 2: 1.
I) смешанного амина, выбранного из группы, состоящей из продукта поликонденсации 1-(2-гидроксиэтил)-2,2,6,6- тетраметил-4-гидроксипиперидина и янтарной кислоты; N,N',N'',N'''-тетракис[4,6-би(бутил-(2,2,6,6-тетраметилпиперидин-4-ил) амино)-с-триазин-2-ил]-1,10-диамино-4,7-диазадекана; продукта поликонденсации 4,4'-гексаметиленбис(амино-2,2,6,6-тетраметилпиперидина) и 2,4-дихлоро-6-морфолино-с-триазина; поли[метил-3-(2,2,6,6-тетраметилпиперидин-4-илокси)пропил] силоксана; бис(2,2,6,6-тетраметилпиперидин-4-ил) циклогексилендиоксидиметилмалоната; 1,3,5-три{N-циклогексил-N-[2-(2,2,6,6-тетраметилпиперазин-3-он-4ил)этил] амино-с-триазина, и продукта поликонденсации 4,4'-гексаметилен-бис(амино-2,2,6,6-тетраметилпиперидина) и 2,4-дихлоро-6-циклогексиламино-с-триазина; и
II) гидроксиламина, выбранного из группы, состоящей из N,N-диоктадецилгидроксиламина; N,N-диалкилгидроксиламина с формулой T1T2OH, где T1 и T2 - смесь алкилов из гидрогенизированного жирного амина; и N,N-диалкилгидроксиламина, полученного прямым окислением N, N-ди(гидрогенизированный жир)амина; причем соотношение компонентов (I) : (II) от 100 : 1 до 1 : 2 по массе.10. Stabilized polypropylene fiber that does not contain or essentially does not contain any phenolic antioxidants, and has increased light resistance, increased heat resistance during prolonged exposure and increased resistance to gas bleaching, said fiber is stabilized by a mixture
I) a mixed amine selected from the group consisting of the polycondensation product of 1- (2-hydroxyethyl) -2,2,6,6-tetramethyl-4-hydroxypiperidine and succinic acid; N, N ', N'',N''' - tetrakis [4,6-bi (butyl- (2,2,6,6-tetramethylpiperidin-4-yl) amino) -c-triazin-2-yl] -1,10-diamino-4,7-diazadecane; the polycondensation product of 4,4'-hexamethylene bis (amino-2,2,6,6-tetramethylpiperidine) and 2,4-dichloro-6-morpholino-s-triazine; poly [methyl-3- (2,2,6,6-tetramethylpiperidin-4-yloxy) propyl] siloxane; bis (2,2,6,6-tetramethylpiperidin-4-yl) cyclohexylene dioxy dimethyl methyl malonate; 1,3,5-tri {N-cyclohexyl-N- [2- (2,2,6,6-tetramethylpiperazin-3-one-4yl) ethyl] amino-s-triazine, and the polycondensation product 4,4'- hexamethylene bis (amino-2,2,6,6-tetramethylpiperidine) and 2,4-dichloro-6-cyclohexylamino-s-triazine; and
Ii) hydroxylamine selected from the group consisting of N, N-dioctadecylhydroxylamine; N, N-dialkylhydroxylamine with the formula T 1 T 2 OH, where T 1 and T 2 is a mixture of alkyls from a hydrogenated fatty amine; and N, N-dialkylhydroxylamine obtained by direct oxidation of an N, N-di (hydrogenated fat) amine; moreover, the ratio of components (I): (II) from 100: 1 to 1: 2 by weight.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US4808693A | 1993-04-15 | 1993-04-15 | |
US08/048,086 | 1993-04-15 | ||
US08/048.086 | 1993-04-15 | ||
PCT/IB1994/000056 WO1994024344A1 (en) | 1993-04-15 | 1994-04-06 | Low color processing, heat and light stabilizer system for polypropylene fiber |
Publications (2)
Publication Number | Publication Date |
---|---|
RU95120604A true RU95120604A (en) | 1997-11-10 |
RU2126065C1 RU2126065C1 (en) | 1999-02-10 |
Family
ID=21952660
