RU2016111708A - The method of preparation and composition for obtaining dry forms of blue anthocyanins - Google Patents

The method of preparation and composition for obtaining dry forms of blue anthocyanins Download PDF

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Publication number
RU2016111708A
RU2016111708A RU2016111708A RU2016111708A RU2016111708A RU 2016111708 A RU2016111708 A RU 2016111708A RU 2016111708 A RU2016111708 A RU 2016111708A RU 2016111708 A RU2016111708 A RU 2016111708A RU 2016111708 A RU2016111708 A RU 2016111708A
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RU
Russia
Prior art keywords
matrix
anthocyanins
spray drying
extraction
extract
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RU2016111708A
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Russian (ru)
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RU2639291C2 (en
Inventor
Людмила Александровна Дейнека
Виктор Иванович Дейнека
Михаил Олегович Костенко
Артем Николаевич Сидоров
Елена Юрьевна Олейниц
Original Assignee
Федеральное государственное автономное образовательное учреждение высшего образования "Белгородский государственный национальный исследовательский университет" (НИУ "БелГУ")
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Priority to RU2016111708A priority Critical patent/RU2639291C2/en
Publication of RU2016111708A publication Critical patent/RU2016111708A/en
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Publication of RU2639291C2 publication Critical patent/RU2639291C2/en

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/40Colouring or decolouring of foods
    • A23L5/42Addition of dyes or pigments, e.g. in combination with optical brighteners
    • A23L5/43Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • B01J13/04Making microcapsules or microballoons by physical processes, e.g. drying, spraying
    • B01J13/043Drying and spraying

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Claims (3)

1. Способ получения сухих инкапсулированных в полисахаридную матрицу форм антоцианов синего цвета методом распылительной сушки, включающий экстракцию антоцианов из растительного сырья, смешивание экстракта с матрицей и распылительную сушку, отличающийся тем, что экстракцию проводят водно-этанольным раствором в объемном соотношении 70:30, после чего полученный экстракт фильтруют и упаривают, затем к выбранному количеству выбранной матрицы добавляют выбранное количество полученного концентрата антоцианов, смесь перемешивают до получения однородной массы и подвергают высушиванию методом распылительной сушки при следующих параметрах: скорость впрыска – 600 мл/час; расход воздуха – 9 м3/мин; температура впрыска – 120°С; температура на выходе – 70-80°С.1. A method of producing dry blue-colored anthocyanins encapsulated in a polysaccharide matrix by spray drying, including the extraction of anthocyanins from plant materials, mixing the extract with the matrix and spray drying, characterized in that the extraction is carried out with an aqueous-ethanol solution in a volume ratio of 70:30, after whereupon the obtained extract is filtered and evaporated, then the selected amount of the obtained anthocyanins concentrate is added to the selected amount of the selected matrix, the mixture is stirred until obtained a homogeneous mass and is subjected to drying by spray drying with the following parameters: injection speed - 600 ml / hour; air consumption - 9 m 3 / min; injection temperature - 120 ° C; outlet temperature - 70-80 ° С. 2. Способ получения сухих инкапсулированных в полисахаридную матрицу форм антоцианов синего цвета методом распылительной сушки, включающий экстракцию антоцианов из растительного сырья, смешивание экстракта с матрицей и распылительную сушку, отличающийся тем, что экстракцию проводят экстрагентом – 0,1 М водным раствором соляной кислоты, после чего полученный экстракт фильтруют, очищают от балластных веществ, упаривают и подщелачивают раствором гидроксида натрия или калия до нейтральной среды, затем к выбранному количеству выбранной матрицы добавляют выбранное количество полученного концентрата антоцианов, смесь перемешивают до получения однородной массы и подвергают высушиванию методом распылительной сушки при следующих параметрах: скорость впрыска – 600 мл/час; расход воздуха – 9 м3/мин; температура впрыска – 120°С; температура на выходе – 70-80°С.2. A method of obtaining dry blue-colored anthocyanin forms encapsulated in a polysaccharide matrix by spray drying, including the extraction of anthocyanins from plant materials, mixing the extract with the matrix and spray drying, characterized in that the extraction is carried out with an extractant - 0.1 M aqueous hydrochloric acid, after then the resulting extract was filtered, purified on roughage, evaporated and basified with sodium hydroxide or potassium hydroxide until a neutral medium, then the selected number of the selected m the matrix of the selected added quantity of anthocyanin obtained concentrate, and the mixture was stirred until a homogeneous mass is subjected to drying and spray-dried with the following parameters: injection rate - 600 ml / hour; air consumption - 9 m 3 / min; injection temperature - 120 ° C; outlet temperature - 70-80 ° С. 3. Состав для получения сухих инкапсулированных в полисахаридную матрицу форм антоцианов синего цвета методом распылительной сушки, характеризующийся тем, что он включает концентрат антоцианов и матрицу, взятые в соотношении от 1:9 до 1:185, причем в качестве матрицы используют полисахариды, разрешенные к использованию в пищевой промышленности и образующие инкапсулированные формы с антоцианами. 3. The composition for producing dry blue-colored anthocyanin forms encapsulated in a polysaccharide matrix by spray drying, characterized in that it includes anthocyanin concentrate and a matrix taken in a ratio of 1: 9 to 1: 185, and polysaccharides allowed to be used as a matrix use in the food industry and encapsulating forms with anthocyanins.
RU2016111708A 2016-03-29 2016-03-29 Method and composition of producing dry forms of blue anthocyanins RU2639291C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2016111708A RU2639291C2 (en) 2016-03-29 2016-03-29 Method and composition of producing dry forms of blue anthocyanins

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Application Number Priority Date Filing Date Title
RU2016111708A RU2639291C2 (en) 2016-03-29 2016-03-29 Method and composition of producing dry forms of blue anthocyanins

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RU2016111708A true RU2016111708A (en) 2017-10-04
RU2639291C2 RU2639291C2 (en) 2017-12-20

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112931764A (en) * 2021-02-08 2021-06-11 陕西师范大学 Method for preparing microcapsule based on alfalfa flower anthocyanin

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2719784C1 (en) * 2019-06-20 2020-04-23 Общество с ограниченной ответственностью "Грумант" Method for preparing dry forms of anthocyanins using two-step extraction

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2294114C2 (en) * 2002-05-27 2007-02-27 Эдванс Холдингз Лимитед Food supplement from vinasse, uses of combination of antioxidant complexes from vinasse with bioavailability promoters and method for production of food supplement
RU2294348C2 (en) * 2004-11-19 2007-02-27 Светлана Николаевна Бутова Method for production of natural anthocyanic food-grade colorant from maize waste and obtained anthocyanic food-grade colorant
WO2011024049A2 (en) * 2009-08-26 2011-03-03 Glenmark Pharmaceuticals Ltd Method for producing proanthocyanidin polymer compositions for pharmaceutical formulations
CN102488158B (en) * 2011-12-26 2013-06-19 江苏省农业科学院 Blackberry anthocyanin microcapsules and preparation method thereof
CN103251674B (en) * 2013-05-30 2015-04-01 南京林业大学 Black wattle bark proanthocyanidin microcapsule and preparation method thereof
CN103725038A (en) * 2013-12-23 2014-04-16 江苏省中国科学院植物研究所 Preparation method of blackberry pigment microcapsules

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112931764A (en) * 2021-02-08 2021-06-11 陕西师范大学 Method for preparing microcapsule based on alfalfa flower anthocyanin

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Effective date: 20210330