PL17028B1 - Method for the production of shapes from potassium cyanides. - Google Patents

Method for the production of shapes from potassium cyanides.

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Publication number
PL17028B1
PL17028B1 PL17028A PL1702830A PL17028B1 PL 17028 B1 PL17028 B1 PL 17028B1 PL 17028 A PL17028 A PL 17028A PL 1702830 A PL1702830 A PL 1702830A PL 17028 B1 PL17028 B1 PL 17028B1
Authority
PL
Poland
Prior art keywords
pressing
shapes
production
pressure
powder
Prior art date
Application number
PL17028A
Other languages
Polish (pl)
Filing date
Publication date
Application filed filed Critical
Publication of PL17028B1 publication Critical patent/PL17028B1/en

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Description

Cyjanek sodu w postaci proszku, otrzy¬ mywany, naprzyklad, przez odparowywa¬ nie (roztworów cyjanku sodu, jest, jak wia¬ domo, bardzo sklonny d)o rozpylania sie i wskutek tego bardzo niebezpieczny w uzy¬ ciu; w handlu znajdujemy go przeto w po¬ staci prasowanych brykietów* Nie udalo sie jednak dotad usunac wspomnianych niedogodnosci, bowiem brykiety latwo roz¬ padaja sie przy transporcie i wytwarzaja pyl, poniewaz zespolenie czasteczek po¬ szczególnych zapomoca prasowania nie da¬ lo w rezultacie pnoduktu scislego i trwale¬ go.Próbowano juz zwiekszyc wytrzyma¬ losc produktu prasowanego przez dluzsze ogrzewanie gotowych form przy zastosowa¬ niu prózni albo przez dodanie wodorotlen¬ ku potasowca przed prasowaniem; propo¬ nowano równiez tworzyc brykiety przez prasowanie zawierajacej wode mieszaniny cyjanku potasu i sodu, przyczem czescio¬ wo rozpuszczajacy sie w zawartej wodzie cyjanek sodu mial rzekomo zlepiac po¬ szczególne ziarna. Jednakze w handlu po¬ zadane sa przewaznie czyste zwiazki, a nie mieszaniny cyjanków potasowców, a po¬ nadto zawartosc wody wplywa ujemnie natrwalosc procjyrtorw pod wzgledem che¬ micznym, [przeto .sposób ten równiez nie zadowala.*"t. ¦ v Stwierdzono, iz wytwarzanie nadzwyczaj trwalych, nie pylacych ksztaltek, przez prasowanie proszku cyjanku potasowoa, u- daje sie, jesli suchy proszek, bez dodatku srodków wiazacych, ptoddac dzialaniu tak wysokich cisnien, aby proszek stracil bu¬ dowe ziarnista, a ksztaltka przybrala bu¬ dowe krystaliczna, przyczem wzrasta znacznie wytrzymalosc na cisnienie. Nada¬ jace sie do tego cisnienie powinno wynosic 800 kg, a lepiej 1000 kg na om2 i wzwyz.Wlajsnosci fizyczne tak otrzymanych mas sa podobne do wlasnosci fizycznych pno- dtttotów, powstajacych przez ochlodzenie stopionych soli.Ksztaltki prasowane z cyjanków otrzy¬ mane powyzszym sposobem wykazuja nad¬ zwyczajna trwalosc i nie daja przy gwal- townem lamaniu pylu, lecz niniejsze lub wieksze odlamki. Okazalo sie, iz wytrzy¬ malosc na cisnienie prasowanych cyjanków potasowców, wzrasta niespodziewanie sil¬ nie w granicach cisnien od 700 — 1000 kg na cm2, podczas gdy powyzej i ponizej tych granic, nastepuje znacznie mniejszy wzrost, jak wynika z przytoczonej tabeli. cisnienie przy wytrzymalosc na prasowaniu cisnienie ksztaltek kg/cm2 kg/cm2 300 114 500 217 700 229 900 321 1000 398 1200 402 Tern samem ilustruje sie liczbowo" nie¬ spodziewane zmiany wlasnosci fizycznych, jakich doznaja cyjanki potasowców piod wplywem wysokich cisnien tloczacych. PLSodium cyanide in the form of a powder, obtained, for example, by evaporation (sodium cyanide solutions, is known to be very prone to spraying and therefore very dangerous to use; Therefore, we find it in the form of pressed briquettes * However, it has not been possible to remove the above-mentioned inconveniences so far, because the briquettes easily disintegrate during transport and generate dust, because the joining of the particles by pressing did not result in a precise product Attempts have already been made to increase the strength of the pressed product by heating the finished molds for longer periods using a vacuum or by adding potassium hydroxide prior to pressing; it has also been proposed to make briquettes by pressing a water-containing mixture of potassium cyanide and sodium cyanide, whereby the sodium cyanide which is partially dissolved in the water content is supposed to stick together individual grains. However, in trade, mostly pure compounds are desired, and not mixtures of potassium cyanides, and in addition, the water content negatively affects the persistence of the procyyrors from a chemical point of view, [therefore, this method is also not satisfactory. * "T. that the production of extremely durable, dust-free shapes by pressing the powder of potassium cyanide is successful, if the dry powder, without the addition of binding agents, is subjected to the action of such high pressures that the powder loses its structure granular and the shape becomes crystalline. Therefore, the pressure resistance increases considerably. The pressure to be applied should be 800 kg, and preferably 1000 kg per square meter and above. The physical properties of the masses obtained in this way are similar to the physical properties of the molten salts produced by cooling. the cyanide presses obtained by the above process show extraordinary stability and do not give rise to sudden dust breaking, but rather smaller or larger fragments. it has been found that the pressure resistance of the pressed potassium cyanide increases surprisingly strongly within the pressure range of 700-1000 kg per cm 2, while above and below these limits, there is much less increase as can be seen from the table above. pressure at pressing strength pressure of the shapes kg / cm2 kg / cm2 300 114 500 217 700 229 900 321 1000 398 1200 402 Tern itself illustrates itself numerically "unexpected changes in physical properties experienced by potassium cyanide with high pressing pressure. EN

Claims (1)

1. Zastrzezenie patentowe, Sposób wytwarzania ksztaltek z proszku cyjanku potasoiwca przez prasowanie, zna¬ mienny tern, ze suchy, wolny od srodków wiazacych proszek poddaje isie cisnieniom tloczacym, wyzszym niz 700 kg/cm2, dzieki czemu proszek traci budowe ziarnista, a ksztaltki prasowane przyjmuja budowe krystaliczna przy równoczesnem znacznem zwiekszeniu swej wytrzymalosci na cisnienie. I. A k t i e n g e s e 11 s c h a f t. Zastepca: Dr. inz. M, Kryzan, rzecznik patentowy. Druk L. Boguslawskiego i Skl, Warszawa. PL1. Claim, A method for producing particles from potassium cyanide powder by pressing, the characteristic dry, free from binding agents is subjected to a pressing pressure of more than 700 kg / cm 2, as a result of which the powder loses its granular structure and the particles are pressed take on a crystalline structure while significantly increasing their pressure resistance. I. A k t i e n g e s e 11 s c h a f t. Deputy: Dr. inz. M, Kryzan, patent attorney. Printed by L. Boguslawski and Skl, Warsaw. PL
PL17028A 1930-08-23 Method for the production of shapes from potassium cyanides. PL17028B1 (en)

Publications (1)

Publication Number Publication Date
PL17028B1 true PL17028B1 (en) 1932-10-31

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