RU2667287C1 - Способ повышения прочности бумаги - Google Patents
Способ повышения прочности бумаги Download PDFInfo
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- RU2667287C1 RU2667287C1 RU2016119058A RU2016119058A RU2667287C1 RU 2667287 C1 RU2667287 C1 RU 2667287C1 RU 2016119058 A RU2016119058 A RU 2016119058A RU 2016119058 A RU2016119058 A RU 2016119058A RU 2667287 C1 RU2667287 C1 RU 2667287C1
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- RU
- Russia
- Prior art keywords
- paper
- polyacrylamide
- range
- cationic
- chloride
- Prior art date
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- 238000000034 method Methods 0.000 title claims abstract description 48
- 229920002401 polyacrylamide Polymers 0.000 claims abstract description 85
- 125000002091 cationic group Chemical group 0.000 claims abstract description 79
- 239000000203 mixture Substances 0.000 claims abstract description 52
- 125000000129 anionic group Chemical group 0.000 claims abstract description 33
- 238000004519 manufacturing process Methods 0.000 claims abstract description 18
- 239000000178 monomer Substances 0.000 claims description 24
- 239000000725 suspension Substances 0.000 claims description 19
- 150000003839 salts Chemical class 0.000 claims description 17
- -1 p-vinylphenyltrimethylammonium chloride -vinylbenzyltrimethylammonium chloride Chemical compound 0.000 claims description 14
- 229920005601 base polymer Polymers 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- NJSSICCENMLTKO-HRCBOCMUSA-N [(1r,2s,4r,5r)-3-hydroxy-4-(4-methylphenyl)sulfonyloxy-6,8-dioxabicyclo[3.2.1]octan-2-yl] 4-methylbenzenesulfonate Chemical compound C1=CC(C)=CC=C1S(=O)(=O)O[C@H]1C(O)[C@@H](OS(=O)(=O)C=2C=CC(C)=CC=2)[C@@H]2OC[C@H]1O2 NJSSICCENMLTKO-HRCBOCMUSA-N 0.000 claims description 11
- 239000011248 coating agent Substances 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 8
- 238000007639 printing Methods 0.000 claims description 6
- 238000005507 spraying Methods 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- TVXNKQRAZONMHJ-UHFFFAOYSA-M (4-ethenylphenyl)methyl-trimethylazanium;chloride Chemical compound [Cl-].C[N+](C)(C)CC1=CC=C(C=C)C=C1 TVXNKQRAZONMHJ-UHFFFAOYSA-M 0.000 claims description 3
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 claims description 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 3
- OHDSHGBRKMRPHC-UHFFFAOYSA-N 2-(4-ethenylphenyl)-n,n-dimethylethanamine Chemical compound CN(C)CCC1=CC=C(C=C)C=C1 OHDSHGBRKMRPHC-UHFFFAOYSA-N 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- DTJIKSRARSRPBU-UHFFFAOYSA-N 2-ethenyl-1-methylpyridin-1-ium Chemical compound C[N+]1=CC=CC=C1C=C DTJIKSRARSRPBU-UHFFFAOYSA-N 0.000 claims description 3
- GFHWCDCFJNJRQR-UHFFFAOYSA-M 2-ethenyl-1-methylpyridin-1-ium;chloride Chemical compound [Cl-].C[N+]1=CC=CC=C1C=C GFHWCDCFJNJRQR-UHFFFAOYSA-M 0.000 claims description 3
- KGIGUEBEKRSTEW-UHFFFAOYSA-N 2-vinylpyridine Chemical compound C=CC1=CC=CC=N1 KGIGUEBEKRSTEW-UHFFFAOYSA-N 0.000 claims description 3
- NYUTUWAFOUJLKI-UHFFFAOYSA-N 3-prop-2-enoyloxypropane-1-sulfonic acid Chemical compound OS(=O)(=O)CCCOC(=O)C=C NYUTUWAFOUJLKI-UHFFFAOYSA-N 0.000 claims description 3
- AJWDVSJQPIRAKK-UHFFFAOYSA-N 4-ethenyl-1-methylpyridin-1-ium Chemical compound C[N+]1=CC=C(C=C)C=C1 AJWDVSJQPIRAKK-UHFFFAOYSA-N 0.000 claims description 3
- KFDVPJUYSDEJTH-UHFFFAOYSA-N 4-ethenylpyridine Chemical compound C=CC1=CC=NC=C1 KFDVPJUYSDEJTH-UHFFFAOYSA-N 0.000 claims description 3
