PL58083B1 - - Google Patents

Info

Publication number

PL58083B1

PL58083B1 PL113335A PL11333566A PL58083B1 PL 58083 B1 PL58083 B1 PL 58083B1 PL 113335 A PL113335 A PL 113335A PL 11333566 A PL11333566 A PL 11333566A PL 58083 B1 PL58083 B1 PL 58083B1

Authority

PL

Poland

Prior art keywords

polyamide

powder

mixture

hexamethylenediamine

benzene

Prior art date

1966-03-04

Links

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• 239000004952 Polyamide Substances 0.000 claims description 40
• 229920002647 polyamide Polymers 0.000 claims description 40
• 239000000945 filler Substances 0.000 claims description 19
• 150000003504 terephthalic acids Chemical class 0.000 claims description 14
• 238000002360 preparation method Methods 0.000 claims description 12
• 238000006243 chemical reaction Methods 0.000 claims description 10
• 238000000034 method Methods 0.000 claims description 10
• -1 aliphatic dicarboxylic acids Chemical class 0.000 claims description 9
• 238000003756 stirring Methods 0.000 claims description 7
• 239000012442 inert solvent Substances 0.000 claims description 6
• 150000004985 diamines Chemical class 0.000 claims description 5
• 239000000428 dust Substances 0.000 claims description 5
• 125000001931 aliphatic group Chemical group 0.000 claims description 3
• YCWSUKQGVSGXJO-NTUHNPAUSA-N nifuroxazide Chemical group C1=CC(O)=CC=C1C(=O)N\N=C\C1=CC=C([N+]([O-])=O)O1 YCWSUKQGVSGXJO-NTUHNPAUSA-N 0.000 claims description 3
• 238000006068 polycondensation reaction Methods 0.000 claims description 3
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 45
• NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 32
• 239000000843 powder Substances 0.000 description 23
• KVNYFPKFSJIPBJ-UHFFFAOYSA-N 1,2-diethylbenzene Chemical compound CCC1=CC=CC=C1CC KVNYFPKFSJIPBJ-UHFFFAOYSA-N 0.000 description 16
• 239000000203 mixture Substances 0.000 description 16
• 238000009833 condensation Methods 0.000 description 15
• 230000005494 condensation Effects 0.000 description 15
• XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 14
• 150000002531 isophthalic acids Chemical class 0.000 description 11
• 239000002245 particle Substances 0.000 description 9
• RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 8
• OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
• 229910002804 graphite Inorganic materials 0.000 description 7
• 239000010439 graphite Substances 0.000 description 7
• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
• ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 5
• GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 5
• 239000000725 suspension Substances 0.000 description 5
• 125000006267 biphenyl group Chemical group 0.000 description 4
• 239000011248 coating agent Substances 0.000 description 4
• 238000000576 coating method Methods 0.000 description 4
• 229910052742 iron Inorganic materials 0.000 description 4
• 238000002156 mixing Methods 0.000 description 4
• 238000005245 sintering Methods 0.000 description 4
• 239000002904 solvent Substances 0.000 description 4
• 229910052782 aluminium Inorganic materials 0.000 description 3
• XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
• 238000001816 cooling Methods 0.000 description 3
• 239000010949 copper Substances 0.000 description 3
• 229910052751 metal Inorganic materials 0.000 description 3
• 239000002184 metal Substances 0.000 description 3
• 239000000049 pigment Substances 0.000 description 3
• 239000004033 plastic Substances 0.000 description 3
• 229920003023 plastic Polymers 0.000 description 3
• 229940058401 polytetrafluoroethylene Drugs 0.000 description 3
• 239000004810 polytetrafluoroethylene Substances 0.000 description 3
• 238000000926 separation method Methods 0.000 description 3
• QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 2
• UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
• CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
• ISKQADXMHQSTHK-UHFFFAOYSA-N [4-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=C(CN)C=C1 ISKQADXMHQSTHK-UHFFFAOYSA-N 0.000 description 2
• 239000002253 acid Substances 0.000 description 2
• 150000007513 acids Chemical class 0.000 description 2
• WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
• 239000000956 alloy Substances 0.000 description 2
• 229910045601 alloy Inorganic materials 0.000 description 2
• IRERQBUNZFJFGC-UHFFFAOYSA-L azure blue Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[S-]S[S-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] IRERQBUNZFJFGC-UHFFFAOYSA-L 0.000 description 2
• 229910052802 copper Inorganic materials 0.000 description 2
