NO324095B1 - Integrert analyseprosess og innretning for hydrokarbonkarakterisering ved distillasjonssimulering - Google Patents
Integrert analyseprosess og innretning for hydrokarbonkarakterisering ved distillasjonssimulering Download PDFInfo
- Publication number
- NO324095B1 NO324095B1 NO19996365A NO996365A NO324095B1 NO 324095 B1 NO324095 B1 NO 324095B1 NO 19996365 A NO19996365 A NO 19996365A NO 996365 A NO996365 A NO 996365A NO 324095 B1 NO324095 B1 NO 324095B1
- Authority
- NO
- Norway
- Prior art keywords
- column
- gas chromatography
- fraction
- retention
- fractions
- Prior art date
Links
- 238000004821 distillation Methods 0.000 title claims description 24
- 238000000034 method Methods 0.000 title claims description 19
- 238000012512 characterization method Methods 0.000 title claims description 12
- 229930195733 hydrocarbon Natural products 0.000 title claims description 10
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 10
- 230000008569 process Effects 0.000 title claims description 10
- 239000004215 Carbon black (E152) Substances 0.000 title claims description 5
- 238000012351 Integrated analysis Methods 0.000 title claims description 4
- 238000004088 simulation Methods 0.000 title description 4
- 238000004817 gas chromatography Methods 0.000 claims description 52
- 238000004811 liquid chromatography Methods 0.000 claims description 37
- 230000014759 maintenance of location Effects 0.000 claims description 29
- 238000002347 injection Methods 0.000 claims description 21
- 239000007924 injection Substances 0.000 claims description 21
- 238000004458 analytical method Methods 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 9
- 238000000926 separation method Methods 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 8
- 238000004587 chromatography analysis Methods 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 6
- 238000001704 evaporation Methods 0.000 claims description 4
- 230000008020 evaporation Effects 0.000 claims description 4
- 238000011010 flushing procedure Methods 0.000 claims description 2
- 238000006073 displacement reaction Methods 0.000 claims 1
- 238000012546 transfer Methods 0.000 description 12
- 239000007789 gas Substances 0.000 description 7
- 230000008878 coupling Effects 0.000 description 6
- 238000010168 coupling process Methods 0.000 description 6
- 238000005859 coupling reaction Methods 0.000 description 6
- 238000010828 elution Methods 0.000 description 6
- 239000012071 phase Substances 0.000 description 6
- 230000005526 G1 to G0 transition Effects 0.000 description 5
- 239000003463 adsorbent Substances 0.000 description 5
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 239000003209 petroleum derivative Substances 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 238000003965 capillary gas chromatography Methods 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- 239000003208 petroleum Substances 0.000 description 3
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- -1 alkyl aliphatic Chemical class 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000012159 carrier gas Substances 0.000 description 2
- 239000012156 elution solvent Substances 0.000 description 2
- 238000004508 fractional distillation Methods 0.000 description 2
- 238000005194 fractionation Methods 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- BKIMMITUMNQMOS-UHFFFAOYSA-N nonane Chemical compound CCCCCCCCC BKIMMITUMNQMOS-UHFFFAOYSA-N 0.000 description 2
- 239000012716 precipitator Substances 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 238000011001 backwashing Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 239000002803 fossil fuel Substances 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000010606 normalization Methods 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/468—Flow patterns using more than one column involving switching between different column configurations
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
- G01N2030/884—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds
- G01N2030/8854—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds involving hydrocarbons
Landscapes
- General Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Sampling And Sample Adjustment (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9816298A FR2787576B1 (fr) | 1998-12-22 | 1998-12-22 | Procede et dispositif d'analyse integree pour la caracterisation d'hydrocarbures, par simulation de distillation |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO996365D0 NO996365D0 (no) | 1999-12-21 |
