RU2014104697A - Соединение термопластичного материала с металлом - Google Patents

Соединение термопластичного материала с металлом Download PDF

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RU2014104697A
RU2014104697A RU2014104697/05A RU2014104697A RU2014104697A RU 2014104697 A RU2014104697 A RU 2014104697A RU 2014104697/05 A RU2014104697/05 A RU 2014104697/05A RU 2014104697 A RU2014104697 A RU 2014104697A RU 2014104697 A RU2014104697 A RU 2014104697A
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sol
gel solution
propoxide
zirconium
butanol
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RU2014104697/05A
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RU2657500C2 (ru
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Кай Янгдал БЛОХОВИАК
Кристин Л. КРИК
Роберт А. АНДЕРСОН
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Зе Боинг Компани
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    • C—CHEMISTRY; METALLURGY
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    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/06—Non-macromolecular additives organic
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    • B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
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    • B29C65/48—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor using adhesives, i.e. using supplementary joining material; solvent bonding
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    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
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Abstract

1. Способ, включающий:выдерживание н-пропоксида циркония (336) в растворителе (342) с получением первой части золь-гелевого раствора (334);объединение указанной первой части с деионизированной водой (340) с получением второй части золь-гелевого раствора (334);объединение аминоарилтриалкоксисилана (338) со спиртом (344) с получением третьей части золь-гелевого раствора (334);объединение указанной третьей части с указанной второй частью с получением смеси для золь-гелевого раствора (334);объединение деионизированной воды (340), или спирта (344), или их комбинации с указанной смесью с получением раствора; ивыдерживание указанного раствора с формированием золь-гелевого раствора (334), содержащего н-пропоксид циркония (336) и аминоарилтриалкоксисилан (338) в равновесном молярном соотношении, которое составляет приблизительно 1:5.2. Способ по п. 1, отличающийся тем, что выдерживание н-пропоксида циркония (336) в растворителе (342) с получением первой части включает перемешивание вращением н-пропоксида циркония (336) в растворителе (342) в течение тридцати минут при комнатной температуре.3. Способ по п. 1, отличающийся тем, что выдерживание указанного раствора с получением золь-гелевого раствора (334) включает перемешивание указанного раствора с помощью мешалки в течение четырех часов при комнатной температуре.4. Способ по п. 1, отличающийся тем, что спирт (344) выбран из группы, состоящей из изопропилового спирта, метанола, этанола, пропанола, н-бутанола (1-бутанола), втор-бутанола (2-бутанола), изобутанола (2-метил-1-пропанола), трет-бутанола (2-метил-2-пропанола) и 3-метил-2-бутанола.5. Способ по п. 1, отличающийся тем, что растворитель (342) выбран из группы, состоящей из л

Claims (15)

