RU2012129236A - METHOD AND DEVICE FOR PRODUCING HYDROCARBON FUEL AND COMPOSITIONS - Google Patents

METHOD AND DEVICE FOR PRODUCING HYDROCARBON FUEL AND COMPOSITIONS Download PDF

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RU2012129236A
RU2012129236A RU2012129236/04A RU2012129236A RU2012129236A RU 2012129236 A RU2012129236 A RU 2012129236A RU 2012129236/04 A RU2012129236/04 A RU 2012129236/04A RU 2012129236 A RU2012129236 A RU 2012129236A RU 2012129236 A RU2012129236 A RU 2012129236A
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stream
pitch
heavy
solvent
specified
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RU2012129236/04A
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Russian (ru)
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RU2517186C2 (en
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Джеймс Ф. МакГИ
Лоренц Дж. БАУЕР
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Юоп Ллк
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Priority claimed from US12/636,135 external-priority patent/US8193401B2/en
Priority claimed from US12/636,142 external-priority patent/US8133446B2/en
Priority claimed from US12/636,137 external-priority patent/US9074143B2/en
Application filed by Юоп Ллк filed Critical Юоп Ллк
Publication of RU2012129236A publication Critical patent/RU2012129236A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/003—Solvent de-asphalting
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/24—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions with moving solid particles
    • C10G47/26—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions with moving solid particles suspended in the oil, e.g. slurries
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G67/00—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only
    • C10G67/02—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only
    • C10G67/04—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only including solvent extraction as the refining step in the absence of hydrogen
    • C10G67/0454—Solvent desasphalting
    • C10G67/049—The hydrotreatment being a hydrocracking
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/04—Liquid carbonaceous fuels essentially based on blends of hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/205—Metal content
    • C10G2300/206—Asphaltenes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/301—Boiling range
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/44—Solvents

Abstract

1. Способ получения углеводородного топлива, который включает в себя:- суспензионный гидрокрекинг тяжелого сырья с получением продуктов суспензионного гидрокрекинга;- разделение указанных продуктов суспензионного гидрокрекинга с получением потока пека и потока тяжелого ВГО;- смешивание, по меньшей мере, части пекового потока с растворителем для того, чтобы растворить часть пека в растворителе; и- смешивание растворенной части пека, по меньшей мере, с частью потока тяжелого ВГО с образованием смешанного продукта.2. Способ по п.1, который дополнительно включает выделение растворенной части пека из растворителя до указанной стадии смешивания.3. Способ по п.1, в котором суспензионный гидрокрекинг указанного тяжелого сырья включает в себя превращение пека, по меньшей мере, на 85 масс.%.4. Способ по п.1, в котором указанный растворитель имеет плотность не больше, чем плотность гептана.5. Устройство для получения углеводородного топлива, которое включает:- реактор суспензионного гидрокрекинга для взаимодействия тяжелого сырья и водорода на катализаторе, чтобы получить продукты суспензионного гидрокрекинга;- сепаратор для выделения водорода из продуктов суспензионного гидрокрекинга, который соединен с указанным реактором суспензионного гидрокрекинга;- секцию 80 фракционирования, которая соединена с указанным реактором суспензионного гидрокрекинга, для фракционирования, по меньшей мере, части указанных продуктов суспензионного гидрокрекинга, причем указанная секция 80 фракционирования имеет боковой выпускной патрубок для выпускания потока тяжелого ВГО и нижний выпускной патрубок для выпускания потока пека;- коло1. A method for producing hydrocarbon fuel, which includes: - slurry hydrocracking of heavy feedstock to obtain slurry hydrocracking products; - separation of these slurry hydrocracking products to obtain a pitch stream and a heavy VGO stream; - mixing at least a part of the pitch stream with a solvent in order to dissolve part of the pitch in the solvent; and mixing the dissolved portion of the pitch with at least a portion of the heavy VGO stream to form a blended product. The method of claim 1, which further comprises separating the dissolved portion of the pitch from the solvent prior to said mixing step. The process of claim 1, wherein the slurry hydrocracking of said heavy feedstock comprises pitch conversion of at least 85% by weight. The method of claim 1, wherein said solvent has a density no greater than that of heptane. A device for producing hydrocarbon fuel, which includes: - a slurry hydrocracking reactor for reacting heavy feedstock and hydrogen on a catalyst to obtain slurry hydrocracking products; - a separator for separating hydrogen from slurry hydrocracking products, which is connected to said slurry hydrocracking reactor; - a fractionation section 80 which is connected to said slurry hydrocracking reactor for fractionating at least a portion of said slurry hydrocracking products, wherein said fractionation section 80 has a side outlet for venting a heavy VGO stream and a bottom outlet for venting a pitch stream;

Claims (10)