- ZWAPMFBHEQZLGK-UHFFFAOYSA-N 5-(dimethylamino)-2-methylidenepentanamide Chemical compound CN(C)CCCC(=C)C(N)=O ZWAPMFBHEQZLGK-UHFFFAOYSA-N 0.000 claims description 3
- VJOWMORERYNYON-UHFFFAOYSA-N 5-ethenyl-2-methylpyridine Chemical compound CC1=CC=C(C=C)C=N1 VJOWMORERYNYON-UHFFFAOYSA-N 0.000 claims description 3
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 claims description 3
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 3
- 150000003863 ammonium salts Chemical class 0.000 claims description 3
- WPKYZIPODULRBM-UHFFFAOYSA-N azane;prop-2-enoic acid Chemical compound N.OC(=O)C=C WPKYZIPODULRBM-UHFFFAOYSA-N 0.000 claims description 3
- DZGUJOWBVDZNNF-UHFFFAOYSA-N azanium;2-methylprop-2-enoate Chemical compound [NH4+].CC(=C)C([O-])=O DZGUJOWBVDZNNF-UHFFFAOYSA-N 0.000 claims description 3
- 238000009472 formulation Methods 0.000 claims description 3
- LVHBHZANLOWSRM-UHFFFAOYSA-N itaconic acid Chemical compound OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 claims description 3
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 3
- 239000011976 maleic acid Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 229940047670 sodium acrylate Drugs 0.000 claims description 3
- 159000000000 sodium salts Chemical class 0.000 claims description 3
- SONHXMAHPHADTF-UHFFFAOYSA-M sodium;2-methylprop-2-enoate Chemical compound [Na+].CC(=C)C([O-])=O SONHXMAHPHADTF-UHFFFAOYSA-M 0.000 claims description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 3
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 3
- AJURYMCOXVKKFB-UHFFFAOYSA-M trimethyl(3-prop-2-enoyloxypropyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCOC(=O)C=C AJURYMCOXVKKFB-UHFFFAOYSA-M 0.000 claims description 3
- GXJFCAAVAPZBDY-UHFFFAOYSA-N trimethyl-[2-(2-methylprop-2-enoylamino)ethyl]azanium;chloride Chemical compound [Cl-].CC(=C)C(=O)NCC[N+](C)(C)C GXJFCAAVAPZBDY-UHFFFAOYSA-N 0.000 claims description 3
- UZNHKBFIBYXPDV-UHFFFAOYSA-N trimethyl-[3-(2-methylprop-2-enoylamino)propyl]azanium;chloride Chemical compound [Cl-].CC(=C)C(=O)NCCC[N+](C)(C)C UZNHKBFIBYXPDV-UHFFFAOYSA-N 0.000 claims description 3
- OEIXGLMQZVLOQX-UHFFFAOYSA-N trimethyl-[3-(prop-2-enoylamino)propyl]azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCNC(=O)C=C OEIXGLMQZVLOQX-UHFFFAOYSA-N 0.000 claims description 3
- NPPUWKCCXAPWKH-UHFFFAOYSA-M (4-ethenylphenyl)-trimethylazanium;chloride Chemical compound [Cl-].C[N+](C)(C)C1=CC=C(C=C)C=C1 NPPUWKCCXAPWKH-UHFFFAOYSA-M 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- DZSVIVLGBJKQAP-UHFFFAOYSA-N 1-(2-methyl-5-propan-2-ylcyclohex-2-en-1-yl)propan-1-one Chemical compound CCC(=O)C1CC(C(C)C)CC=C1C DZSVIVLGBJKQAP-UHFFFAOYSA-N 0.000 claims 4
- AGBXYHCHUYARJY-UHFFFAOYSA-N 2-phenylethenesulfonic acid Chemical compound OS(=O)(=O)C=CC1=CC=CC=C1 AGBXYHCHUYARJY-UHFFFAOYSA-N 0.000 claims 2
- WIYVVIUBKNTNKG-UHFFFAOYSA-N 6,7-dimethoxy-3,4-dihydronaphthalene-2-carboxylic acid Chemical compound C1CC(C(O)=O)=CC2=C1C=C(OC)C(OC)=C2 WIYVVIUBKNTNKG-UHFFFAOYSA-N 0.000 claims 2
- BWYYYTVSBPRQCN-UHFFFAOYSA-M sodium;ethenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C=C BWYYYTVSBPRQCN-UHFFFAOYSA-M 0.000 claims 2
- FZGFBJMPSHGTRQ-UHFFFAOYSA-M trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCOC(=O)C=C FZGFBJMPSHGTRQ-UHFFFAOYSA-M 0.000 claims 2
- OIFLLGNCLZLPAF-UHFFFAOYSA-M trimethyl-(5-methyl-4-oxohex-5-enyl)azanium;chloride Chemical compound [Cl-].CC(=C)C(=O)CCC[N+](C)(C)C OIFLLGNCLZLPAF-UHFFFAOYSA-M 0.000 claims 2
