NO20091038L - System, reaktor og fremgangsmate for kontinuerlig industriell fremstilling av 3-metakryloksypropylalkoksysilaner - Google Patents

System, reaktor og fremgangsmate for kontinuerlig industriell fremstilling av 3-metakryloksypropylalkoksysilaner

Info

Publication number
NO20091038L
NO20091038L NO20091038A NO20091038A NO20091038L NO 20091038 L NO20091038 L NO 20091038L NO 20091038 A NO20091038 A NO 20091038A NO 20091038 A NO20091038 A NO 20091038A NO 20091038 L NO20091038 L NO 20091038L
Authority
NO
Norway
Prior art keywords
reactor
alkoxysilanes
methacryloxypropyl
continuous industrial
industrial preparation
Prior art date
Application number
NO20091038A
Other languages
English (en)
Inventor
Juergen Erwin Lang
Georg Markowz
Dietmar Wewers
Harald Metz
Norbert Schladerbeck
Original Assignee
Evonik Degussa Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Degussa Gmbh filed Critical Evonik Degussa Gmbh
Publication of NO20091038L publication Critical patent/NO20091038L/no

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B61/00Other general methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093Microreactors, e.g. miniaturised or microfabricated reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42Platinum
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/18Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/18Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804Compounds having Si-O-C linkages
    • C07F7/1872Preparation; Treatments not provided for in C07F7/20
    • C07F7/1876Preparation; Treatments not provided for in C07F7/20 by reactions involving the formation of Si-C linkages
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00788Three-dimensional assemblies, i.e. the reactor comprising a form other than a stack of plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00822Metal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00831Glass
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00835Comprising catalytically active material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00819Materials of construction
    • B01J2219/00837Materials of construction comprising coatings other than catalytically active coatings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00858Aspects relating to the size of the reactor
    • B01J2219/0086Dimensions of the flow channels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00867Microreactors placed in series, on the same or on different supports
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00869Microreactors placed in parallel, on the same or on different supports
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00873Heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00889Mixing

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

SAMMENDRAG Foreliggende oppfinnelse vedrører et system, en reaktor og en framgangsmåte for kontinuerlig industriell gjennomføring av en omsetting hvorved man omsetter metakrylsyreallylester A med en HSi-forbindelse B i nærvær av en katalysator C og eventuelt ytterligere hjelpestoffer, og anlegget er basert minst på reaktantsammenleding (3) av komponentene A (1) og B (2), minst en multielementreaktor (5) som på sin side inkluderer minst to reaktorenheter i form av omskiftbare for-reaktorer (5. 1) og minst en etter for-reaktorene tilkoplet ytterligere reaktorenhet (5.3), og på produktopparbeiding (8).
NO20091038A 2006-08-10 2009-03-09 System, reaktor og fremgangsmate for kontinuerlig industriell fremstilling av 3-metakryloksypropylalkoksysilaner NO20091038L (no)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102006037403 2006-08-10
DE102007023760A DE102007023760A1 (de) 2006-08-10 2007-05-22 Anlage, Reaktor und Verfahren zur kontinuierlichen industriellen Herstellung von 3-Methacryloxypropylalkoxysilanen
PCT/EP2007/056947 WO2008017554A1 (de) 2006-08-10 2007-07-09 Anlage, reaktor und verfahren zur kontinuierlichen industriellen herstellung von 3-methacryloxypropylalkoxysilanen

Publications (1)

Publication Number Publication Date
NO20091038L true NO20091038L (no) 2009-05-06

Family

ID=38738916

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20091038A NO20091038L (no) 2006-08-10 2009-03-09 System, reaktor og fremgangsmate for kontinuerlig industriell fremstilling av 3-metakryloksypropylalkoksysilaner

Country Status (9)

