NZ768101B2 - Highly-soluble rebaudioside d - Google Patents

Highly-soluble rebaudioside d

Info

Publication number
NZ768101B2
NZ768101B2 NZ768101A NZ76810119A NZ768101B2 NZ 768101 B2 NZ768101 B2 NZ 768101B2 NZ 768101 A NZ768101 A NZ 768101A NZ 76810119 A NZ76810119 A NZ 76810119A NZ 768101 B2 NZ768101 B2 NZ 768101B2
Authority
NZ
New Zealand
Prior art keywords
crystal
rebaudioside
food
highly
exhibiting
Prior art date
Application number
NZ768101A
Other versions
NZ768101A (en
Inventor
Shoji Kudo
Koji Nagao
Hiroshi Takiyama
Soichiro Urai
Yoshiaki Yokoo
Original Assignee
Suntory Holdings Limited
Filing date
Publication date
Application filed by Suntory Holdings Limited filed Critical Suntory Holdings Limited
Priority claimed from PCT/JP2019/007753 external-priority patent/WO2019168082A1/en
Publication of NZ768101A publication Critical patent/NZ768101A/en
Publication of NZ768101B2 publication Critical patent/NZ768101B2/en

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A23L2/60—Sweeteners
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A23L27/36—Terpene glycosides
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2250/00—Food ingredients
    • A23V2250/24—Non-sugar sweeteners
    • A23V2250/262—Stevioside
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C07H15/256—Polyterpene radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J51/00—Normal steroids with unmodified cyclopenta(a)hydrophenanthrene skeleton not provided for in groups C07J1/00 - C07J43/00

Abstract

The purpose of the present invention is to provide a crystal of rebaudioside D that exhibits high solubility in water. In one embodiment, the present invention provides a rebaudioside D crystal having a crystalline form a that shows peaks in X-ray diffraction (CuKa:?=1.5405 Å) at two or more positions selected from the group consisting of 2?=6.7±0.2 deg, 10.8±0.2 deg, 12.9±0.15 deg, and 22.2±0.2 deg.

Claims (9)

Claims
1. A crystal of rebaudioside D in a crystalline form ? exhibiting peaks at 2? = 6.7 ? 0.2 deg, 10.8 ? 0.2 deg, 12.9 ? 0.15 deg, and 22.2 ? 0.2 deg, in X-ray diffraction (CuK?: ? = 1.5405 Å).
2. A crystal of rebaudioside D in a crystalline form ? exhibiting peaks at 2? = 5.9 ? 0.2 deg, 7.3 ? 0.2 deg, 11.5 ? 0.2 deg, and 16.8 ? 0.2 deg, in X-ray diffraction (CuK?:? = 1.5405 Å).
3. The crystal according to claim 1, further exhibiting a peak at at least one position selected from the group consisting of 2? = 6.3 ? 0.2 deg, 8.9 ? 0.2 deg, 10.3 ? 0.2 deg, 14.4 ? 0.2 deg, 17.4 ? 0.2 deg, and 17.8 ? 0.2
4. The crystal according to claim 2, further exhibiting a peak at at least one position ed from the group consisting of 2? = 18.0 ? 0.2 deg and 19.0 ? 0.2 deg.
5. The crystal according to any one of claims 1 to 4, having a moisture content of 0.1 wt% to 2.0 wt%.
6. A sweetener composition sing the crystal ing to any one of claims 1 to 5.
7. A food or beverage comprising the sweetener composition according to claim 6.
8. The food or beverage according to claim 7, wherein the rebaudioside D is contained in the food or ge in an amount of 10 mass ppm to 600 mass ppm. 20209263_1 (GHMatters) P113974.NZ
9. The crystal ing to claim 1 or 2, substantially as herein described with reference to any one of the Examples or any one of the
NZ768101A 2019-02-28 Highly-soluble rebaudioside d NZ768101B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2018036638 2018-03-01
PCT/JP2019/007753 WO2019168082A1 (en) 2018-03-01 2019-02-28 Highly-soluble rebaudioside d

Publications (2)

Publication Number Publication Date
NZ768101A NZ768101A (en) 2023-12-22
NZ768101B2 true NZ768101B2 (en) 2024-03-26

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