- RRHXZLALVWBDKH-UHFFFAOYSA-M trimethyl-[2-(2-methylprop-2-enoyloxy)ethyl]azanium;chloride Chemical compound [Cl-].CC(=C)C(=O)OCC[N+](C)(C)C RRHXZLALVWBDKH-UHFFFAOYSA-M 0.000 claims 2
- CCVMLEHYQVSFOM-UHFFFAOYSA-N trimethyl-[2-(prop-2-enoylamino)ethyl]azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCNC(=O)C=C CCVMLEHYQVSFOM-UHFFFAOYSA-N 0.000 claims 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 229940048053 acrylate Drugs 0.000 claims 1
- 150000001735 carboxylic acids Chemical class 0.000 claims 1
- 150000003460 sulfonic acids Chemical class 0.000 claims 1
- 230000014759 maintenance of location Effects 0.000 abstract description 11
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- 239000006260 foam Substances 0.000 description 7
- 239000007864 aqueous solution Substances 0.000 description 6
- 239000004744 fabric Substances 0.000 description 6
- LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 6
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 5
- 239000000654 additive Substances 0.000 description 5
- 239000007900 aqueous suspension Substances 0.000 description 5
- 239000008367 deionised water Substances 0.000 description 5
- 229910021641 deionized water Inorganic materials 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 239000011111 cardboard Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
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- 230000018044 dehydration Effects 0.000 description 4
- 238000006297 dehydration reaction Methods 0.000 description 4
- 239000002655 kraft paper Substances 0.000 description 4
- 238000004806 packaging method and process Methods 0.000 description 4
- 238000010998 test method Methods 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000009881 electrostatic interaction Effects 0.000 description 3
- 229940015043 glyoxal Drugs 0.000 description 3
- 238000011065 in-situ storage Methods 0.000 description 3
- 230000003993 interaction Effects 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- VVJKKWFAADXIJK-UHFFFAOYSA-N Allylamine Chemical compound NCC=C VVJKKWFAADXIJK-UHFFFAOYSA-N 0.000 description 2
- 229920003043 Cellulose fiber Polymers 0.000 description 2
- 229920001131 Pulp (paper) Polymers 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000000701 coagulant Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 239000008394 flocculating agent Substances 0.000 description 2
- 239000011121 hardwood Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 description 2
- 239000011859 microparticle Substances 0.000 description 2
- ZIWDVJPPVMGJGR-UHFFFAOYSA-N n-ethyl-2-methylprop-2-enamide Chemical compound CCNC(=O)C(C)=C ZIWDVJPPVMGJGR-UHFFFAOYSA-N 0.000 description 2
- 239000011087 paperboard Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
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- 239000011122 softwood Substances 0.000 description 2
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- 125000004178 (C1-C4) alkyl group Chemical group 0.000 description 1
- SJIXRGNQPBQWMK-UHFFFAOYSA-N 2-(diethylamino)ethyl 2-methylprop-2-enoate Chemical group CCN(CC)CCOC(=O)C(C)=C SJIXRGNQPBQWMK-UHFFFAOYSA-N 0.000 description 1
- QHVBLSNVXDSMEB-UHFFFAOYSA-N 2-(diethylamino)ethyl prop-2-enoate Chemical group CCN(CC)CCOC(=O)C=C QHVBLSNVXDSMEB-UHFFFAOYSA-N 0.000 description 1
- JKNCOURZONDCGV-UHFFFAOYSA-N 2-(dimethylamino)ethyl 2-methylprop-2-enoate Chemical group CN(C)CCOC(=O)C(C)=C JKNCOURZONDCGV-UHFFFAOYSA-N 0.000 description 1
- SPPGBVHTKYQNLW-UHFFFAOYSA-N 2-(dimethylamino)ethyl 2-methylprop-2-enoate;sulfuric acid Chemical group OS(O)(=O)=O.CN(C)CCOC(=O)C(C)=C SPPGBVHTKYQNLW-UHFFFAOYSA-N 0.000 description 1