1. Способ получения углеводородного топлива, который включает в себя:1. A method of producing a hydrocarbon fuel, which includes: - суспензионный гидрокрекинг тяжелого сырья с получением продуктов суспензионного гидрокрекинга;- suspension hydrocracking of heavy raw materials to obtain products of suspension hydrocracking; - разделение указанных продуктов суспензионного гидрокрекинга с получением потока пека и потока тяжелого ВГО;- separation of these products of suspension hydrocracking to obtain a pitch stream and a stream of heavy VGO; - смешивание, по меньшей мере, части пекового потока с растворителем для того, чтобы растворить часть пека в растворителе; и- mixing at least a portion of the pitch stream with a solvent in order to dissolve a portion of the pitch in a solvent; and - смешивание растворенной части пека, по меньшей мере, с частью потока тяжелого ВГО с образованием смешанного продукта.- mixing the dissolved portion of the pitch with at least a portion of the heavy VGO stream to form a mixed product. 2. Способ по п.1, который дополнительно включает выделение растворенной части пека из растворителя до указанной стадии смешивания.2. The method according to claim 1, which further comprises isolating the dissolved portion of the pitch from the solvent prior to said mixing step. 3. Способ по п.1, в котором суспензионный гидрокрекинг указанного тяжелого сырья включает в себя превращение пека, по меньшей мере, на 85 масс.%.3. The method according to claim 1, wherein the suspension hydrocracking of said heavy feedstock comprises converting the pitch to at least 85% by weight. 4. Способ по п.1, в котором указанный растворитель имеет плотность не больше, чем плотность гептана.4. The method according to claim 1, wherein said solvent has a density no greater than that of heptane. 5. Устройство для получения углеводородного топлива, которое включает:5. A device for producing hydrocarbon fuel, which includes: - реактор суспензионного гидрокрекинга для взаимодействия тяжелого сырья и водорода на катализаторе, чтобы получить продукты суспензионного гидрокрекинга;- a suspension hydrocracking reactor for reacting heavy feedstocks and hydrogen on a catalyst to obtain suspension hydrocracking products; - сепаратор для выделения водорода из продуктов суспензионного гидрокрекинга, который соединен с указанным реактором суспензионного гидрокрекинга;- a separator for hydrogen evolution from suspension hydrocracking products, which is connected to the specified suspension hydrocracking reactor; - секцию 80 фракционирования, которая соединена с указанным реактором суспензионного гидрокрекинга, для фракционирования, по меньшей мере, части указанных продуктов суспензионного гидрокрекинга, причем указанная секция 80 фракционирования имеет боковой выпускной патрубок для выпускания потока тяжелого ВГО и нижний выпускной патрубок для выпускания потока пека;a fractionation section 80, which is connected to said slurry hydrocracking reactor, for fractionating at least a portion of said slurry hydrocracking products, said fractionation section 80 having a lateral outlet for discharging a heavy VGO stream and a lower outlet for discharging a pitch stream; - колонну деасфальтизации с растворителем, которая соединена с указанным потоком пека для получения деасфальтизированного потока из выпускного патрубка деасфальтизированной фракции; и- a deasphalting column with a solvent, which is connected to the specified pitch stream to obtain a deasphalted stream from the outlet pipe of the deasphalted fraction; and - емкость или трубопровод, который соединен с указанным боковым выпускным патрубком и указанным выпускным патрубком деасфальтизированной фракции для смешивания, по меньшей мере, части указанных потока тяжелого ВГО и потока деасфальтизированной фракции.- a tank or pipeline that is connected to the specified lateral outlet pipe and the specified outlet pipe of the deasphalted fraction for mixing at least part of the specified stream of heavy VGO and the stream of deasphalted fraction. 6. Углеводородная композиция, содержащая:6. Hydrocarbon composition containing: не менее чем 73 мас.% ароматических соединений;not less than 73 wt.% aromatic compounds; не больше, чем 5 мас.% фракции, нерастворимой в гептане; иnot more than 5 wt.% fraction insoluble in heptane; and не больше, чем 50 м.д. по массе ванадия;no more than 50 ppm by weight of vanadium; в которой, по меньшей мере, 80 об.% от указанной композиции выкипают при температуре выше 426°С (800°F).in which at least 80 vol.% of the specified composition is boiled off at a temperature above 426 ° C (800 ° F). 7. Углеводородная композиция по п.6, которая дополнительно содержит не больше, чем 5 мас.% фракции, нерастворимой в гексане.7. The hydrocarbon composition according to claim 6, which additionally contains not more than 5 wt.% Fractions insoluble in hexane. 8. Углеводород композиция по п.6, которая дополнительно содержит не больше, чем 5 мас.% фракции, нерастворимой в пентане.8. The hydrocarbon composition according to claim 6, which further comprises not more than 5 wt.% Of a fraction insoluble in pentane. 9. Углеводородная композиция по п.6, которая дополнительно содержит меньше, чем 10 м.д. по массе ванадия.9. The hydrocarbon composition according to claim 6, which further comprises less than 10 ppm. by weight of vanadium. 10. Углеводородная композиция по п.6, где, по меньшей мере, 90 об.% указанной композиции выкипает при температуре выше 426°С (800°F). 10. The hydrocarbon composition according to claim 6, where at least 90 vol.% Of the specified composition boils at a temperature above 426 ° C (800 ° F).
RU2012129236/04A 2009-12-11 2010-11-29 Procedure and device for production of hydrocarbon fuel and its composition RU2517186C2 (en)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US12/636,135 2009-12-11
US12/636,137 2009-12-11
US12/636,142 2009-12-11
US12/636,135 US8193401B2 (en) 2009-12-11 2009-12-11 Composition of hydrocarbon fuel
US12/636,142 US8133446B2 (en) 2009-12-11 2009-12-11 Apparatus for producing hydrocarbon fuel
US12/636,137 US9074143B2 (en) 2009-12-11 2009-12-11 Process for producing hydrocarbon fuel
PCT/US2010/058152 WO2011071705A2 (en) 2009-12-11 2010-11-29 Process and apparatus for producing hydrocarbon fuel and composition

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RU2012129236A true RU2012129236A (en) 2014-01-20
RU2517186C2 RU2517186C2 (en) 2014-05-27

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JP (2) JP2013513693A (en)
CN (2) CN102652169B (en)
BR (1) BR112012013470A2 (en)
CA (2) CA2862613C (en)
MX (1) MX2012003049A (en)
RU (1) RU2517186C2 (en)
SG (2) SG188922A1 (en)
WO (1) WO2011071705A2 (en)

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