RO71605B - Process for preparing some s-triazines with herbicide action - Google Patents
Process for preparing some s-triazines with herbicide actionInfo
- Publication number
- RO71605B RO71605B RO74881A RO7488173A RO71605B RO 71605 B RO71605 B RO 71605B RO 74881 A RO74881 A RO 74881A RO 7488173 A RO7488173 A RO 7488173A RO 71605 B RO71605 B RO 71605B
- Authority
- RO
- Romania
- Prior art keywords
- general formula
- methyl
- triazines
- preparing
- sulfate
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/30—Only oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C335/00—Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C335/30—Isothioureas
- C07C335/38—Isothioureas containing any of the groups, X being a hetero atom, Y being any atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Plural Heterocyclic Compounds (AREA)
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Abstract
Procedeu de preparare a unor s-triazine cu actiune erbicida cu formula generala I: (vezi form. in desc.) în care R1 reprezinta alchil C2-C8, cicloalchil C5-C8 norbonil, metilcicloahexil, fenil sau clor-fenil, R3 reprezinta hidrogen sau metil, R4 reprezinta alchil C1-C4 si X reprezinta oxigen sau sulf, cu conditia ca, atunci cînd X reprezinta sulf, R3 reprezinta metil, caracterizat prin aceea ca se trateaza metoxicarbonilcianamida cu un agent de metilare cu formula generala II:(vezi form. in desc.)în care Z reprezinta iod sau o grupa -O-SO2-OCH3, pentru a obtine N-metoxicarbonil-N-metil-cianamida, care se grateaza cu o amina cu formula generala III: (vezi form. in desc.) sub forma de sulfat sau clorhidrat în care R3 si R4 au semnificatiile de mai sus, pentru a obtine o guanidina cu formula generala IV:(vezi form. in desc.) sub forma de sulfat sau clorhidrat, în care R1, R3, R4 si X au semnificatiile de mai sus, reactia avînd loc în solutie apoasa.....Process for the preparation of herbicidal s-triazine derivatives of the general formula I: (wherein R 1 represents C 2 -C 8 alkyl, C 5 -C 8 cycloalkyl, methylcyclohexyl, phenyl or chlorophenyl, R 3 represents hydrogen or methyl, R 4 represents C 1 -C 4 alkyl and X represents oxygen or sulfur, with the proviso that when X represents sulfur, R 3 represents methyl, characterized in that the methoxycarbonylcyanamide is treated with a methylation agent of the general formula II: in which Z represents iodine or a group -O-SO2-OCH3, to obtain N-methoxycarbonyl-N-methyl-cyanamide, which is cleaved with an amine of general formula III: ) in the form of a sulfate or a hydrochloride in which R3 and R4 are as defined above to obtain a guanidine of general formula IV: (in the form as shown) as the sulfate or hydrochloride salt, wherein R1, R3, R4 and X are as defined above, the reaction being carried out in aqueous solution .....
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US25624972A | 1972-05-24 | 1972-05-24 | |
| US34832173A | 1973-04-05 | 1973-04-05 | |
| US00348324A US3850924A (en) | 1973-04-05 | 1973-04-05 | Process for preparing herbicidal triazines |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RO71605A RO71605A (en) | 1983-04-29 |
| RO71605B true RO71605B (en) | 1983-04-30 |
Family
ID=27400932
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO7383863A RO68557A (en) | 1972-05-24 | 1973-05-23 | PROCESS FOR THE PREPARATION OF HERBICIDE-ACID TRIAZINES |
| RO74881A RO71605B (en) | 1972-05-24 | 1973-05-23 | Process for preparing some s-triazines with herbicide action |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO7383863A RO68557A (en) | 1972-05-24 | 1973-05-23 | PROCESS FOR THE PREPARATION OF HERBICIDE-ACID TRIAZINES |
Country Status (30)
| Country | Link |
|---|---|
| JP (2) | JPS5418339B2 (en) |
| AR (1) | AR213607A1 (en) |
| BG (1) | BG22363A3 (en) |
| CH (1) | CH583506A5 (en) |
| CY (1) | CY972A (en) |
| DD (2) | DD112651A5 (en) |
| DE (1) | DE2326358C3 (en) |
| DK (1) | DK139911B (en) |
| EG (1) | EG10976A (en) |
| ES (1) | ES441014A1 (en) |
| FI (1) | FI57940C (en) |
| FR (1) | FR2185625B1 (en) |
