RO128793A0 - Fortifying whey-based beverage and process for preparing the same - Google Patents
Fortifying whey-based beverage and process for preparing the same Download PDFInfo
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BĂUTURĂ FORTIFIANTA PE BAZA DE ZER SI PROCEDEU DE OBȚINERESTRENGTHENING DRINK BASED ON ZERO AND PROCESS FOR OBTAINING
Invenția se refera la obținerea unui produs de nisa, o băutură “ready to drink” cu ingrediente naturale, pe baza de zer si la un procedeu de realizare a acesteia. Produsele de nisa se adreseaza unui segment mic, dar clar definit din populație, in acest caz sportivilor, pentru o nutriție si hidratare moderna care sa susțină efortul fizic prelungit.The invention relates to obtaining a niche product, a drink "ready to drink" with natural ingredients, based on whey and a process for making it. Niche products address a small, but clearly defined segment of the population, in this case athletes, for a modern nutrition and hydration that supports prolonged physical exertion.
Zerul este fracțiunea lichida care se separa la fabricarea branzeturilor, in urma precipitării si înlăturării cazeinei, si reprezintă 85-90% din volumul laptelui prelucrat. Se apreciaza ca la o producție mondiala de peste 10 milioane tone brânzeturi, rezulta cea. 85-90 milioane tone zer, fiecare kg de branza generând 8-12 kg de zer. In zer ramane intre 46-52% din substanța uscata a laptelui, in care componentele nutritive (lactoza, proteine serice, săruri minerale, enzime, hormoni, factori de creștere) sunt prezente in cantitati mari (Stroia C, Tarala R, 2008, Valorificarea pe cale biotehnologica a zerului, Sesiunea Cercurilor Științifice Studențești, Universitatea Dunarea de Jos, Galați).Whey is the liquid fraction that separates in the manufacture of cheese, after precipitation and removal of casein, and represents 85-90% of the volume of processed milk. It is estimated that at a world production of over 10 million tons of cheese, the result is. 85-90 million tons of whey, each kg of cheese generating 8-12 kg of whey. Whey remains between 46-52% of the dry matter of milk, in which the nutrient components (lactose, serum proteins, mineral salts, enzymes, hormones, growth factors) are present in large quantities (Stroia C, Tarala R, 2008, Recovery biotechnology of whey, Student Scientific Circles Session, Lower Danube University, Galați).
Proteinele din zer au o valoare biologica superioara proteinelor din ou, soia si cazeinei din lapte, conținând aminoacizi esențiali ramificați (leucina, izoleucina, valina), foarte importanți pentru atleti. Spre deosebire de alti aminoacizi esențiali, cei ramificați sunt metabolizati direct in tesutul muscular si sunt primii aminoacizi folosiți in timpul perioadei de antrenament si anduranta. Leucina joaca un rol important in sinteza proteinelor țesutului muscular contribuind la reconstrucția si dezvoltarea țesutului muscular. De asemenea, proteinele din zer sunt bogate in aminoacizi conținând sulf (cisteina, metionina) care participa la biosinteza glutationului, un antioxidant, stimulator al sistemului imunitar.Whey proteins have a higher biological value than egg proteins, soy and milk casein, containing branched essential amino acids (leucine, isoleucine, valine), very important for athletes. Unlike other essential amino acids, branched ones are metabolized directly into muscle tissue and are the first amino acids used during training and endurance. Leucine plays an important role in the synthesis of muscle tissue proteins contributing to the reconstruction and development of muscle tissue. Also, whey proteins are rich in amino acids containing sulfur (cysteine, methionine) that participates in the biosynthesis of glutathione, an antioxidant, stimulator of the immune system.
Sărurile minerale (magneziu, zinc, fier, mangan, sodiu, calciu, fosfor, potasiu) contribuie la menținerea concentrațiilor de electroliti din fluidele corpului, înlocuind electrolitii care se pierd prin transpirație in urma exercitiilor fizice, si al căror rol este esențial in transmiterea impulsurilor electrice de la o celula la alta. înlocuirea electrolitilor eliminați prin transpirație determina rehidratarea, care este foarte importanta in întârzierea instalării oboselii după exercițiile fizice.Mineral salts (magnesium, zinc, iron, manganese, sodium, calcium, phosphorus, potassium) help maintain electrolyte concentrations in body fluids, replacing electrolytes that are lost through perspiration after exercise, and whose role is essential in transmitting impulses. electrical from one cell to another. Replacement of electrolytes removed by perspiration causes rehydration, which is very important in delaying the onset of fatigue after exercise.
