NO130671B - - Google Patents
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- Publication number
- NO130671B NO130671B NO40072A NO40072A NO130671B NO 130671 B NO130671 B NO 130671B NO 40072 A NO40072 A NO 40072A NO 40072 A NO40072 A NO 40072A NO 130671 B NO130671 B NO 130671B
- Authority
- NO
- Norway
- Prior art keywords
- thiadiazole
- water
- nitroph
- uryl
- recrystallization
- Prior art date
Links
- 125000003277 amino group Chemical group 0.000 claims description 8
- 125000001424 substituent group Chemical group 0.000 claims description 6
- XWUHTDIIQSYUDH-FPYGCLRLSA-N [(e)-(5-nitrofuran-2-yl)methylideneamino]thiourea Chemical compound NC(=S)N\N=C\C1=CC=C([N+]([O-])=O)O1 XWUHTDIIQSYUDH-FPYGCLRLSA-N 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 239000007800 oxidant agent Substances 0.000 claims description 4
- 125000002723 alicyclic group Chemical group 0.000 claims description 3
- 125000000623 heterocyclic group Chemical group 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- FXPGPQYXWANAFW-UHFFFAOYSA-N NC1=C(OC=C1)C=1N=NSC1[N+](=O)[O-] Chemical class NC1=C(OC=C1)C=1N=NSC1[N+](=O)[O-] FXPGPQYXWANAFW-UHFFFAOYSA-N 0.000 claims description 2
- 125000003342 alkenyl group Chemical group 0.000 claims description 2
- 125000004183 alkoxy alkyl group Chemical group 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 2
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 125000004181 carboxyalkyl group Chemical group 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 24
- -1 alkyl radicals Chemical class 0.000 description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 18
- MBIZXFATKUQOOA-UHFFFAOYSA-N 1,3,4-thiadiazole Chemical compound C1=NN=CS1 MBIZXFATKUQOOA-UHFFFAOYSA-N 0.000 description 14
- 150000001875 compounds Chemical class 0.000 description 14
- 238000001953 recrystallisation Methods 0.000 description 14
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 10
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 10
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 9
- 239000013078 crystal Substances 0.000 description 9
- SVYOXGBINYWSDQ-UHFFFAOYSA-N 1,4-dioxane;ethanol Chemical compound CCO.C1COCCO1 SVYOXGBINYWSDQ-UHFFFAOYSA-N 0.000 description 5
- 239000012043 crude product Substances 0.000 description 5
- 238000002844 melting Methods 0.000 description 5
- 230000008018 melting Effects 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 230000003385 bacteriostatic effect Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- SXZZHGJWUBJKHH-UHFFFAOYSA-N 2-Amino-5-(5-nitro-2-furyl)-1,3,4-thiadiazole Chemical class S1C(N)=NN=C1C1=CC=C([N+]([O-])=O)O1 SXZZHGJWUBJKHH-UHFFFAOYSA-N 0.000 description 2
- FPFSGDXIBUDDKZ-UHFFFAOYSA-N 3-decyl-2-hydroxycyclopent-2-en-1-one Chemical compound CCCCCCCCCCC1=C(O)C(=O)CC1 FPFSGDXIBUDDKZ-UHFFFAOYSA-N 0.000 description 2
- FWSYYTQNROEZQP-UHFFFAOYSA-N 5-(5-nitrofuran-2-yl)-n-phenyl-1,3,4-thiadiazol-2-amine Chemical compound O1C([N+](=O)[O-])=CC=C1C(S1)=NN=C1NC1=CC=CC=C1 FWSYYTQNROEZQP-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000009036 growth inhibition Effects 0.000 description 2
- VCJMYUPGQJHHFU-UHFFFAOYSA-N iron(3+);trinitrate Chemical compound [Fe+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VCJMYUPGQJHHFU-UHFFFAOYSA-N 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- ZJZVRRACFFNDCQ-UHFFFAOYSA-N 1-(2-methylpropyl)-3-[(5-nitrofuran-2-yl)methylideneamino]thiourea Chemical compound CC(C)CNC(=S)NN=CC1=CC=C([N+]([O-])=O)O1 ZJZVRRACFFNDCQ-UHFFFAOYSA-N 0.000 description 1
- UIEWYHUUSJLKRI-UHFFFAOYSA-N 1-ethyl-3-[(5-nitrofuran-2-yl)methylideneamino]thiourea Chemical compound CCNC(=S)NN=CC1=CC=C([N+]([O-])=O)O1 UIEWYHUUSJLKRI-UHFFFAOYSA-N 0.000 description 1
