RU2009112600A - Способ конверсии нитрата металла - Google Patents
Способ конверсии нитрата металла Download PDFInfo
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- RU2009112600A RU2009112600A RU2009112600/04A RU2009112600A RU2009112600A RU 2009112600 A RU2009112600 A RU 2009112600A RU 2009112600/04 A RU2009112600/04 A RU 2009112600/04A RU 2009112600 A RU2009112600 A RU 2009112600A RU 2009112600 A RU2009112600 A RU 2009112600A
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- Prior art keywords
- metal
- carrier
- oxide
- nitrate
- metal nitrate
- Prior art date
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- 238000000034 method Methods 0.000 title claims abstract 23
- 229910001960 metal nitrate Inorganic materials 0.000 title claims abstract 15
- 238000006243 chemical reaction Methods 0.000 title claims abstract 4
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims abstract 12
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract 12
- 150000004706 metal oxides Chemical class 0.000 claims abstract 12
- 239000007789 gas Substances 0.000 claims abstract 9
- 239000000203 mixture Substances 0.000 claims abstract 8
- 239000001272 nitrous oxide Substances 0.000 claims abstract 6
- 238000010438 heat treatment Methods 0.000 claims abstract 5
- 229910052751 metal Inorganic materials 0.000 claims abstract 5
- 239000002184 metal Substances 0.000 claims abstract 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims abstract 4
- 239000011261 inert gas Substances 0.000 claims abstract 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910002651 NO3 Inorganic materials 0.000 claims abstract 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims abstract 2
- 150000004645 aluminates Chemical class 0.000 claims abstract 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910000323 aluminium silicate Inorganic materials 0.000 claims abstract 2
- 229910052786 argon Inorganic materials 0.000 claims abstract 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910052799 carbon Inorganic materials 0.000 claims abstract 2
- 239000000969 carrier Substances 0.000 claims abstract 2
- 239000012876 carrier material Substances 0.000 claims abstract 2
- 229910017052 cobalt Inorganic materials 0.000 claims abstract 2
- 239000010941 cobalt Substances 0.000 claims abstract 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910052802 copper Inorganic materials 0.000 claims abstract 2
- 239000010949 copper Substances 0.000 claims abstract 2
- 239000001307 helium Substances 0.000 claims abstract 2
- 229910052734 helium Inorganic materials 0.000 claims abstract 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000005470 impregnation Methods 0.000 claims abstract 2
- 229910052742 iron Inorganic materials 0.000 claims abstract 2
- 229910003455 mixed metal oxide Inorganic materials 0.000 claims abstract 2
- 229910052759 nickel Inorganic materials 0.000 claims abstract 2
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract 2
- 239000001301 oxygen Substances 0.000 claims abstract 2
- 229910052760 oxygen Inorganic materials 0.000 claims abstract 2
- 229920000642 polymer Polymers 0.000 claims abstract 2
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract 2
- 239000000377 silicon dioxide Substances 0.000 claims abstract 2
- 239000007787 solid Substances 0.000 claims abstract 2
- 239000002904 solvent Substances 0.000 claims abstract 2
- 239000004408 titanium dioxide Substances 0.000 claims abstract 2
- 229910002001 transition metal nitrate Inorganic materials 0.000 claims abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 1
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 claims 1
- 239000005751 Copper oxide Substances 0.000 claims 1
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 1
- 229910000428 cobalt oxide Inorganic materials 0.000 claims 1
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims 1
- 229910000431 copper oxide Inorganic materials 0.000 claims 1
- 229910000480 nickel oxide Inorganic materials 0.000 claims 1
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical group [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims 1
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- B01J29/00—Catalysts comprising molecular sieves
- B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
- B01J29/0308—Mesoporous materials not having base exchange properties, e.g. Si-MCM-41
- B01J29/0316—Mesoporous materials not having base exchange properties, e.g. Si-MCM-41 containing iron group metals, noble metals or copper
- B01J29/0333—Iron group metals or copper
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- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