Conținutul mineral si proteic al zerului permite orientarea valorificării eficiente a acestuia. Acest subprodus poate fi utilizat in proporție de 100%, prin recuperarea tuturor substanțelor utile din compoziția sa.The mineral and protein content of whey allows the orientation of its efficient recovery. This by-product can be used 100%, by recovering all the useful substances in its composition.
Producția de băuturi pe baza de zer a început in anii 1970 si pana in prezent au fost dezvoltate numeroase variante, ca o noua generație a produselor lactate. Băuturile pot fi produse ^- 2 0 1 2 - 0 0^44-2 0 -11- 2012 din zer dulce sau zer acid, zer deproteinizat, din zer diluat cu apa, zer pudra, zer fermentat, concentrat proteic din zer, izolat proteic din zer. Băuturile nealcoolice pe baza de zer includ o gama larga de produse obținute prin amestecarea zerului dulce diluat sau acid cu diferiți aditivi ca de exemplu: fructe, cereale, izolate de proteine vegetale, CO2, ciocolata, cacao, extract de vanilie si alti agenti de aromatizare. O atentie speciala se acorda producerii de băuturi ferementate din zer cu bacterii probiotice unde cel mai important aspect este alegerea culturii potrivite de bacterii in scopul producerii de băuturi funcționale cu valoare nutritiva ridicata si caracteristici senzoriale acceptabile. Băuturile pe baza de zer se adreseaza unei game largi de consumatori de la copii pana la persoane in varsta. Ele au valoare nutritiva ridicata si caracteristici terapeutice bune.The production of whey drinks began in the 1970s and until now many variants have been developed, such as a new generation of dairy products. Beverages can be produced ^ - 2 0 1 2 - 0 0 ^ 44-2 0 -11- 2012 from sweet whey or acid whey, deproteinized whey, water diluted whey, whey powder, fermented whey, whey protein concentrate, isolated whey protein. Whey-based soft drinks include a wide range of products obtained by mixing diluted or acidic sweet whey with various additives such as: fruits, cereals, vegetable protein isolates, CO 2 , chocolate, cocoa, vanilla extract and other agents. flavoring. Special attention is paid to the production of fermented whey beverages with probiotic bacteria where the most important aspect is choosing the right culture of bacteria in order to produce functional drinks with high nutritional value and acceptable sensory characteristics. Whey-based drinks cater to a wide range of consumers from children to the elderly. They have high nutritional value and good therapeutic characteristics.
Cercetătorii de la Universitatea Novi Sad au investigat băuturile pe baza de zer obținute cu ajutorul culturilor de Kombucha (Rodomir VM, 2009, Whey utilization, Journal of Food Chemistry, 57-58 ). In Brazilia s-au obtinut băuturi pe baza de zer neprocesat/deproteinizat, fermentat folosind ca si cultura starter kefirul (Magalhaes KT, 2010, Evaluation of morphological and microbial variations, Journal of Bioresource Technology, Biology Department, Federal University of Lavras).Researchers at Novi Sad University investigated whey-based beverages obtained using Kombucha cultures (Rodomir VM, 2009, Whey utilization, Journal of Food Chemistry, 57-58). In Brazil, beverages based on unprocessed / deproteinized whey were obtained, fermented using kefir as a starter culture (Magalhaes KT, 2010, Evaluation of morphological and microbial variations, Journal of Bioresource Technology, Biology Department, Federal University of Lavras).