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU95120604A RU2126065C1 (en) | 1993-04-15 | 1994-04-06 | Light and heat-stabilizing mixture for polypropylene fiber without significant effect on color change |
Country Status (20)
Country | Link |
---|---|
JP (1) | JP3424080B2 (en) |
KR (1) | KR100282620B1 (en) |
CN (1) | CN1051340C (en) |
AT (1) | AT405412B (en) |
AU (1) | AU6263294A (en) |
BE (1) | BE1006850A3 (en) |
BR (1) | BR9406876A (en) |
CA (1) | CA2160574C (en) |
DE (2) | DE4492361C2 (en) |
DK (1) | DK175151B1 (en) |
FR (1) | FR2704009B1 (en) |
GB (1) | GB2292944B (en) |
HK (1) | HK1005489A1 (en) |
IT (1) | IT1269313B (en) |
NL (1) | NL9420023A (en) |
NO (1) | NO309683B1 (en) |
RU (1) | RU2126065C1 (en) |
SK (1) | SK284817B6 (en) |
TW (1) | TW268052B (en) |
WO (1) | WO1994024344A1 (en) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2705679B1 (en) * | 1993-05-24 | 1998-07-10 | Sandoz Sa | New stabilizing compositions for polymeric materials, based on phosphonites or phosphites and a stabilizer against hydrolysis. |
EP0710677A3 (en) * | 1994-11-03 | 1998-02-04 | Ciba SC Holding AG | Process for producing stabilized olefin polymers |
TW401437B (en) | 1995-02-10 | 2000-08-11 | Ciba Sc Holding Ag | Synergistic stabilizer mixture |
WO1997030199A1 (en) | 1996-02-12 | 1997-08-21 | Fibervisions A/S | Particle-containing fibres |
CN1064416C (en) * | 1996-05-02 | 2001-04-11 | 上海石油化工股份有限公司 | Method for manufacturing dyeable fine denier polypropylene fibre |
KR100227221B1 (en) * | 1997-04-01 | 1999-11-01 | 이정국 | A polypropylene resin fiber composition having improved water-resistance and the textile using their fibers |
US5834541A (en) * | 1997-05-02 | 1998-11-10 | Montell North America Inc. | Olefin polymer composition having low smoke generation and fiber and film prepared therefrom |
US5994436A (en) * | 1997-12-18 | 1999-11-30 | Montell North America Inc. | Ductile gamma radiation resistant polyolefin composition and articles produced therefrom |
US6172153B1 (en) * | 1998-06-12 | 2001-01-09 | Montell North America Inc. | Olefin polymer composition having low smoke generation and fiber, film and fabric prepared therefrom |
EP1115783A1 (en) * | 1998-08-26 | 2001-07-18 | Union Carbide Chemicals & Plastics Technology Corporation | Novel polypropylene compositions |
US6214915B1 (en) * | 1998-12-10 | 2001-04-10 | General Electric Company | Stabilized thermoplastic compositions |
NL1014465C2 (en) * | 1999-03-01 | 2002-01-29 | Ciba Sc Holding Ag | Stabilizer combination for the rotomolding process. |
US6444733B1 (en) * | 1999-03-01 | 2002-09-03 | Ciba Specialty Chemicals Corporation | Stabilizer combination for the rotomolding process |
JP2002097322A (en) * | 2000-09-25 | 2002-04-02 | Grand Polymer Co Ltd | Polypropylene-based resin composition and molded product therefrom |
JP4785135B2 (en) * | 2006-07-31 | 2011-10-05 | 三菱レイヨン株式会社 | Polypropylene flame retardant fiber |
CN101195944B (en) * | 2007-12-11 | 2011-09-07 | 卢宗广 | Non-zillerite environment protection energy-saving diaphragm cloth and weaving method thereof |
KR101062997B1 (en) | 2009-05-29 | 2011-09-07 | 코오롱글로텍주식회사 | Polypropylene short fibers with high heat resistance and light resistance, manufacturing method thereof, nonwoven fabric made therefrom |