1. Способ, включающий:
выдерживание н-пропоксида циркония (336) в растворителе (342) с получением первой части золь-гелевого раствора (334);
объединение указанной первой части с деионизированной водой (340) с получением второй части золь-гелевого раствора (334);
объединение аминоарилтриалкоксисилана (338) со спиртом (344) с получением третьей части золь-гелевого раствора (334);
объединение указанной третьей части с указанной второй частью с получением смеси для золь-гелевого раствора (334);
объединение деионизированной воды (340), или спирта (344), или их комбинации с указанной смесью с получением раствора; и
выдерживание указанного раствора с формированием золь-гелевого раствора (334), содержащего н-пропоксид циркония (336) и аминоарилтриалкоксисилан (338) в равновесном молярном соотношении, которое составляет приблизительно 1:5.
2. Способ по п. 1, отличающийся тем, что выдерживание н-пропоксида циркония (336) в растворителе (342) с получением первой части включает перемешивание вращением н-пропоксида циркония (336) в растворителе (342) в течение тридцати минут при комнатной температуре.
3. Способ по п. 1, отличающийся тем, что выдерживание указанного раствора с получением золь-гелевого раствора (334) включает перемешивание указанного раствора с помощью мешалки в течение четырех часов при комнатной температуре.
4. Способ по п. 1, отличающийся тем, что спирт (344) выбран из группы, состоящей из изопропилового спирта, метанола, этанола, пропанола, н-бутанола (1-бутанола), втор-бутанола (2-бутанола), изобутанола (2-метил-1-пропанола), трет-бутанола (2-метил-2-пропанола) и 3-метил-2-бутанола.
5. Способ по п. 1, отличающийся тем, что растворитель (342) выбран из группы, состоящей из ледяной уксусной кислоты, гликолей, гликолевых простых эфиров и бутилового сложного эфира.
6. Способ по любому из пп. 1-5, отличающийся тем, что золь-гелевый раствор (334) содержит н-пропоксид циркония (336) в количестве примерно от 0,005% до 8,10% в молярных процентах.
7. Способ по любому из пп. 1-5, отличающийся тем, что минимальное молярное соотношение между спиртом (344) и аминоарилтриалкоксисиланом (338) в золь-гелевом растворе (334) составляет приблизительно 18:1, при этом минимальное молярное соотношение между деионизированной водой (340) и аминоарилтриалкоксисиланом (336) в золь-гелевом растворе (334) составляет приблизительно 18:1.
8. Способ по любому из пп. 1-5, дополнительно включающий перед выдерживанием н-пропоксида циркония (336) в растворителе (342) перемешивание вращением н-пропоксида циркония (336) в растворителе (342), и где:
выдерживание н-пропоксида циркония (336) в растворителе (342) с получением первой части включает перемешивание вращением в течение тридцати минут при комнатной температуре, при этом растворитель (342) содержит ледяную уксусную кислоту;
выдерживание раствора с получением золь-гелевого раствора (334) включает перемешивание в течение четырех часов при комнатной температуре;
объединение аминоарилтриалкоксисилана (338) со спиртом (344) с получением третьей части золь-гелевого раствора (334) включает объединение аминоарилтриалкоксисилана (338) с изопропиловым спиртом; и
выдерживание раствора с получением золь-гелевого раствора (334), содержащего н-пропоксид циркония (336) и аминоарилтриалкоксисилан (338) в равновесном молярном соотношении, составляющем приблизительно 1:5, дополнительно включает золь-гелевый раствор (334), содержащий примерно от 0,005% до 8,10% н-пропоксида циркония (336) в молярных процентах.
9. Способ по любому из пп. 1-5, дополнительно включающий:
очистку металла;
предварительную обработку металла;
нанесение золь-гелевого раствора (334) на металл;
высушивание в печи золь-гелевого раствора (334) на металле с получением металла (502) с обработанной поверхностью;
сборку термопластичного материала и металла с обработанной поверхностью (502); и
склеивание термопластичного материала с металлом с обработанной поверхностью (502), где металл выбран из группы, состоящей из титана, титановых сплавов, алюминиевых сплавов, никелевых сплавов, сплавов нержавеющих сталей и медных сплавов.
10. Золь-гелевый раствор (334), содержащий:
н-пропоксида циркония (336);
аминоарилтриалкоксисилан (338), где золь-гелевый раствор (334) содержит н-пропоксид циркония (336) и аминоарилтриалкоксисилан (338) в равновесном молярном соотношении, составляющем приблизительно 1:5;
растворитель (342);
спирт (344); и
деионизированную воду (340).
11. Золь-гелевый раствор (334) по п. 10, отличающийся тем, что равновесное молярное соотношение между н-пропоксидом циркония (336) и аминоарилтриалкоксисиланом (338) в золь-гелевом растворе (334) составляет приблизительно 1:5.
12. Золь-гелевый раствор (334) по п. 10, отличающийся тем, что минимальное равновесное молярное соотношение между спиртом (344) и аминоарилтриалкоксисиланом (338) в золь-гелевом растворе (334) составляет приблизительно 18:1; при этом минимальное равновесное молярное соотношение между деионизированной водой (340) и н-пропоксидом циркония (336) в золь-гелевом растворе (334) составляет приблизительно 18:1.
13. Золь-гелевый раствор (334) по любому из пп. 10-12, отличающийся тем, что спирт (344) имеет низкую молекулярную массу и легко испаряется.
14. Золь-гелевый раствор (334) по любому из пп. 10-12, отличающийся тем, что спирт (344) выбран из группы, состоящей из изопропилового спирта, метанола, этанола, пропанола, н-бутанола (1-бутанола), втор-бутанола (2-бутанола), изобутанола (2-метил-1-пропанола), трет-бутанола (2-метил-2-пропанола) и 3-метил-2-бутанола.
15. Золь-гелевый раствор (334) по любому из пп. 10-12, отличающийся тем, что растворитель (342) выбран из группы, состоящей из ледяной уксусной кислоты, гликолей, гликолевых простых эфиров и бутилового сложного эфира.
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