RU2016114308A - FLUOROPHORUS AND METHOD FOR PRODUCING A SALTINE DEPOSITION INHIBITOR CONTAINING A FLUOROPHOR AS A FLUORESCENT TAG - Google Patents

FLUOROPHORUS AND METHOD FOR PRODUCING A SALTINE DEPOSITION INHIBITOR CONTAINING A FLUOROPHOR AS A FLUORESCENT TAG Download PDF

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RU2016114308A
RU2016114308A RU2016114308A RU2016114308A RU2016114308A RU 2016114308 A RU2016114308 A RU 2016114308A RU 2016114308 A RU2016114308 A RU 2016114308A RU 2016114308 A RU2016114308 A RU 2016114308A RU 2016114308 A RU2016114308 A RU 2016114308A
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Russia
Prior art keywords
producing
fluorophorus
saltine
fluorophor
inhibitor containing
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RU2016114308A
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Russian (ru)
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RU2640339C2 (en
Inventor
Семен Дмитриевич Камагуров
Наталья Евгеньевна Ковалева
Максим Сергеевич Ощепков
Константин Иванович Попов
Сергей Витальевич Ткаченко
Елена Сергеевна Старкова
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Публичное акционерное общество Научный центр "Малотоннажная химия"
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Priority to RU2016114308A priority Critical patent/RU2640339C2/en
Publication of RU2016114308A publication Critical patent/RU2016114308A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/06—Luminescent, e.g. electroluminescent, chemiluminescent materials containing organic luminescent materials
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
    • C02F1/56—Macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/04—Acids; Metal salts or ammonium salts thereof
    • C08F220/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B57/00—Other synthetic dyes of known constitution
    • C09B57/12—Perinones, i.e. naphthoylene-aryl-imidazoles
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B57/00—Other synthetic dyes of known constitution
    • C09B57/14—Benzoxanthene dyes; Benzothioxanthene dyes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Hydrology & Water Resources (AREA)
  • Health & Medical Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Materials Engineering (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Claims (9)

1. Флуорофор, содержащий двойную связь в соединении общей формулы 1:1. Fluorophore containing a double bond in the compound of General formula 1:
Figure 00000001
Figure 00000001
 1, R=H1, R = H 2, R=Br, где2, R = Br, where R=H или R=BrR = H or R = Br или формулы 2:or formula 2:
Figure 00000002
, где
Figure 00000002
where
Figure 00000003
или R1=Оме.
Figure 00000003
or R 1 = Ohm. 2. Способ получения ингибитора солеотложений, содержащего связанную флуоресцентную метку, заключается в том, что проводят радикальную сополимеризацию компонентов, отличающийся тем, что проводят радикальную сополимеризацию акриловой кислоты, моноэфира фумаровой кислоты и соединения формулы 1 или 2 по п. 1 в водной среде при нагревании в присутствии инициатора, сополимеризацию проводят при массовом содержании моноэфира фумаровой кислоты от 2 до 80% от общей массы мономеров и массовом содержании флуорофора от 1 до 10% от общей массы мономеров, а остальное составляет акриловая кислота, причем последняя представляет собой водный раствор с массовой долей мономеров от 15 до 30%.2. A method of producing a scale inhibitor containing an associated fluorescent label consists in the radical copolymerization of components, characterized in that the radical copolymerization of acrylic acid, fumaric acid monoester and a compound of formula 1 or 2 according to claim 1 is carried out in an aqueous medium under heating in the presence of an initiator, copolymerization is carried out with a mass content of fumaric acid monoester from 2 to 80% of the total weight of monomers and a mass content of fluorophore from 1 to 10% of the total weight of monomers, the rest is acrylic acid, the latter is an aqueous solution of monomers with a mass fraction of from 15 to 30%.
RU2016114308A 2016-04-13 2016-04-13 Fluorophor and method for obtaining salt inhibitor containing fluorofor as fluorescent mark RU2640339C2 (en)

Priority Applications (1)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2699104C1 (en) * 2018-07-18 2019-09-03 Акционерное общество Научный центр "Малотоннажная химия" Novel fluorescent derivatives of α-hydroxy-bisphosphonates as scale inhibitors and methods of producing same
EP3977104A4 (en) 2019-05-28 2023-08-16 Nouryon Chemicals International B.V. Method of controlling scale in aqueous systems

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* Cited by examiner, † Cited by third party
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DE10228628A1 (en) * 2002-06-26 2004-01-22 Stockhausen Gmbh & Co. Kg Copolymers to avoid deposits in water-bearing systems, their production and use
CN101289257A (en) * 2008-05-29 2008-10-22 东南大学 Fluorescence labeling polyether carboxyl acids antisludging agent and preparation
CN102786152A (en) * 2012-08-01 2012-11-21 东南大学 Fluorescently labeled phosphorus-free environment-friendly polyether water treatment agent and preparation method thereof
CN102910744B (en) * 2012-08-01 2013-12-11 东南大学 Fluorescent tracing green environmental-friendly polyglycol ether water treatment agent and preparation method thereof
CN102807286B (en) * 2012-08-01 2013-11-20 东南大学 Fluorescent-traced green and environment-friendly polyether corrosion and scale inhibiting and dispersing agent and preparation method thereof
CN102910745B (en) * 2012-08-01 2014-01-01 东南大学 Fluorescent tracing green environmental-friendly polyglycol type water treatment agent and preparation method thereof
CN103159333B (en) * 2013-03-26 2014-07-09 东南大学 Fluorescent marking polyether carboxylate environment-friendly corrosion/scale inhibitor

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