- SSZXAJUPVKMUJH-UHFFFAOYSA-N 2-(dimethylamino)ethyl prop-2-enoate;hydrochloride Chemical group Cl.CN(C)CCOC(=O)C=C SSZXAJUPVKMUJH-UHFFFAOYSA-N 0.000 description 1
- 229920000536 2-Acrylamido-2-methylpropane sulfonic acid Polymers 0.000 description 1
- XHZPRMZZQOIPDS-UHFFFAOYSA-N 2-Methyl-2-[(1-oxo-2-propenyl)amino]-1-propanesulfonic acid Chemical compound OS(=O)(=O)CC(C)(C)NC(=O)C=C XHZPRMZZQOIPDS-UHFFFAOYSA-N 0.000 description 1
- CSYIAHQWGAMMBM-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate;5-phenylpenta-2,4-dienoic acid Chemical compound OCCOC(=O)C=C.OC(=O)C=CC=CC1=CC=CC=C1 CSYIAHQWGAMMBM-UHFFFAOYSA-N 0.000 description 1
- LPNSCOVIJFIXTJ-UHFFFAOYSA-N 2-methylidenebutanamide Chemical compound CCC(=C)C(N)=O LPNSCOVIJFIXTJ-UHFFFAOYSA-N 0.000 description 1
- NLHGHROUDDOASY-UHFFFAOYSA-N 5-(dimethylamino)-2-methylidenepentanamide;methyl hydrogen sulfate Chemical compound COS(O)(=O)=O.CN(C)CCCC(=C)C(N)=O NLHGHROUDDOASY-UHFFFAOYSA-N 0.000 description 1
- TZBHKBVAZQKTKW-UHFFFAOYSA-N 5-(dimethylamino)-2-methylidenepentanamide;sulfuric acid Chemical group OS(O)(=O)=O.CN(C)CCCC(=C)C(N)=O TZBHKBVAZQKTKW-UHFFFAOYSA-N 0.000 description 1
- RNIHAPSVIGPAFF-UHFFFAOYSA-N Acrylamide-acrylic acid resin Chemical compound NC(=O)C=C.OC(=O)C=C RNIHAPSVIGPAFF-UHFFFAOYSA-N 0.000 description 1
- 229920002126 Acrylic acid copolymer Polymers 0.000 description 1
- RUODMMHMXVSXGI-UHFFFAOYSA-M C(=CC1=CC=CC=C1)S(=O)(=O)[O-].C(=C)S(=O)(=O)O.[Na+] Chemical compound C(=CC1=CC=CC=C1)S(=O)(=O)[O-].C(=C)S(=O)(=O)O.[Na+] RUODMMHMXVSXGI-UHFFFAOYSA-M 0.000 description 1
- LEXVCMKNCARLIO-UHFFFAOYSA-N COS(=O)(=O)O.CN(C)CCCC=C(C(=O)N)C Chemical compound COS(=O)(=O)O.CN(C)CCCC=C(C(=O)N)C LEXVCMKNCARLIO-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- MOLSQELXOJIIKB-UHFFFAOYSA-N Cl.CN(C)CCCC=C(C)C(N)=O Chemical group Cl.CN(C)CCCC=C(C)C(N)=O MOLSQELXOJIIKB-UHFFFAOYSA-N 0.000 description 1
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 1
- 102100024008 Glycerol-3-phosphate acyltransferase 1, mitochondrial Human genes 0.000 description 1
- 101000904268 Homo sapiens Glycerol-3-phosphate acyltransferase 1, mitochondrial Proteins 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- OCJYIGYOJCODJL-UHFFFAOYSA-N Meclizine Chemical compound CC1=CC=CC(CN2CCN(CC2)C(C=2C=CC=CC=2)C=2C=CC(Cl)=CC=2)=C1 OCJYIGYOJCODJL-UHFFFAOYSA-N 0.000 description 1
- UTRAYYNGUVDKPZ-UHFFFAOYSA-N S(O)(O)(=O)=O.CN(C)CCCC=C(C(=O)N)C Chemical group S(O)(O)(=O)=O.CN(C)CCCC=C(C(=O)N)C UTRAYYNGUVDKPZ-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
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- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
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- BHDFTVNXJDZMQK-UHFFFAOYSA-N chloromethane;2-(dimethylamino)ethyl 2-methylprop-2-enoate Chemical group ClC.CN(C)CCOC(=O)C(C)=C BHDFTVNXJDZMQK-UHFFFAOYSA-N 0.000 description 1
- WQHCGPGATAYRLN-UHFFFAOYSA-N chloromethane;2-(dimethylamino)ethyl prop-2-enoate Chemical compound ClC.CN(C)CCOC(=O)C=C WQHCGPGATAYRLN-UHFFFAOYSA-N 0.000 description 1
- ZTUMLBMROBHIIH-UHFFFAOYSA-N chloromethylbenzene;2-(dimethylamino)ethyl 2-methylprop-2-enoate Chemical group ClCC1=CC=CC=C1.CN(C)CCOC(=O)C(C)=C ZTUMLBMROBHIIH-UHFFFAOYSA-N 0.000 description 1
- 238000010668 complexation reaction Methods 0.000 description 1
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- 238000007791 dehumidification Methods 0.000 description 1