- UIJPWDSKPZLJAN-UHFFFAOYSA-N 2-(1,4-dioxan-2-yl)ethanol Chemical compound OCCC1COCCO1 UIJPWDSKPZLJAN-UHFFFAOYSA-N 0.000 description 1
- 125000000094 2-phenylethyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- OEBUQQJTQXRLSZ-UHFFFAOYSA-N 4-(furan-2-yl)-5-nitrothiadiazole Chemical class [N+](=O)([O-])C1=C(N=NS1)C=1OC=CC=1 OEBUQQJTQXRLSZ-UHFFFAOYSA-N 0.000 description 1
- 241000586542 Aonidiella citrina Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241001630118 Chrysomphalus bifasciculatus Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 1
- 239000005955 Ferric phosphate Substances 0.000 description 1
- 241000606768 Haemophilus influenzae Species 0.000 description 1
- ISTLEQBEBWKYAM-UHFFFAOYSA-N N-benzyl-5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-amine Chemical compound O1C([N+](=O)[O-])=CC=C1C(S1)=NN=C1NCC1=CC=CC=C1 ISTLEQBEBWKYAM-UHFFFAOYSA-N 0.000 description 1
- 241000607142 Salmonella Species 0.000 description 1
- 241000607768 Shigella Species 0.000 description 1
- 241000224527 Trichomonas vaginalis Species 0.000 description 1
- 241000223238 Trichophyton Species 0.000 description 1
- UYHCMAZIKNVDSX-UXBLZVDNSA-N [(e)-benzylideneamino]thiourea Chemical compound NC(=S)N\N=C\C1=CC=CC=C1 UYHCMAZIKNVDSX-UXBLZVDNSA-N 0.000 description 1
- FRHBOQMZUOWXQL-UHFFFAOYSA-L ammonium ferric citrate Chemical compound [NH4+].[Fe+3].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O FRHBOQMZUOWXQL-UHFFFAOYSA-L 0.000 description 1
- 150000005840 aryl radicals Chemical class 0.000 description 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- 239000012888 bovine serum Substances 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 229960001760 dimethyl sulfoxide Drugs 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 229960004642 ferric ammonium citrate Drugs 0.000 description 1
- VEPSWGHMGZQCIN-UHFFFAOYSA-H ferric oxalate Chemical compound [Fe+3].[Fe+3].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O VEPSWGHMGZQCIN-UHFFFAOYSA-H 0.000 description 1
- 229940032958 ferric phosphate Drugs 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 230000009422 growth inhibiting effect Effects 0.000 description 1
- 229940047650 haemophilus influenzae Drugs 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 235000000011 iron ammonium citrate Nutrition 0.000 description 1
- 239000004313 iron ammonium citrate Substances 0.000 description 1
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical compound [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 description 1
- RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 description 1
- PVFSDGKDKFSOTB-UHFFFAOYSA-K iron(3+);triacetate Chemical compound [Fe+3].CC([O-])=O.CC([O-])=O.CC([O-])=O PVFSDGKDKFSOTB-UHFFFAOYSA-K 0.000 description 1
- ITAUHKJMPRCVIH-UHFFFAOYSA-K iron(3+);tribenzoate Chemical compound [Fe+3].[O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1 ITAUHKJMPRCVIH-UHFFFAOYSA-K 0.000 description 1
- 229910000399 iron(III) phosphate Inorganic materials 0.000 description 1
- 229910000360 iron(III) sulfate Inorganic materials 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- IAIWVQXQOWNYOU-FPYGCLRLSA-N nitrofural Chemical compound NC(=O)N\N=C\C1=CC=C([N+]([O-])=O)O1 IAIWVQXQOWNYOU-FPYGCLRLSA-N 0.000 description 1
- 229960001907 nitrofurazone Drugs 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 125000004076 pyridyl group Chemical group 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 description 1
- MKBNNYRMBCFUSH-UHFFFAOYSA-J sodium;iron(3+);oxalate Chemical compound [Na+].[Fe+3].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O MKBNNYRMBCFUSH-UHFFFAOYSA-J 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 125000000547 substituted alkyl group Chemical group 0.000 description 1