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- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/08—Heat treatment
- B01J37/082—Decomposition and pyrolysis
- B01J37/088—Decomposition of a metal salt
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- B01J37/16—Reducing
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- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
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- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
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- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
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- C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
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- C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
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- C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
- C10G45/06—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof
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Abstract
1. Способ конверсии нитрата металла, нанесенного на носитель, в соответствующий оксид металла, нанесенный на носитель, включающий нагрев нитрата металла для осуществления его разложения в атмосфере смеси газов, содержащей закись азота, содержание кислорода в которой составляет менее 5 об.%, причем концентрация закиси азота в смеси газов лежит в интервале от 0,001 до 15 об.%. ! 2. Способ по п.1, отличающийся тем, что нитрат металла наносят на материал-носитель путем пропитки из раствора и сушат для удаления растворителя перед стадией нагрева нитрата металла для его конверсии в соответствующий оксид металла. ! 3. Способ по п.1, отличающийся тем, что смесь газов состоит из одного или нескольких инертных газов и закиси азота. ! 4. Способ по п.3, отличающийся тем, что инертный газ выбран из азота, гелия или аргона. ! 5. Способ по п.1, отличающийся тем, что нитрат металла, нанесенный на носитель, нагревают до температуры 100-1200°С. ! 6. Способ по п.1, отличающийся тем, что нитрат металла представляет собой нитрат переходного металла. ! 7. Способ по п.1, отличающийся тем, что нитрат металла представляет собой нитрат никеля, кобальта, меди или железа. ! 8. Способ по п.1, отличающийся тем, что носитель выбирают из носителей из металла, углерода, оксида металла, смешанного оксида металла или твердого полимера. ! 9. Способ по п.1, отличающийся тем, что носитель выбирают из оксида алюминия, алюминатов металлов, диоксида кремния, алюмосиликатов, диоксида титана, диоксида циркония или их смесей. ! 10. Способ по п.1, отличающийся тем, что оксид металла, нанесенный на носитель, представляет собой способный к восстановлению оксид металла, и дополнительно включает �
Claims (12)
1. Способ конверсии нитрата металла, нанесенного на носитель, в соответствующий оксид металла, нанесенный на носитель, включающий нагрев нитрата металла для осуществления его разложения в атмосфере смеси газов, содержащей закись азота, содержание кислорода в которой составляет менее 5 об.%, причем концентрация закиси азота в смеси газов лежит в интервале от 0,001 до 15 об.%.
2. Способ по п.1, отличающийся тем, что нитрат металла наносят на материал-носитель путем пропитки из раствора и сушат для удаления растворителя перед стадией нагрева нитрата металла для его конверсии в соответствующий оксид металла.
3. Способ по п.1, отличающийся тем, что смесь газов состоит из одного или нескольких инертных газов и закиси азота.
4. Способ по п.3, отличающийся тем, что инертный газ выбран из азота, гелия или аргона.
5. Способ по п.1, отличающийся тем, что нитрат металла, нанесенный на носитель, нагревают до температуры 100-1200°С.
6. Способ по п.1, отличающийся тем, что нитрат металла представляет собой нитрат переходного металла.
7. Способ по п.1, отличающийся тем, что нитрат металла представляет собой нитрат никеля, кобальта, меди или железа.
8. Способ по п.1, отличающийся тем, что носитель выбирают из носителей из металла, углерода, оксида металла, смешанного оксида металла или твердого полимера.
9. Способ по п.1, отличающийся тем, что носитель выбирают из оксида алюминия, алюминатов металлов, диоксида кремния, алюмосиликатов, диоксида титана, диоксида циркония или их смесей.
10. Способ по п.1, отличающийся тем, что оксид металла, нанесенный на носитель, представляет собой способный к восстановлению оксид металла, и дополнительно включает нагрев оксида металла, нанесенного на носитель, в потоке газа-восстановителя для восстановления по меньшей мере части оксида металла.
11. Способ по п.10, отличающийся тем, что поток газа-восстановителя содержит моноксид углерода и/или водород.