In scopul preparării unei băuturi pe baza de zer, brevetul RU2422028/2011 (Varivoda Al Bina Alekseevna , Method for preparation of drink based on dairy whey) prezintă o metoda de preparare conform careia in zerul încălzit se introduce o polizaharida de origine vegetala (gel de aloe vera) cu adaos de fructoza, acid citric si aroma naturala de struguri. Pentru extinderea gamei de produse pe baza de lapte, brevetul RU2421007/2011 (Kim Igor' Nikolaevich, ; Shtanko Tatjana Ivanovna, Dairy whey drink preparation method) prezintă o băutură cu proprietăți organoleptice imbunatatite obtinuta prin adugarea, in zerul pasteurizat, a unui agent de ingrosare reprezentat printr-o pasta de somon sarat in cantitate de 20-50% din greutatea zerului. Brevetul RU2403795/2010 (Shchepochkina Julija Alekseevna, Dairy whey drink preparation method) propune aromatizarea cu sirop de zahar si piure de pepene, sau suc de pepene, cu amestecare ulterioara. Băutură conform brevetului EP1829457/2007 (Sauer Wemer, Beverage containing whey) conține zer, concentrat multi-fruct, CO2 dizolvat, apa si are acțiune imunostimulanta. Brevetul CAI 103513/1981 (Scibelli Gabriele,Whey protein softdrink fortifier) prezintă o băutură acida cu aroma de citrice pe baza de concentrat proteic din zer, sau o combinație de 50-95% concentrat proteic de zer si corespunzător 50-5% lapte praf degresat.For the purpose of preparing a whey-based beverage, patent RU2422028 / 2011 (Varivoda Al Bina Alekseevna, Method for preparation of drink based on dairy whey) discloses a method of preparation according to which a polysaccharide of vegetable origin (gel of aloe vera) with the addition of fructose, citric acid and natural grape flavor. For the extension of the range of milk-based products, patent RU2421007 / 2011 (Kim Igor 'Nikolaevich; Shtanko Tatjana Ivanovna, Dairy whey drink preparation method) presents a beverage with improved organoleptic properties obtained by adding, in pasteurized whey, an agent of thickening represented by a salted salmon paste in the amount of 20-50% of the weight of the whey. Patent RU2403795 / 2010 (Shchepochkina Julija Alekseevna, Dairy whey drink preparation method) proposes flavoring with sugar syrup and melon puree, or melon juice, with subsequent mixing. Beverage according to patent EP1829457 / 2007 (Sauer Wemer, Beverage containing whey) contains whey, multi-fruit concentrate, dissolved CO 2 , water and has immunostimulatory action. CAI patent 103513/1981 (Scibelli Gabriele, Whey protein softdrink fortifier) presents an acidic drink with citrus flavor based on whey protein concentrate, or a combination of 50-95% whey protein concentrate and corresponding 50-5% milk powder skimmed.
Problema tehnica pe care o rezolva aceasta invenție consta in obținerea unei băuturi fortifiante „ready to drink” pe baza de zer integral, fara adaos de apa, cu un raport echilibrat intre electroliti si aminoacizi esențiali ramificați si care sa posede caracteristici senzoriale acceptabile,The technical problem solved by this invention is to obtain a fortifying drink "ready to drink" based on whole whey, without added water, with a balanced ratio between electrolytes and branched essential amino acids and having acceptable sensory characteristics,
Ar 2 Ο 1 2 - Ο Ο 8 4 4 - 2 Ο -11- 2012 gustul si mirosul de zer nefiind sesizabile, cu valoare biologica ridicata, care sa ofere aroma, funcționalitate si nutriție, in scopul hidratării si combaterii oboselii si hipoxiei in urma efortului sportiv. Compoziția chimica a zerului, bogata in electroliti, nu a necesitat suplimentarea acestora, asigurând cantitatea optima de săruri de Na, K, Ca, Mg eliminate prin transpirație.Ar 2 Ο 1 2 - Ο Ο 8 4 4 - 2 Ο -11- 2012 the taste and smell of whey are not noticeable, with high biological value, which provides aroma, functionality and nutrition, in order to hydrate and combat fatigue and hypoxia after sports effort. The chemical composition of the whey, rich in electrolytes, did not require their supplementation, ensuring the optimal amount of Na, K, Ca, Mg salts eliminated by perspiration.
Băutură „ready to drink” pe baza de zer integral, fara adaos de apa, conform invenției, este formata din 79...92% zer filtrat, clarificat si sterilizat prin pasteurizare, 3...10% fructoza, 0,05...0,15% stabilizator xantan sau 0,08...0,35% pectina, 5...10% concentrat de fructe, 0,04%....0,12% arome naturale de fructe, 0,03....0,8% coloranti naturali si acidifiant pentru pH = 3,4-3,8 la variantele pe baza de fructe.Beverage "ready to drink" based on whole whey, without added water, according to the invention, consists of 79 ... 92% filtered whey, clarified and sterilized by pasteurization, 3 ... 10% fructose, 0.05. ..0.15% xanthan stabilizer or 0.08 ... 0.35% pectin, 5 ... 10% fruit concentrate, 0.04% .... 0.12% natural fruit flavors, 0, 03 .... 0.8% natural dyes and acidifier for pH = 3.4-3.8 for fruit-based variants.