- 150000004867 thiadiazoles Chemical group 0.000 description 1
- DCXPBOFGQPCWJY-UHFFFAOYSA-N trisodium;iron(3+);hexacyanide Chemical compound [Na+].[Na+].[Na+].[Fe+3].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] DCXPBOFGQPCWJY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/16—Fractionating columns in which vapour bubbles through liquid
- B01D3/18—Fractionating columns in which vapour bubbles through liquid with horizontal bubble plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
- B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
- B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
- B41J2/01—Ink jet
- B41J2/135—Nozzles
- B41J2/14—Structure thereof only for on-demand ink jet heads
- B41J2002/14403—Structure thereof only for on-demand ink jet heads including a filter
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treating Waste Gases (AREA)
- Gas Separation By Absorption (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Separation Of Particles Using Liquids (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Nitrogen- Or Sulfur-Containing Heterocyclic Ring Compounds With Rings Of Six Or More Members (AREA)
- Plural Heterocyclic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB458971 | 1971-02-12 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO130671B true NO130671B (cg-RX-API-DMAC7.html) | 1974-10-14 |
| NO130671C NO130671C (cg-RX-API-DMAC7.html) | 1975-01-22 |
Family
ID=9780023
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO40072A NO130671C (cg-RX-API-DMAC7.html) | 1971-02-12 | 1972-02-11 |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS5257158Y2 (cg-RX-API-DMAC7.html) |
| DE (1) | DE2206603C3 (cg-RX-API-DMAC7.html) |
| ES (1) | ES399628A1 (cg-RX-API-DMAC7.html) |
| FR (1) | FR2125400B1 (cg-RX-API-DMAC7.html) |
| GB (1) | GB1333877A (cg-RX-API-DMAC7.html) |
| NO (1) | NO130671C (cg-RX-API-DMAC7.html) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4214880A (en) | 1977-05-03 | 1980-07-29 | Kamphorst Hendrik A | Liquid seal system, e.g. for a flare stack |
| DE2928598C2 (de) * | 1979-07-14 | 1984-01-19 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Reinigung fluoridhaltiger Abfallschwefelsäure |
| CA1320431C (en) * | 1988-08-19 | 1993-07-20 | James O. Nye | Distillation tray |
| ES2059233B1 (es) * | 1992-04-22 | 1997-07-16 | Mendez Fernandez Manuel Ismael | Instalacion de filtro para depuracion de gases emitidos a la atmosfera por explotaciones industriales. |
| MA33456B1 (fr) * | 2009-06-25 | 2012-07-03 | Enviroresolutions Inc | Appareil laveur de gaz amélioré et procédé |
| CN114225617B (zh) * | 2021-12-17 | 2023-09-08 | 镇海石化工程股份有限公司 | 高凝点重油油气处理方法 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1363916A (fr) * | 1962-02-28 | 1964-06-19 | Julius Montz | Colonne d'échange de chaleur et de matière |
-
1971
- 1971-02-12 GB GB1333877D patent/GB1333877A/en not_active Expired
-
1972
- 1972-02-10 ES ES399628A patent/ES399628A1/es not_active Expired
- 1972-02-11 FR FR7204688A patent/FR2125400B1/fr not_active Expired
- 1972-02-11 DE DE19722206603 patent/DE2206603C3/de not_active Expired
- 1972-02-11 NO NO40072A patent/NO130671C/no unknown
-
1977
- 1977-02-02 JP JP1154877U patent/JPS5257158Y2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2206603B2 (de) | 1980-04-24 |
| JPS52106449U (cg-RX-API-DMAC7.html) | 1977-08-13 |
| JPS5257158Y2 (cg-RX-API-DMAC7.html) | 1977-12-24 |
| FR2125400A1 (cg-RX-API-DMAC7.html) | 1972-09-29 |
| FR2125400B1 (cg-RX-API-DMAC7.html) | 1976-06-18 |
| ES399628A1 (es) | 1975-07-01 |
| NO130671C (cg-RX-API-DMAC7.html) | 1975-01-22 |
| DE2206603C3 (de) | 1980-12-11 |
| GB1333877A (en) | 1973-10-17 |
| DE2206603A1 (de) | 1972-09-07 |
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