- JCRDPEHHTDKTGB-UHFFFAOYSA-N dimethyl-[2-(2-methylprop-2-enoyloxy)ethyl]azanium;chloride Chemical group Cl.CN(C)CCOC(=O)C(C)=C JCRDPEHHTDKTGB-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
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- SUPCQIBBMFXVTL-UHFFFAOYSA-N ethyl 2-methylprop-2-enoate Chemical compound CCOC(=O)C(C)=C SUPCQIBBMFXVTL-UHFFFAOYSA-N 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
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- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
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- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
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- JZMJDSHXVKJFKW-UHFFFAOYSA-M methyl sulfate(1-) Chemical compound COS([O-])(=O)=O JZMJDSHXVKJFKW-UHFFFAOYSA-M 0.000 description 1
- IHBKAGRPNRKYAO-UHFFFAOYSA-M methyl sulfate;trimethyl-[2-(2-methylprop-2-enoyloxy)ethyl]azanium Chemical compound COS([O-])(=O)=O.CC(=C)C(=O)OCC[N+](C)(C)C IHBKAGRPNRKYAO-UHFFFAOYSA-M 0.000 description 1
- VQGWOOIHSXNRPW-UHFFFAOYSA-N n-butyl-2-methylprop-2-enamide Chemical compound CCCCNC(=O)C(C)=C VQGWOOIHSXNRPW-UHFFFAOYSA-N 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
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- 238000007645 offset printing Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920000962 poly(amidoamine) Polymers 0.000 description 1
- 239000002952 polymeric resin Substances 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229920013730 reactive polymer Polymers 0.000 description 1
- 239000012758 reinforcing additive Substances 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- CYFLXLSBHQBMFT-UHFFFAOYSA-N sulfamoxole Chemical group O1C(C)=C(C)N=C1NS(=O)(=O)C1=CC=C(N)C=C1 CYFLXLSBHQBMFT-UHFFFAOYSA-N 0.000 description 1
- 239000005031 sulfite paper Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 238000009864 tensile test Methods 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/41—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing ionic groups
- D21H17/42—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing ionic groups anionic
- D21H17/43—Carboxyl groups or derivatives thereof
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/37—Polymers of unsaturated acids or derivatives thereof, e.g. polyacrylates
- D21H17/375—Poly(meth)acrylamide
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/41—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing ionic groups
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/06—Paper forming aids
- D21H21/10—Retention agents or drainage improvers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/18—Reinforcing agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/18—Reinforcing agents
- D21H21/20—Wet strength agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H23/00—Processes or apparatus for adding material to the pulp or to the paper
- D21H23/02—Processes or apparatus for adding material to the pulp or to the paper characterised by the manner in which substances are added
- D21H23/04—Addition to the pulp; After-treatment of added substances in the pulp
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H23/00—Processes or apparatus for adding material to the pulp or to the paper
- D21H23/02—Processes or apparatus for adding material to the pulp or to the paper characterised by the manner in which substances are added
- D21H23/22—Addition to the formed paper
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paper (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/087,038 US9347181B2 (en) | 2013-11-22 | 2013-11-22 | Method for increasing paper strength |