DE102010006364B4 (en) * | 2010-01-29 | 2015-07-23 | Carl Freudenberg Kg | Use of sterically hindered amines for oxidation-stabilized polyolefins |
CN106319665A (en) * | 2015-06-15 | 2017-01-11 | 东丽纤维研究所(中国)有限公司 | Colored polypropylene fiber and preparation method thereof |
EA201991032A1 (en) * | 2016-11-09 | 2019-10-31 | POLYPROPYLENE COMPOSITION | |
GB2584305B (en) * | 2019-05-30 | 2022-07-13 | Si Group Switzerland Chaa Gmbh | Antidegradant blend |
CN110229421B (en) * | 2019-07-02 | 2021-11-09 | 中广核俊尔(浙江)新材料有限公司 | High-temperature-resistant injection molding polypropylene material and preparation method and application thereof |
CN111057288A (en) * | 2019-12-12 | 2020-04-24 | 宿迁联盛科技股份有限公司 | Composition for preventing polyolefin copolymer from photo-aging and polyolefin red-change |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4590231A (en) * | 1983-10-11 | 1986-05-20 | Ciba-Geigy Corporation | Polyolefin compositions stabilized against degradation using hydroxylamine derivatives |
JPS60190443A (en) * | 1984-03-13 | 1985-09-27 | Mitsui Toatsu Chem Inc | Polypropylene resin composition stable to radiation |
JP2553537B2 (en) * | 1987-01-23 | 1996-11-13 | 東燃化学 株式会社 | Polypropylene fiber yarn-proofing composition |
US4876300A (en) * | 1987-12-30 | 1989-10-24 | Ciba-Geigy Corporation | Polyolefin compositions stabilized with long chain N,N-dialkylhydroxylamines |
-
1994
- 1994-03-26 TW TW083102663A patent/TW268052B/zh not_active IP Right Cessation
- 1994-04-06 AT AT0903394A patent/AT405412B/en not_active IP Right Cessation
- 1994-04-06 GB GB9520527A patent/GB2292944B/en not_active Expired - Lifetime
- 1994-04-06 RU RU95120604A patent/RU2126065C1/en active
- 1994-04-06 DE DE4492361A patent/DE4492361C2/en not_active Expired - Lifetime
- 1994-04-06 CA CA002160574A patent/CA2160574C/en not_active Expired - Lifetime
- 1994-04-06 BR BR9406876A patent/BR9406876A/en not_active IP Right Cessation
- 1994-04-06 AU AU62632/94A patent/AU6263294A/en not_active Abandoned
- 1994-04-06 CN CN94191786A patent/CN1051340C/en not_active Expired - Lifetime
- 1994-04-06 NL NL9420023A patent/NL9420023A/en active Search and Examination
- 1994-04-06 JP JP52295194A patent/JP3424080B2/en not_active Expired - Lifetime
- 1994-04-06 DE DE4492361T patent/DE4492361T1/en active Granted
- 1994-04-06 WO PCT/IB1994/000056 patent/WO1994024344A1/en active Application Filing
- 1994-04-06 SK SK1272-95A patent/SK284817B6/en not_active IP Right Cessation
- 1994-04-06 KR KR1019950704499A patent/KR100282620B1/en not_active IP Right Cessation
- 1994-04-14 FR FR9404431A patent/FR2704009B1/en not_active Expired - Lifetime
- 1994-04-14 BE BE9400382A patent/BE1006850A3/en not_active IP Right Cessation
- 1994-04-14 IT ITMI940706A patent/IT1269313B/en active IP Right Grant
-
1995
- 1995-10-03 NO NO953932A patent/NO309683B1/en not_active IP Right Cessation
- 1995-10-04 DK DK199501109A patent/DK175151B1/en not_active IP Right Cessation
-
1998
- 1998-05-28 HK HK98104631A patent/HK1005489A1/en not_active IP Right Cessation
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