• FHESUNXRPBHDQM-UHFFFAOYSA-N diphenyl benzene-1,3-dicarboxylate Chemical compound C=1C=CC(C(=O)OC=2C=CC=CC=2)=CC=1C(=O)OC1=CC=CC=C1 FHESUNXRPBHDQM-UHFFFAOYSA-N 0.000 description 2
• HPGJOUYGWKFYQW-UHFFFAOYSA-N diphenyl benzene-1,4-dicarboxylate Chemical compound C=1C=C(C(=O)OC=2C=CC=CC=2)C=CC=1C(=O)OC1=CC=CC=C1 HPGJOUYGWKFYQW-UHFFFAOYSA-N 0.000 description 2
• KWKXNDCHNDYVRT-UHFFFAOYSA-N dodecylbenzene Chemical compound CCCCCCCCCCCCC1=CC=CC=C1 KWKXNDCHNDYVRT-UHFFFAOYSA-N 0.000 description 2
• 238000001746 injection moulding Methods 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
• 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
• 150000003839 salts Chemical class 0.000 description 2
• 239000000243 solution Substances 0.000 description 2
• 150000005199 trimethylbenzenes Chemical class 0.000 description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
• 239000008096 xylene Substances 0.000 description 2
• AILDTIZEPVHXBF-UHFFFAOYSA-N Argentine Natural products C1C(C2)C3=CC=CC(=O)N3CC1CN2C(=O)N1CC(C=2N(C(=O)C=CC=2)C2)CC2C1 AILDTIZEPVHXBF-UHFFFAOYSA-N 0.000 description 1
• 102100030393 G-patch domain and KOW motifs-containing protein Human genes 0.000 description 1
• 244000308495 Potentilla anserina Species 0.000 description 1
• 235000016594 Potentilla anserina Nutrition 0.000 description 1
• ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
• HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
• 239000005083 Zinc sulfide Substances 0.000 description 1
• 235000011037 adipic acid Nutrition 0.000 description 1
• 239000001361 adipic acid Substances 0.000 description 1
• 230000000181 anti-adherent effect Effects 0.000 description 1
• KKEYFWRCBNTPAC-UHFFFAOYSA-N benzene-dicarboxylic acid Natural products OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• BDIFKMOUQSYRRD-UHFFFAOYSA-N diphenyl hexanedioate Chemical compound C=1C=CC=CC=1OC(=O)CCCCC(=O)OC1=CC=CC=C1 BDIFKMOUQSYRRD-UHFFFAOYSA-N 0.000 description 1
• OPDNNKCDHDLBCJ-UHFFFAOYSA-N diphenyl nonanedioate Chemical compound C=1C=CC=CC=1OC(=O)CCCCCCCC(=O)OC1=CC=CC=C1 OPDNNKCDHDLBCJ-UHFFFAOYSA-N 0.000 description 1
• 238000000227 grinding Methods 0.000 description 1
• 230000017525 heat dissipation Effects 0.000 description 1
• 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
• 238000007373 indentation Methods 0.000 description 1
• 238000002347 injection Methods 0.000 description 1
• 239000007924 injection Substances 0.000 description 1
• 239000011256 inorganic filler Substances 0.000 description 1
• 229910003475 inorganic filler Inorganic materials 0.000 description 1
• NNIPDXPTJYIMKW-UHFFFAOYSA-N iron tin Chemical compound [Fe].[Sn] NNIPDXPTJYIMKW-UHFFFAOYSA-N 0.000 description 1
• JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
• 238000005304 joining Methods 0.000 description 1
• 239000007788 liquid Substances 0.000 description 1
• 230000005415 magnetization Effects 0.000 description 1
• 238000005259 measurement Methods 0.000 description 1
• 239000000320 mechanical mixture Substances 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• 229910044991 metal oxide Inorganic materials 0.000 description 1
• 150000004706 metal oxides Chemical class 0.000 description 1
• 229910052976 metal sulfide Inorganic materials 0.000 description 1
• 150000002739 metals Chemical class 0.000 description 1
• CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 description 1
• 229910052982 molybdenum disulfide Inorganic materials 0.000 description 1
• 239000012766 organic filler Substances 0.000 description 1
• 239000003973 paint Substances 0.000 description 1
• QQVIHTHCMHWDBS-UHFFFAOYSA-N perisophthalic acid Natural products OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 1
• 150000002989 phenols Chemical class 0.000 description 1
• 239000011541 reaction mixture Substances 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 238000007873 sieving Methods 0.000 description 1
• 239000011877 solvent mixture Substances 0.000 description 1
• PTISTKLWEJDJID-UHFFFAOYSA-N sulfanylidenemolybdenum Chemical compound [Mo]=S PTISTKLWEJDJID-UHFFFAOYSA-N 0.000 description 1
• 150000004763 sulfides Chemical class 0.000 description 1
• 229910052718 tin Inorganic materials 0.000 description 1
• 239000004408 titanium dioxide Substances 0.000 description 1
• OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
• 239000002966 varnish Substances 0.000 description 1
• 229910052725 zinc Inorganic materials 0.000 description 1
• 239000011701 zinc Substances 0.000 description 1
• DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 description 1