| US14/087,038 | 2013-11-22 | ||
| PCT/FI2014/050896 WO2015075318A1 (en) | 2013-11-22 | 2014-11-24 | Method for increasing paper strength |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2667287C1 true RU2667287C1 (ru) | 2018-09-18 |
Family
ID=52117905
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2016119058A RU2667287C1 (ru) | 2013-11-22 | 2014-11-24 | Способ повышения прочности бумаги |
| RU2016119058D RU2016119058A (ru) | 2013-11-22 | 2014-11-24 | Способ повышения прочности бумаги |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2016119058D RU2016119058A (ru) | 2013-11-22 | 2014-11-24 | Способ повышения прочности бумаги |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9347181B2 (https=) |
| EP (1) | EP3071751B1 (https=) |
| JP (1) | JP2016539256A (https=) |
| KR (2) | KR102377934B1 (https=) |
| CN (1) | CN105899729B (https=) |
| AU (1) | AU2014351736B2 (https=) |
| BR (1) | BR112016011477B1 (https=) |
| CA (1) | CA2931193C (https=) |
| ES (1) | ES2907276T3 (https=) |
| NZ (1) | NZ720188A (https=) |
| PL (1) | PL3071751T3 (https=) |
| PT (1) | PT3071751T (https=) |
| RU (2) | RU2667287C1 (https=) |
| WO (1) | WO2015075318A1 (https=) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8088250B2 (en) | 2008-11-26 | 2012-01-03 | Nalco Company | Method of increasing filler content in papermaking |
| FI125714B (en) * | 2012-11-12 | 2016-01-15 | Kemira Oyj | A process for treating fibrous pulp for making paper, cardboard or the like, and a product |
| FI125712B (en) * | 2012-11-13 | 2016-01-15 | Kemira Oyj | Paper-making material and its use |
| US9562326B2 (en) * | 2013-03-14 | 2017-02-07 | Kemira Oyj | Compositions and methods of making paper products |
| US9567708B2 (en) * | 2014-01-16 | 2017-02-14 | Ecolab Usa Inc. | Wet end chemicals for dry end strength in paper |
| US10435843B2 (en) * | 2016-02-16 | 2019-10-08 | Kemira Oyj | Method for producing paper |
| CN109072556A (zh) * | 2016-02-16 | 2018-12-21 | 凯米罗总公司 | 制造纸的方法 |
| CA3014062A1 (en) * | 2016-02-26 | 2017-08-31 | Buckman Laboratories International, Inc. | Glyoxalated polyacrylamide terpolymer, base copolymer thereof, compositions containing same, uses in papermaking and products thereof |
| AU2016395426C1 (en) | 2016-02-29 | 2021-01-21 | Kemira Oyj | A softener composition |
| WO2018063273A1 (en) * | 2016-09-30 | 2018-04-05 | Kemira Oyj | Drainage system and process for manufacturing paper product or the like |
| WO2018122443A1 (en) * | 2016-12-28 | 2018-07-05 | Kemira Oyj | Glyoxylated polyacrylamide polymer composition, its use and method for increasing the strength properties of paper, board or the like |
| PL3638845T3 (pl) | 2017-06-16 | 2025-07-21 | Kemira Oyj | Układ dodatków zwiększających wytrzymałość i sposób wytwarzania wstęgi zawierającej włókna celulozowe |
| WO2018229345A1 (en) | 2017-06-16 | 2018-12-20 | Kemira Oyj | Strength additive system and method for manufacturing a web comprising cellulosic fibres |
| CN111183255A (zh) | 2017-09-29 | 2020-05-19 | 凯米拉公司 | 表面处理组合物、其用途及纸、纸板或类似物的制造方法 |
| MX2020007581A (es) * | 2018-01-16 | 2020-09-03 | Solenis Tech Lp | Proceso para producir papel con retencion de relleno y opacidad mejoradas mientras mantiene la resistencia a la tension en condiciones de humedad. |
| MX2020010472A (es) * | 2018-04-04 | 2021-01-08 | Solenis Tech Lp | Aplicacion asistida con espuma de aditivos de resistencia a los productos de papel. |