Country Link
US (1) US20100179340A1 (no)
EP (1) EP2049242A1 (no)
JP (1) JP2010500312A (no)
KR (1) KR20090037459A (no)
BR (1) BRPI0715805A2 (no)
CA (1) CA2660406A1 (no)
DE (1) DE102007023760A1 (no)
NO (1) NO20091038L (no)
WO (1) WO2008017554A1 (no)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2135844A1 (de) 2008-06-17 2009-12-23 Evonik Degussa GmbH Verfahren zur Herstellung höherer Hydridosilane
DE102008040475A1 (de) 2008-07-16 2010-01-21 Wacker Chemie Ag Verfahren zur Verhinderung der Polymerisation von ungesättigten Organosiliciumverbindungen
DE102008043422B3 (de) 2008-11-03 2010-01-07 Evonik Degussa Gmbh Verfahren zur Aufreinigung niedermolekularer Hydridosilane
DE102009048087A1 (de) 2009-10-02 2011-04-07 Evonik Degussa Gmbh Verfahren zur Herstellung höherer Hydridosilane
CN102108085A (zh) 2009-12-24 2011-06-29 瓦克化学股份公司 一种在离子液体中制备官能化硅烷的方法
DE102013214830A1 (de) 2013-07-30 2015-02-05 Evonik Industries Ag Verfahren, Vorrichtung und deren Verwendung zur Herstellung von Acryloxy- und Methacryloxypropyltrialkoxysilanen
GB201412406D0 (en) * 2014-07-11 2014-08-27 Geo Speciality Chemicals Uk Ltd Process

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4709067A (en) * 1986-05-20 1987-11-24 Union Carbide Corporation Method for preparing methacryloxy and acryloxy containing organosilanes and organosilicones
US5145979A (en) * 1990-08-23 1992-09-08 Tonen Corporation Processes for the preparation of γ-methacryloxypropylsilane compounds
US5580523A (en) * 1994-04-01 1996-12-03 Bard; Allen J. Integrated chemical synthesizers
DE4434200C2 (de) * 1994-09-24 2002-06-27 Degussa Verfahren zur Herstellung von 3-Acryloxypropylalkoxysilanen
DE19858856A1 (de) * 1998-12-19 2000-06-21 Merck Patent Gmbh Verfahren zur Herstellung von Arylmetallverbindungen und deren Umsetzung mit Elektrophilen
DE19920794A1 (de) * 1999-05-06 2000-11-09 Merck Patent Gmbh Verfahren zur Herstellung von Perlpolymerisaten
DE19959249A1 (de) * 1999-12-08 2001-07-19 Inst Mikrotechnik Mainz Gmbh Modulares Mikroreaktionssystem
US7485454B1 (en) * 2000-03-10 2009-02-03 Bioprocessors Corp. Microreactor
DE10014298A1 (de) * 2000-03-23 2001-09-27 Merck Patent Gmbh Verfahren zur Reduktion aliphatischer, aromatischer oder heterocyclischer organischer Verbindungen mittels Hydriden und/oder deren Derivaten
GB0118858D0 (en) * 2001-08-02 2001-09-26 Dow Corning Hydrosilylation process
DE10333174A1 (de) * 2003-07-22 2005-02-17 Cpc Cellular Process Chemistry Systems Gmbh Verfahren zur Durchführung einer In-Situ-Quench Reaktion
GB0413400D0 (en) * 2004-06-16 2004-07-21 Accentus Plc Catalytic plant and process
WO2006045533A1 (de) * 2004-10-28 2006-05-04 Wacker Chemie Ag Herstellung von organosilanen in gegenwart von iridium-katalysatoren und cokatalysatoren
DE102004058000A1 (de) * 2004-12-01 2006-06-08 Wacker Chemie Ag Verfahren zur kontinuierlichen Hydrosilylierung

Also Published As

Publication number Publication date
KR20090037459A (ko) 2009-04-15
CA2660406A1 (en) 2008-02-14
JP2010500312A (ja) 2010-01-07
WO2008017554A1 (de) 2008-02-14
US20100179340A1 (en) 2010-07-15
DE102007023760A1 (de) 2008-02-14
EP2049242A1 (de) 2009-04-22
BRPI0715805A2 (pt) 2013-03-05

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