| NO996365L NO996365L (no) | 2000-06-23 |
| NO324095B1 true NO324095B1 (no) | 2007-08-13 |
Family
ID=9534377
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO19996365A NO324095B1 (no) | 1998-12-22 | 1999-12-21 | Integrert analyseprosess og innretning for hydrokarbonkarakterisering ved distillasjonssimulering |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US6237396B1 (fr) |
| CA (1) | CA2296194C (fr) |
| FR (1) | FR2787576B1 (fr) |
| GB (1) | GB2346094B (fr) |
| NO (1) | NO324095B1 (fr) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6632268B2 (en) * | 2001-02-08 | 2003-10-14 | Oakland University | Method and apparatus for comprehensive two-dimensional gas chromatography |
| US6908557B2 (en) * | 2002-06-25 | 2005-06-21 | Thar Technologies, Inc. | Collection system for chromatographic system |
| CN1307419C (zh) * | 2003-08-29 | 2007-03-28 | 中国石油化工股份有限公司 | 利用固相萃取和质谱分析柴油烃族组成的方法 |
| FR2873816B1 (fr) * | 2004-08-02 | 2006-11-17 | Inst Francais Du Petrole | Procede et dispositif d'analyse integree d'un echantillon d'hydrocarbures |
| AU2005287017B2 (en) * | 2004-09-17 | 2009-06-11 | Bp Oil International Limited | Portable apparatus for analysis of a refinery feedstock or a product of a refinery process |
| CN101470105B (zh) * | 2007-12-25 | 2011-12-21 | 上海神开石油化工装备股份有限公司 | 一种对泥浆中c1～c8烃组分分析方法和系统 |
| US20100206812A1 (en) * | 2009-02-19 | 2010-08-19 | Primafuel, Inc | High efficiency separations method and apparatus |
| WO2012012346A1 (fr) * | 2010-07-19 | 2012-01-26 | Sgs North America Inc. | Analyse automatisée de fluides de réservoir pressurisé |
| US8522600B2 (en) | 2010-10-12 | 2013-09-03 | Saudi Arabian Oil Company | Fluid compositional analysis by combined gas chromatographic and direct flash methods |
| CN103091430B (zh) * | 2013-02-20 | 2015-05-20 | 上海烟草集团有限责任公司 | 一种液相色谱-气相色谱在线联用接口的溶剂排空装置及方法 |
| CN106168630A (zh) * | 2015-08-21 | 2016-11-30 | 福建永晶科技有限公司 | 一种利用进样装置实现高纯六氟化硫气体的进样方法 |
| CN105092875A (zh) * | 2015-09-24 | 2015-11-25 | 北京楚翔飞科技开发有限责任公司 | 一种全自动气液多用途进样器 |
| CN105954365B (zh) * | 2015-12-29 | 2018-03-02 | 上海神开石油化工装备股份有限公司 | 一种适用于c1‑c8油气快速录井的气测仪 |
| WO2018059639A1 (fr) * | 2016-09-28 | 2018-04-05 | Evosep Aps | Analyse chromatographique à refocalisation de gradient double à basse pression |
| US11441978B1 (en) * | 2018-04-12 | 2022-09-13 | Elemental Scientific, Inc. | Automatic evaporative sample preparation |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4204952A (en) | 1978-07-07 | 1980-05-27 | Technicon Instruments Corporation | Chromatographic apparatus and method |
| IT1196389B (it) * | 1984-12-28 | 1988-11-16 | Erba Strumentazione | Metodo ed apparecchiatura per la distillazione simulata mediante gas-cromatografia con iniezione diretta non vaporizzante |
| US4935145A (en) | 1985-01-25 | 1990-06-19 | The Dow Chemical Company | On-line coupled liquid and gas chromatography system |
| US4971915A (en) * | 1987-05-15 | 1990-11-20 | Applied Biosystems, Inc. | Simulated distillation of petroleum residues by capillary SFC |
| FI86416C (fi) | 1988-06-09 | 1992-08-25 | Suomen Sokeri Oy | Foerfarande foer tillvaratagande av betain ur melass. |
| DE69208449T2 (de) | 1992-01-10 | 1996-07-04 | Hewlett Packard Co | Hochauflösende Füllkörpersäulenchromatographie in überkritischer Flüssigkeit |
| US5242471A (en) | 1992-05-22 | 1993-09-07 | The Dow Chemical Company | Coupling capillary gas chromatography to traditional liquid chromatography detectors |
| US5808180A (en) | 1996-09-12 | 1998-09-15 | Exxon Research And Engineering Company | Direct method for determination of true boiling point distillation profiles of crude oils by gas chromatography/mass spectrometry |
-
1998
- 1998-12-22 FR FR9816298A patent/FR2787576B1/fr not_active Expired - Fee Related
-
1999
- 1999-12-20 CA CA002296194A patent/CA2296194C/fr not_active Expired - Fee Related
- 1999-12-21 US US09/468,335 patent/US6237396B1/en not_active Expired - Fee Related
- 1999-12-21 NO NO19996365A patent/NO324095B1/no not_active IP Right Cessation
- 1999-12-22 GB GB9930377A patent/GB2346094B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CA2296194A1 (fr) | 2000-06-22 |
| FR2787576A1 (fr) | 2000-06-23 |
| FR2787576B1 (fr) | 2001-01-12 |
| GB2346094A (en) | 2000-08-02 |
| NO996365L (no) | 2000-06-23 |
| US6237396B1 (en) | 2001-05-29 |
| CA2296194C (fr) | 2006-11-07 |
| NO996365D0 (no) | 1999-12-21 |
| GB9930377D0 (en) | 2000-02-16 |
| GB2346094B (en) | 2002-04-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM1K | Lapsed by not paying the annual fees |