RU2013149722A - METHOD FOR PRODUCING BIS- (ENDO-Bicyclo [4.2.1] NONA-2,4-DIENOV) - Google Patents

METHOD FOR PRODUCING BIS- (ENDO-Bicyclo [4.2.1] NONA-2,4-DIENOV) Download PDF

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RU2013149722A
RU2013149722A RU2013149722/04A RU2013149722A RU2013149722A RU 2013149722 A RU2013149722 A RU 2013149722A RU 2013149722/04 A RU2013149722/04 A RU 2013149722/04A RU 2013149722 A RU2013149722 A RU 2013149722A RU 2013149722 A RU2013149722 A RU 2013149722A
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nona
endo
bicyclo
dienov
producing bis
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RU2013149722/04A
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RU2556007C2 (en
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Усеин Меметович Джемилев
Владимир Анатольевич Дьяконов
Гульнара Назифовна Кадикова
Леонард Мухибович Халилов
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Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Способ получения бис-(эндо-бицикло[4.2.1]нона-2,4-диенов) общей формулы (1)характеризующийся тем, что α,ω-диаллены общей формулывзаимодействуют с 1,3,5-циклогептатриеном (ЦГТ) в присутствии каталитической системы TiCl-EtAlCl при соотношении α,ω-диаллен : ЦГТ : TiCl: EtAlCl = (9-11):20:(0.1-0.3):4, температуре 20-80°C, в бензоле, в течение 10-48 ч.A method for producing bis (endo-bicyclo [4.2.1] nona-2,4-dienes) of the general formula (1) characterized in that α, ω-diallenes of the general formula interact with 1,3,5-cycloheptatriene (CHT) in the presence of TiCl-EtAlCl catalyst system with the ratio α, ω-diallen: TSHT: TiCl: EtAlCl = (9-11): 20: (0.1-0.3): 4, temperature 20-80 ° C, in benzene, for 10-48 hours

Claims (1)

Способ получения бис-(эндо-бицикло[4.2.1]нона-2,4-диенов) общей формулы (1)The method of obtaining bis- (endobicyclo [4.2.1] nona-2,4-dienes) of the general formula (1)
Figure 00000001
Figure 00000001
 характеризующийся тем, что α,ω-диаллены общей формулы
Figure 00000002
characterized in that α, ω-diallenes of the general formula
Figure 00000002
 взаимодействуют с 1,3,5-циклогептатриеном (ЦГТ) в присутствии каталитической системы TiCl4-Et2AlCl при соотношении α,ω-диаллен : ЦГТ : TiCl4 : Et2AlCl = (9-11):20:(0.1-0.3):4, температуре 20-80°C, в бензоле, в течение 10-48 ч. interact with 1,3,5-cycloheptatriene (CGT) in the presence of the TiCl 4 -Et 2 AlCl catalyst system with the ratio α, ω-diallen: CGT: TiCl 4 : Et 2 AlCl = (9-11): 20: (0.1- 0.3): 4, at a temperature of 20-80 ° C, in benzene, for 10-48 hours.
RU2013149722/04A 2013-11-06 2013-11-06 Method of obtaining bis-(endo-bicyclo[4,2,1]none-2,4-dienes) RU2556007C2 (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1239298B (en) * 1966-03-14 1967-04-27 Shell Int Research Process for the preparation of dimers of bicyclo- [2, 2, 1] -heptadiene- (2, 5)
RU2402513C2 (en) * 2008-04-28 2010-10-27 Государственное образовательное учреждение высшего профессионального образования Иркутский государственный университет Tricyclo-[6;6;0;0]-hexadecadiene-6,10 synthesis method

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