Procedeul de obținere a băuturii pe baza de zer integral, conform invenției, consta in dizolvarea/hidratarea amestecului de fructoza si stabilizator in zer filtrat, clarificat si pasteurizat, rece sau încălzit la 50 °C in funcție de stabilizatorul folosit, sub agitare ușoara pentru reducerea/prevenirea incorporării de aer timp de 20...30 minute pentru reducerea turbiditatii, amestecarea concentratelor de fructe, a aromelor naturale de fructe si a colorantului natural corespunzător, adaugarea zerului cu stabilizator, ajustarea pH-ului la 3,8 cu soluție 50% acid citric sau soluție 80% acid lactic, omogenizare la 60 °C/50...200 bari pentru dispersia completa a stabilizatorului înainte de tratamentul termic, pasteurizare la 80 °C, 10 minute. Procedeul este redat schematic in figura 1.The process for obtaining the drink based on whole whey, according to the invention, consists in dissolving / hydrating the mixture of fructose and stabilizer in filtered whey, clarified and pasteurized, cold or heated to 50 ° C depending on the stabilizer used, with gentle stirring to reduce / prevention of air incorporation for 20 ... 30 minutes to reduce turbidity, mixing fruit concentrates, natural fruit flavors and the corresponding natural dye, adding whey with stabilizer, adjusting the pH to 3.8 with 50% solution citric acid or 80% lactic acid solution, homogenization at 60 ° C / 50 ... 200 bar for complete dispersion of the stabilizer before heat treatment, pasteurization at 80 ° C, 10 minutes. The procedure is shown schematically in figure 1.
Băutură fortifianta ’ready to drink’ pe baza de zer integral, conform invenției, conferă comoditate si portabilitate consumatorilor, inlaturand dezavantajele pulberilor proteice (concentrat proteic de zer, izolat proteic de zer), preferate pentru acest tip de băuturi, care trebuie reconstituite sub forma de shake, si care nu furnizează electroliti si vitamine, a căror pierdere in urma efortului sportiv susținut trebuie compensata.The fortified drink 'ready to drink' based on whole whey, according to the invention, provides convenience and portability to consumers, eliminating the disadvantages of protein powders (whey protein concentrate, whey protein isolate), preferred for this type of beverage, which must be reconstituted as of shake, and which does not provide electrolytes and vitamins, the loss of which as a result of sustained sports effort must be compensated.
Compoziția si procedeul, conform invenției, prezintă următoarele avantaje:The composition and process according to the invention have the following advantages:
folosirea zerului integral, fara adaos de apa, asigura rehidratarea, furnizează aminoacizi esențiali ramificați si vitamine si aduce un aport de electroliti (in special calciu si magneziu), care compensează pierderile, prin transpirație, in urma efortului fizic folosirea zerului integral pentru minimalizarea costurilor de producție adaugarea hidrocoloizilor (pectina, xantan) protejează proteinele din zer, prevenind precipitarea lor si le stabilizează in timpul procesării termice si pe perioada de depozitare; de asemenea, previn apariția sinerezei si imprima textura si consistenta produsului finit \· 2 Ο 1 2 - Ο Ο 8 4 4 - - Μthe use of whole whey, without the addition of water, ensures rehydration, provides branched essential amino acids and vitamins and brings an intake of electrolytes (especially calcium and magnesium), which compensates for losses through perspiration, using physical effort using whole whey to minimize costs. production the addition of hydrocolloids (pectin, xanthan) protects whey proteins, preventing their precipitation and stabilizing them during heat processing and storage; also prevent the appearance of syneresis and print the texture and consistency of the finished product \ · 2 Ο 1 2 - Ο Ο 8 4 4 - - Μ
Ο -11- 2012 concentratele naturale de fructe furnizează carbohidrati, un surplus de energie înainte sau după antrenamente, si cantitati mici de electroliti (sodiu, potasiu, clor) aromele naturale de fructe si concentratele naturale de fructe selecționate acopera gustul si mirosul de zer, oferind băuturii caracteristici organoleptice superioare diversificarea gamei de băuturi „ready to drink” pe baza de zer integral, pentru sportivi termen de valabilitate prelungit al băuturii fortifiante pe baza din zer datorita omogenizării amestecului la presiune ridicata si prezentei hidrocoloizilor care stabilizează amestecul tehnologie simpla, ușor de realizatΟ -11- 2012 natural fruit concentrates provide carbohydrates, a surplus of energy before or after workouts, and small amounts of electrolytes (sodium, potassium, chlorine) natural fruit flavors and selected natural fruit concentrates cover the taste and smell of whey, offering the drink superior organoleptic characteristics diversification of the range of ready-to-drink drinks based on whole whey, for athletes extended shelf life of the fortifying drink based on whey due to the homogenization of the mixture at high pressure and the presence of hydrocolloids that stabilize the mixture. accomplished
Prezenta invenție se ilustrează prin 2 exemple de realizare.The present invention is illustrated by 2 embodiments.
