PL113384B1 - Method of separation of cyanogen chloride from gas mixtures containing cyanogen,chloride,hydrogen chloride and chlorine as a chief constituents - Google Patents
Method of separation of cyanogen chloride from gas mixtures containing cyanogen,chloride,hydrogen chloride and chlorine as a chief constituents Download PDFInfo
- Publication number
- PL113384B1 PL113384B1 PL20147877A PL20147877A PL113384B1 PL 113384 B1 PL113384 B1 PL 113384B1 PL 20147877 A PL20147877 A PL 20147877A PL 20147877 A PL20147877 A PL 20147877A PL 113384 B1 PL113384 B1 PL 113384B1
- Authority
- PL
- Poland
- Prior art keywords
- chlorine
- chloride
- chlorocyanate
- hydrogen chloride
- weight
- Prior art date
Links
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 title claims description 40
- 239000000460 chlorine Substances 0.000 title claims description 40
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 title claims description 39
- 229910052801 chlorine Inorganic materials 0.000 title claims description 39
- 239000000203 mixture Substances 0.000 title claims description 37
- 229910000041 hydrogen chloride Inorganic materials 0.000 title claims description 36
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 title claims description 36
- 239000007789 gas Substances 0.000 title claims description 32
- 238000000034 method Methods 0.000 title claims description 24
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 title description 17
- 238000000926 separation method Methods 0.000 title description 12
- JMANVNJQNLATNU-UHFFFAOYSA-N glycolonitrile Natural products N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 title description 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 title description 5
- 239000000470 constituent Substances 0.000 title 1
- JEVCWSUVFOYBFI-UHFFFAOYSA-N cyanyl Chemical compound N#[C] JEVCWSUVFOYBFI-UHFFFAOYSA-N 0.000 title 1
- SJXIVKQAVJISKW-UHFFFAOYSA-N chloro cyanate Chemical compound ClOC#N SJXIVKQAVJISKW-UHFFFAOYSA-N 0.000 claims description 32
- 239000007788 liquid Substances 0.000 claims description 9
- 238000010992 reflux Methods 0.000 claims description 9
- 238000009835 boiling Methods 0.000 claims description 6
- 239000007792 gaseous phase Substances 0.000 claims 1
- 238000009833 condensation Methods 0.000 description 12
- 230000005494 condensation Effects 0.000 description 12
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 7
- 238000000746 purification Methods 0.000 description 7
- 238000011403 purification operation Methods 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- 238000005829 trimerization reaction Methods 0.000 description 6
- 238000005660 chlorination reaction Methods 0.000 description 4
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 4
- 239000008246 gaseous mixture Substances 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- BNIXVQGCZULYKV-UHFFFAOYSA-N pentachloroethane Chemical compound ClC(Cl)C(Cl)(Cl)Cl BNIXVQGCZULYKV-UHFFFAOYSA-N 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- -1 titanium chlorocyanate Chemical compound 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treating Waste Gases (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL20147877A PL113384B1 (en) | 1977-10-11 | 1977-10-11 | Method of separation of cyanogen chloride from gas mixtures containing cyanogen,chloride,hydrogen chloride and chlorine as a chief constituents |
| YU233078A YU233078A (en) | 1977-10-11 | 1978-10-03 | Process for the separation of cyanochloride from gaseous mixtures containing chiefly cyanochloride,hydrogen chloride and chlorine |
| DD20834278A DD139569A5 (de) | 1977-10-11 | 1978-10-09 | Verfahren zur abtrennung von chlorcyan aus gasgemischen |
| BG041031A BG29278A3 (en) | 1977-10-11 | 1978-10-09 | Meyhod for determining of chlorcyan in gas mixtures containing principally chlorcyan, chlorhydrogen and chlorine |
| HUII000274 HU179494B (en) | 1977-10-11 | 1978-10-10 | Process for the separation of chlorocyan from a gaseous mixture containing chlorocyan,hydrochloric acid gas and chlorine gas |
| RO7895376A RO75465A (ro) | 1977-10-11 | 1978-10-10 | Procedeu pentru separarea clorcianului din amestecuri gazoase |
| CS658378A CS222666B2 (cs) | 1977-10-11 | 1978-10-10 | Způsob oddělování chlorkyanu z plynných směsí, obsahujících převážně chlorkyan, chlorovodík a chlor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL20147877A PL113384B1 (en) | 1977-10-11 | 1977-10-11 | Method of separation of cyanogen chloride from gas mixtures containing cyanogen,chloride,hydrogen chloride and chlorine as a chief constituents |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL201478A1 PL201478A1 (pl) | 1979-05-07 |
| PL113384B1 true PL113384B1 (en) | 1980-12-31 |
Family
ID=19985038
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL20147877A PL113384B1 (en) | 1977-10-11 | 1977-10-11 | Method of separation of cyanogen chloride from gas mixtures containing cyanogen,chloride,hydrogen chloride and chlorine as a chief constituents |
Country Status (7)
| Country | Link |
|---|---|
| BG (1) | BG29278A3 (cs) |
| CS (1) | CS222666B2 (cs) |
| DD (1) | DD139569A5 (cs) |
| HU (1) | HU179494B (cs) |
| PL (1) | PL113384B1 (cs) |
| RO (1) | RO75465A (cs) |
| YU (1) | YU233078A (cs) |
-
1977
- 1977-10-11 PL PL20147877A patent/PL113384B1/pl unknown
-
1978
- 1978-10-03 YU YU233078A patent/YU233078A/xx unknown
- 1978-10-09 DD DD20834278A patent/DD139569A5/de unknown
- 1978-10-09 BG BG041031A patent/BG29278A3/xx unknown
- 1978-10-10 HU HUII000274 patent/HU179494B/hu unknown
- 1978-10-10 RO RO7895376A patent/RO75465A/ro unknown
- 1978-10-10 CS CS658378A patent/CS222666B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DD139569A5 (de) | 1980-01-09 |
| BG29278A3 (en) | 1980-10-15 |
| YU233078A (en) | 1982-06-30 |
| RO75465A (ro) | 1981-01-30 |
| PL201478A1 (pl) | 1979-05-07 |
| HU179494B (en) | 1982-10-28 |
| CS222666B2 (cs) | 1983-07-29 |
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