12. Способ по п.10, отличающийся тем, что оксид металла, нанесенный на носитель, представляет собой оксид никеля, оксид кобальта, оксид меди или оксид железа, и восстановление проводят с использованием водородсодержащего газа.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB0617529.3 | 2006-09-07 | ||
| GBGB0617529.3A GB0617529D0 (en) | 2006-09-07 | 2006-09-07 | Metal nitrate conversion method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2009112600A true RU2009112600A (ru) | 2010-10-20 |
| RU2437717C2 RU2437717C2 (ru) | 2011-12-27 |
Family
ID=37232447
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2009112600/04A RU2437717C2 (ru) | 2006-09-07 | 2007-08-14 | Способ конверсии нитрата металла |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8263522B2 (ru) |
| EP (1) | EP2061595B1 (ru) |
| JP (1) | JP5284963B2 (ru) |
| CN (1) | CN101511475B (ru) |
| AT (1) | ATE473049T1 (ru) |
| DE (1) | DE602007007631D1 (ru) |
| DK (1) | DK2061595T3 (ru) |
| GB (1) | GB0617529D0 (ru) |
| PL (1) | PL2061595T3 (ru) |
| RU (1) | RU2437717C2 (ru) |
| WO (1) | WO2008029177A1 (ru) |
| ZA (1) | ZA200901370B (ru) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8148292B2 (en) * | 2008-07-25 | 2012-04-03 | Exxonmobil Research And Engineering Company | Preparation of high activity cobalt catalysts, the catalysts and their use |
| DE102009006404B3 (de) * | 2009-01-28 | 2010-08-26 | Süd-Chemie AG | Diesel-Oxidationskatalysator mit guter Tieftemperaturaktivität |
| JP5067700B2 (ja) * | 2009-02-23 | 2012-11-07 | 独立行政法人日本原子力研究開発機構 | 金属酸化物粒子の製造方法 |
| GB0905222D0 (en) | 2009-03-26 | 2009-05-13 | Johnson Matthey Plc | Method for producing a supported metal nitrate |
| MX352582B (es) * | 2012-11-06 | 2017-11-07 | Mexicano Inst Petrol | Composito mesoporoso de mallas moleculares para la hidrodesintegracion de crudos pesados y residuos. |
| TWI642481B (zh) * | 2013-07-17 | 2018-12-01 | 東楚股份有限公司 | Catalyst system for the production of heterogeneous catalysts and 1,2-dichloroethane |
| KR101629804B1 (ko) * | 2014-06-19 | 2016-06-14 | (주)써스텍 | 수소 제거용 촉매 제조 방법 |
| CN110492112A (zh) * | 2019-07-11 | 2019-11-22 | 江苏师范大学 | 一种氧还原复合催化剂及其制备方法 |
| CN111847405A (zh) * | 2020-08-17 | 2020-10-30 | 眉山顺应动力电池材料有限公司 | 一种硝酸盐热分解回收硝酸的装置系统及其使用方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3909455A (en) * | 1973-05-01 | 1975-09-30 | Philip Morris Inc | Catalyst and process for making same |
| GB8918845D0 (en) * | 1989-08-18 | 1989-09-27 | Shell Int Research | Process for the preparation of a catalyst suitable for the preparation of hydrocarbons from carbon monoxide and hydrogen,and said catalyst |
| FR2780313B1 (fr) | 1998-06-25 | 2000-08-11 | Inst Francais Du Petrole | Procede de sulfuration de catalyseurs par reduction suivie d'une sulfuration |
| US6706661B1 (en) * | 2000-09-01 | 2004-03-16 | Exxonmobil Research And Engineering Company | Fischer-Tropsch catalyst enhancement |
| CN1184005C (zh) * | 2002-08-23 | 2005-01-12 | 中国科学院兰州化学物理研究所 | 镍基催化剂的制备方法 |
| RU2429073C2 (ru) | 2005-12-21 | 2011-09-20 | Джонсон Мэтти Плс | Способ конверсии нитратов металлов |
-
2006
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- 2007-08-14 WO PCT/GB2007/050492 patent/WO2008029177A1/en active Application Filing
- 2007-08-14 PL PL07789378T patent/PL2061595T3/pl unknown
- 2007-08-14 AT AT07789378T patent/ATE473049T1/de not_active IP Right Cessation
- 2007-08-14 DK DK07789378.2T patent/DK2061595T3/da active
- 2007-08-14 JP JP2009527210A patent/JP5284963B2/ja not_active Expired - Fee Related
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- 2007-08-14 DE DE602007007631T patent/DE602007007631D1/de active Active
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Also Published As
| Publication number | Publication date |
|---|---|
| EP2061595B1 (en) | 2010-07-07 |
| ZA200901370B (en) | 2010-03-31 |
| US8263522B2 (en) | 2012-09-11 |
| GB0617529D0 (en) | 2006-10-18 |
| DK2061595T3 (da) | 2010-10-25 |
| WO2008029177A1 (en) | 2008-03-13 |
| PL2061595T3 (pl) | 2010-12-31 |
| CN101511475A (zh) | 2009-08-19 |
| RU2437717C2 (ru) | 2011-12-27 |
| EP2061595A1 (en) | 2009-05-27 |
| CN101511475B (zh) | 2012-08-01 |
| JP5284963B2 (ja) | 2013-09-11 |
| ATE473049T1 (de) | 2010-07-15 |
| DE602007007631D1 (de) | 2010-08-19 |
| JP2010502556A (ja) | 2010-01-28 |
| US20100099553A1 (en) | 2010-04-22 |
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