Exemplul 1Example 1
Pentru prepararea unui litru de băutură pe baza de zer, condiționată conform prezentei invenții, procedeul este următorul:For the preparation of one liter of whey beverage, packaged according to the present invention, the process is as follows:
0,5...1,5 g xantan in amestec cu 30...100 g fructoza naturala cristalina „food grade” se hidrateaza in 500...1000 mL zer filtrat, clarificat si pasteurizat, sub agitare continua, timp de 20...30 minute si la temperatura de 40...50 °C, pentru dispersia completa a xantanului. După dizolvarea acestora se adauga 15...20 g cicoare sau cacao si se continua agitarea. Amestecul final se omogenizează la înalta presiune de 50...100 bari si temperatura de 30...60 °C, timp de 3...5 minute. Se imbuteliaza in sticle sterilizate in prealabil si se pasteurizează la temperaturi cuprinse intre 70...80 °C. Se răcește brusc si se pastreaza la frigider la temperatura de 2...4 °C. Produsul obtinut are pH-ul 6.0.5 ... 1.5 g xanthan mixed with 30 ... 100 g natural crystalline fructose "food grade" is hydrated in 500 ... 1000 mL filtered whey, clarified and pasteurized, under continuous stirring, for 20 ... 30 minutes and at a temperature of 40 ... 50 ° C, for the complete dispersion of xanthan. After dissolving them, add 15-20 g of chicory or cocoa and continue stirring. The final mixture is homogenized at a high pressure of 50 ... 100 bar and a temperature of 30 ... 60 ° C, for 3 ... 5 minutes. It is bottled in previously sterilized bottles and pasteurized at temperatures between 70 ... 80 ° C. Cool suddenly and store in the refrigerator at a temperature of 2 ... 4 ° C. The product obtained has a pH of 6.
Exemplul 2Example 2
1.. .3.5 g pectina in amestec cu 30...100 g fructoza naturala cristalina „food grade” se hidrateaza in1 .. .3.5 g pectin mixed with 30 ... 100 g natural crystalline fructose "food grade" is hydrated in
500.. .1000 mL zer filtrat, clarificat si pasteurizat sub agitare continua timp de 20...30 minute si la temperatura de 40...50 °C pentru dispersia completa a pectinei. Separat se amesteca 50...100 g concentrat de fructe cu 0,4...1,2 g aroma de fructe si cu 0,30...8g colorant natural corespunzător peste care se adauga zerul cu pectina hidratata pana la 1000 mL, se ajusteaza pH-ul la 3,8 cu soluție 50% acid citric sau soluție 80% acid lactic. Amestecul final se omogenizează la înalta presiune de 50...100 bari si temperatura de 30...60 °C, timp de 3...5 minute. Se imbuteliaza in sticle sterilizate in prealabil si se pasteurizează la temperaturi cuprinse intre 7O...8O°C. Se răcește brusc si se pastreaza la frigider la temperatura de 2...4 °C. Produsul obtinut are pH-ul 3,8.500 .. .1000 mL filtered whey, clarified and pasteurized under continuous stirring for 20 ... 30 minutes and at a temperature of 40 ... 50 ° C for complete dispersion of pectin. Separately mix 50 ... 100 g fruit concentrate with 0.4 ... 1.2 g fruit flavor and with 0.30 ... 8 g corresponding natural dye over which the whey with hydrated pectin up to 1000 mL is added , adjust the pH to 3.8 with 50% citric acid solution or 80% lactic acid solution. The final mixture is homogenized at a high pressure of 50 ... 100 bar and a temperature of 30 ... 60 ° C, for 3 ... 5 minutes. It is bottled in pre-sterilized bottles and pasteurized at temperatures between 7O ... 8O ° C. Cool suddenly and store in the refrigerator at a temperature of 2 ... 4 ° C. The product obtained has a pH of 3.8.
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