| EP3947814B1 (en) | 2019-04-02 | 2026-02-18 | Kemira Oyj | Paper strength improvement using metal chelates and synthetic cationic polymers |
| CN110230231A (zh) * | 2019-06-17 | 2019-09-13 | 联盛纸业（龙海）有限公司 | 一种纱管纸及其制备工艺 |
| CN111074688A (zh) * | 2019-12-30 | 2020-04-28 | 玖龙纸业（东莞）有限公司 | 一种高强度牛卡纸及其生产工艺 |
| US12553188B2 (en) * | 2020-03-18 | 2026-02-17 | Kemira Oyj | GPAM compositions and methods |
| BR112022017487A2 (pt) * | 2020-03-18 | 2022-10-18 | Kemira Oyj | Composições e métodos para resistência úmida e seca aumentada |
| KR20230108277A (ko) | 2020-12-02 | 2023-07-18 | 케미라 오와이제이 | 종이, 판지 등의 제조를 위한 처리 시스템 |
| EP4262498A4 (en) | 2020-12-17 | 2024-04-24 | First Quality Tissue, LLC | Wet laid disposable absorent structures with high wet strenght and method of making the same |
| CN117157001A (zh) * | 2020-12-17 | 2023-12-01 | 优质纸巾有限公司 | 具有高湿强度的湿法成网一次性吸收结构及其制造方法 |
| CN112900145B (zh) * | 2021-01-12 | 2023-01-20 | 赵慧哲 | 一种超薄热升华转印纸及其制备方法 |
| FI4036305T3 (fi) * | 2021-02-02 | 2024-01-31 | Billerud Ab Publ | Paperinvalmistusmenetelmä |
| US20240110337A1 (en) * | 2021-02-02 | 2024-04-04 | Billerud Aktiebolag (Publ) | Papermaking Method |
| EP4202119B8 (en) * | 2021-12-22 | 2025-11-26 | Billerud Aktiebolag (publ) | Recyclable paper of high wet strength |
| US20240344271A1 (en) * | 2021-08-30 | 2024-10-17 | Ecolab Usa Inc. | Use of modified lignin as a wet end strength additive |
| CA3243785A1 (en) * | 2022-02-14 | 2023-08-17 | Kemira Oyj | HIGH MOLECULAR MASS GPAM WITH ANIONIC POLYMER PROMOTER |
| AU2023219719A1 (en) * | 2022-02-14 | 2024-08-15 | Kemira Oyj | High molecular weight gpam with anionic polysaccharide promoter |
| PT117820B (pt) | 2022-02-28 | 2024-02-27 | Univ De Coimbra | Método de produção de papel tissue |
| WO2023244871A1 (en) | 2022-06-16 | 2023-12-21 | First Quality Tissue, Llc | Wet laid paper and paperboard products with high wet strength and method of making the same |
| US11952721B2 (en) | 2022-06-16 | 2024-04-09 | First Quality Tissue, Llc | Wet laid disposable absorbent structures with high wet strength and method of making the same |
| WO2023245090A1 (en) | 2022-06-16 | 2023-12-21 | First Quality Tissue, Llc | Wet laid paper and paperboard products with high wet strength and method of making the same |
| CN116180486A (zh) * | 2023-02-24 | 2023-05-30 | 山东金蔡伦纸业有限公司 | 一种造纸湿部化学品 |
| CN121194998A (zh) * | 2023-04-04 | 2025-12-23 | 索理思科技开曼公司 | 用于造纸的添加剂组合物 |
| EP4603639A1 (en) * | 2024-02-16 | 2025-08-20 | Smurfit Kappa Services Limited | Packaging material and method of wrapping articles |
| WO2026015766A1 (en) * | 2024-07-12 | 2026-01-15 | Kemira Oyj | Flushable tissue products |
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| US4079043A (en) * | 1974-11-04 | 1978-03-14 | Hercules Incorporated | Glyoxal modified poly(beta-alanine) strengthening resins for use in paper |
| US4605702A (en) * | 1984-06-27 | 1986-08-12 | American Cyanamid Company | Temporary wet strength resin |
| RU2318088C2 (ru) * | 2001-08-20 | 2008-02-27 | Армстронг Уорлд Индастриз, Инк. | Связующие вещества для волкнистых листов |
| US20090165978A1 (en) * | 2004-08-17 | 2009-07-02 | Georgia-Pacific Chemicals Llc | Blends of glyoxalated polyacrylamides and paper strengthening agents |
| US20120118523A1 (en) * | 2010-11-15 | 2012-05-17 | Kemira Oyj | Composition and Process for Increasing the Dry Strength of a Paper Product |
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| BRPI0513054A (pt) | 2004-07-08 | 2008-07-15 | Lanxess Corp | resinas com resistência de elevado desempenho em indústrias de fabricação de papel |