| GB (1) | GB1435585A (en) |
| HK (1) | HK31378A (en) |
| HU (1) | HU167436B (en) |
| IE (1) | IE37629B1 (en) |
| IL (1) | IL42103A (en) |
| IN (1) | IN139019B (en) |
| IT (1) | IT987878B (en) |
| KE (1) | KE2845A (en) |
| LU (1) | LU67653A1 (en) |
| MX (1) | MX147114A (en) |
| MY (1) | MY7800316A (en) |
| NL (1) | NL160259C (en) |
| NO (2) | NO140268C (en) |
| OA (1) | OA04410A (en) |
| RO (2) | RO68557A (en) |
| SU (1) | SU616994A3 (en) |
| YU (6) | YU137073A (en) |
| ZM (1) | ZM8373A1 (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS602306B2 (en) * | 1972-11-06 | 1985-01-21 | バイエル アクチエンゲゼルシヤフト | Method for producing tetrahydro-1,3,5-triazine-2,6-diones |
| DE2254200C2 (en) * | 1972-11-06 | 1982-04-22 | Bayer Ag, 5090 Leverkusen | Tetrahydro-1,3,5-triazine-2,6-diones, process for their preparation and their use as herbicides |
| GB1543037A (en) * | 1975-02-05 | 1979-03-28 | Ici Ltd | Selective herbicidal triazine-diones |
| US4226990A (en) * | 1973-11-01 | 1980-10-07 | Imperial Chemical Industries Limited | Triazine-diones |
| BR7602779A (en) * | 1975-05-05 | 1976-11-09 | Du Pont | PROCESS FOR THE PREPARATION OF HERBICIDE TRIAZINS |
| US4197112A (en) * | 1977-10-12 | 1980-04-08 | E. I. Du Pont De Nemours And Company | Water-dispersible herbicide compositions |
| US4246409A (en) * | 1978-11-13 | 1981-01-20 | William H. Rorer, Inc. | Triazinones |
| MX2023010673A (en) * | 2021-03-17 | 2023-09-22 | Hansoh Bio Llc | Nitrogen-containing heterocyclic ketones, preparation methods and medicinal uses thereof. |
| WO2023222103A1 (en) * | 2022-05-20 | 2023-11-23 | 江苏恒瑞医药股份有限公司 | Crystal forms of triazine dione derivative and preparation method therefor |
-
1973
- 1973-04-25 IL IL42103A patent/IL42103A/en unknown
- 1973-04-26 IN IN980/CAL/73A patent/IN139019B/en unknown
- 1973-05-14 ZM ZM83/73A patent/ZM8373A1/en unknown
- 1973-05-15 IE IE762/73A patent/IE37629B1/en unknown
- 1973-05-16 AR AR248054A patent/AR213607A1/en active
- 1973-05-17 OA OA54914A patent/OA04410A/en unknown
- 1973-05-22 JP JP5642873A patent/JPS5418339B2/ja not_active Expired
- 1973-05-22 EG EG189/73A patent/EG10976A/en active
- 1973-05-22 BG BG23690A patent/BG22363A3/xx unknown
- 1973-05-22 DD DD179515*A patent/DD112651A5/xx unknown
- 1973-05-22 DD DD170989A patent/DD106938A5/xx unknown
- 1973-05-23 LU LU67653A patent/LU67653A1/xx unknown
- 1973-05-23 HU HUDU203A patent/HU167436B/hu unknown
- 1973-05-23 RO RO7383863A patent/RO68557A/en unknown
- 1973-05-23 NL NL7307218.A patent/NL160259C/en not_active IP Right Cessation
- 1973-05-23 RO RO74881A patent/RO71605B/en unknown
- 1973-05-23 DK DK283473AA patent/DK139911B/en not_active IP Right Cessation
- 1973-05-23 FR FR7318733A patent/FR2185625B1/fr not_active Expired
- 1973-05-23 GB GB2467773A patent/GB1435585A/en not_active Expired
- 1973-05-23 FI FI1667/73A patent/FI57940C/en active
- 1973-05-23 SU SU731923101A patent/SU616994A3/en active
- 1973-05-23 CY CY972A patent/CY972A/en unknown
- 1973-05-23 NO NO2120/73A patent/NO140268C/en unknown
- 1973-05-23 DE DE2326358A patent/DE2326358C3/en not_active Expired
- 1973-05-24 YU YU01370/73A patent/YU137073A/en unknown
- 1973-05-24 CH CH747673A patent/CH583506A5/xx not_active IP Right Cessation
- 1973-05-24 IT IT24541/73A patent/IT987878B/en active
- 1973-06-04 MX MX143886A patent/MX147114A/en unknown
- 1973-12-07 NO NO4674/73A patent/NO141300C/en unknown
-
1975
- 1975-09-16 ES ES441014A patent/ES441014A1/en not_active Expired
-
1976
- 1976-06-24 JP JP51073894A patent/JPS527980A/en active Pending
-
1978
- 1978-06-13 KE KE2845A patent/KE2845A/en unknown
- 1978-06-22 HK HK313/78A patent/HK31378A/en unknown
- 1978-12-31 MY MY1978316A patent/MY7800316A/en unknown
-
1979
- 1979-06-29 YU YU01562/79A patent/YU156279A/en unknown
- 1979-06-29 YU YU01566/79A patent/YU156679A/en unknown
- 1979-06-29 YU YU01563/79A patent/YU156379A/en unknown
- 1979-06-29 YU YU01564/79A patent/YU156479A/en unknown
- 1979-06-29 YU YU01561/79A patent/YU156179A/en unknown
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