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| MX2007007396A (es) | 2004-12-21 | 2007-08-14 | Hercules Inc | Resinas cationicas reactivas para usarse como agentes de resistencia secos y humedos en sistemas de fabricacion de papel que contienen iones sulfito. |
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| CN103930619B (zh) * | 2011-08-25 | 2016-12-07 | 索理思科技开曼公司 | 增加强度助剂在制造纸和纸板中的优势的方法 |
| WO2013179139A1 (en) | 2012-05-30 | 2013-12-05 | Kemira Oyj | Compositions and methods of making paper products |
| CA2876651C (en) * | 2012-06-22 | 2018-10-09 | Kemira Oyj | Compositions and methods of making paper products |
-
2013
- 2013-11-22 US US14/087,038 patent/US9347181B2/en active Active
-
2014
- 2014-11-24 NZ NZ720188A patent/NZ720188A/en unknown
- 2014-11-24 KR KR1020167016475A patent/KR102377934B1/ko active Active
- 2014-11-24 RU RU2016119058A patent/RU2667287C1/ru not_active IP Right Cessation
- 2014-11-24 KR KR1020227008961A patent/KR102492250B1/ko active Active
- 2014-11-24 WO PCT/FI2014/050896 patent/WO2015075318A1/en not_active Ceased
- 2014-11-24 PT PT148149040T patent/PT3071751T/pt unknown
- 2014-11-24 RU RU2016119058D patent/RU2016119058A/ru unknown
- 2014-11-24 BR BR112016011477-9A patent/BR112016011477B1/pt active IP Right Grant
- 2014-11-24 PL PL14814904T patent/PL3071751T3/pl unknown
- 2014-11-24 CN CN201480073537.9A patent/CN105899729B/zh active Active
- 2014-11-24 CA CA2931193A patent/CA2931193C/en active Active
- 2014-11-24 EP EP14814904.0A patent/EP3071751B1/en active Active
- 2014-11-24 ES ES14814904T patent/ES2907276T3/es active Active
- 2014-11-24 AU AU2014351736A patent/AU2014351736B2/en not_active Ceased
- 2014-11-24 JP JP2016532518A patent/JP2016539256A/ja not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4079043A (en) * | 1974-11-04 | 1978-03-14 | Hercules Incorporated | Glyoxal modified poly(beta-alanine) strengthening resins for use in paper |
| US4605702A (en) * | 1984-06-27 | 1986-08-12 | American Cyanamid Company | Temporary wet strength resin |
| RU2318088C2 (ru) * | 2001-08-20 | 2008-02-27 | Армстронг Уорлд Индастриз, Инк. | Связующие вещества для волкнистых листов |
| US20090165978A1 (en) * | 2004-08-17 | 2009-07-02 | Georgia-Pacific Chemicals Llc | Blends of glyoxalated polyacrylamides and paper strengthening agents |
| US20120118523A1 (en) * | 2010-11-15 | 2012-05-17 | Kemira Oyj | Composition and Process for Increasing the Dry Strength of a Paper Product |
Also Published As
| Publication number | Publication date |
|---|---|
| AU2014351736B2 (en) | 2017-09-21 |
| BR112016011477A2 (pt) | 2017-08-08 |
| CN105899729A (zh) | 2016-08-24 |
| AU2014351736A1 (en) | 2016-06-09 |
| US9347181B2 (en) | 2016-05-24 |
| US20150144282A1 (en) | 2015-05-28 |
| KR102492250B1 (ko) | 2023-01-26 |
| NZ720188A (en) | 2019-01-25 |
| ES2907276T3 (es) | 2022-04-22 |
| JP2016539256A (ja) | 2016-12-15 |
| CA2931193C (en) | 2023-04-04 |
| CA2931193A1 (en) | 2015-05-28 |
| EP3071751A1 (en) | 2016-09-28 |
| KR20220038543A (ko) | 2022-03-28 |
| BR112016011477B1 (pt) | 2021-12-21 |
| EP3071751B1 (en) | 2022-01-05 |
| PL3071751T3 (pl) | 2022-04-25 |
| KR102377934B1 (ko) | 2022-03-23 |
| PT3071751T (pt) | 2022-02-21 |
| CN105899729B (zh) | 2018-11-13 |
| RU2016119058A (ru) | 2017-12-25 |
| KR20160089433A (ko) | 2016-07-27 |
| WO2015075318A1 (en) | 2015-05-28 |
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| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20201125 |