NO128820B - - Google Patents
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- Publication number
- NO128820B NO128820B NO487969A NO487969A NO128820B NO 128820 B NO128820 B NO 128820B NO 487969 A NO487969 A NO 487969A NO 487969 A NO487969 A NO 487969A NO 128820 B NO128820 B NO 128820B
- Authority
- NO
- Norway
- Prior art keywords
- reaction
- chlorine
- chloride
- carbon
- carbon disulphide
- Prior art date
Links
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 claims description 61
- 238000006243 chemical reaction Methods 0.000 claims description 42
- 238000000034 method Methods 0.000 claims description 31
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 30
- RYFZYYUIAZYQLC-UHFFFAOYSA-N perchloromethyl mercaptan Chemical compound ClSC(Cl)(Cl)Cl RYFZYYUIAZYQLC-UHFFFAOYSA-N 0.000 claims description 27
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 24
- 229910052801 chlorine Inorganic materials 0.000 claims description 24
- 239000000460 chlorine Substances 0.000 claims description 24
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000005660 chlorination reaction Methods 0.000 description 19
- PXJJSXABGXMUSU-UHFFFAOYSA-N disulfur dichloride Chemical compound ClSSCl PXJJSXABGXMUSU-UHFFFAOYSA-N 0.000 description 17
- FWMUJAIKEJWSSY-UHFFFAOYSA-N sulfur dichloride Chemical compound ClSCl FWMUJAIKEJWSSY-UHFFFAOYSA-N 0.000 description 15
- 239000000203 mixture Substances 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 11
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 10
- 239000006227 byproduct Substances 0.000 description 9
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 8
- 238000009835 boiling Methods 0.000 description 8
- 238000000926 separation method Methods 0.000 description 8
- 238000004821 distillation Methods 0.000 description 7
- 239000011541 reaction mixture Substances 0.000 description 5
- 230000007306 turnover Effects 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 229910052740 iodine Inorganic materials 0.000 description 3
- 239000011630 iodine Substances 0.000 description 3
- 238000001256 steam distillation Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical class OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- KOLWTTZDSQSSBF-UHFFFAOYSA-N [Cl].C(=S)=S Chemical compound [Cl].C(=S)=S KOLWTTZDSQSSBF-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- -1 aliphatic ethers Chemical class 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- MAHNFPMIPQKPPI-UHFFFAOYSA-N disulfur Chemical compound S=S MAHNFPMIPQKPPI-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- ZWZVWGITAAIFPS-UHFFFAOYSA-N thiophosgene Chemical compound ClC(Cl)=S ZWZVWGITAAIFPS-UHFFFAOYSA-N 0.000 description 1
- DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical compound [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C313/00—Sulfinic acids; Sulfenic acids; Halides, esters or anhydrides thereof; Amides of sulfinic or sulfenic acids, i.e. compounds having singly-bound oxygen atoms of sulfinic or sulfenic groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C313/08—Sulfenic acids; Derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691900659 DE1900659C3 (de) | 1969-01-08 | 1969-01-08 | Verfahren zur Herstellung von Tri chlormethan su lfenylchlorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO128820B true NO128820B (enrdf_load_stackoverflow) | 1974-01-14 |
Family
ID=5721887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO487969A NO128820B (enrdf_load_stackoverflow) | 1969-01-08 | 1969-12-10 |
Country Status (19)
-
1969
- 1969-01-08 DE DE19691900659 patent/DE1900659C3/de not_active Expired
- 1969-12-10 NO NO487969A patent/NO128820B/no unknown
- 1969-12-11 SE SE1713069A patent/SE351629B/xx unknown
- 1969-12-12 DK DK658169A patent/DK125393B/da unknown
- 1969-12-12 GB GB6072269A patent/GB1244898A/en not_active Expired
- 1969-12-17 FI FI365969A patent/FI50118C/fi active
- 1969-12-19 CH CH1890469A patent/CH517716A/de not_active IP Right Cessation
- 1969-12-20 RO RO6192769A patent/RO58248A/ro unknown
- 1969-12-22 YU YU320269A patent/YU32476B/xx unknown
- 1969-12-25 BG BG013618A patent/BG17555A3/xx unknown
- 1969-12-30 IE IE173069A patent/IE33907B1/xx unknown
- 1969-12-31 BE BE743941D patent/BE743941A/xx unknown
-
1970
- 1970-01-06 LU LU60140D patent/LU60140A1/xx unknown
- 1970-01-07 FR FR7000421A patent/FR2031084A5/fr not_active Expired
- 1970-01-07 NL NL7000150A patent/NL7000150A/xx not_active Application Discontinuation
- 1970-01-07 PL PL13803570A patent/PL80428B1/xx unknown
- 1970-01-07 ES ES375204A patent/ES375204A1/es not_active Expired
- 1970-01-08 AT AT15170A patent/AT291957B/de not_active IP Right Cessation
- 1970-01-08 CS CS15770A patent/CS157080B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| LU60140A1 (enrdf_load_stackoverflow) | 1970-03-06 |
| FR2031084A5 (enrdf_load_stackoverflow) | 1970-11-13 |
| AT291957B (de) | 1971-08-10 |
| IE33907B1 (en) | 1974-12-11 |
| YU32476B (en) | 1974-12-31 |
| CS157080B2 (enrdf_load_stackoverflow) | 1974-08-23 |
| DK125393B (da) | 1973-02-12 |
| PL80428B1 (enrdf_load_stackoverflow) | 1975-08-30 |
| NL7000150A (enrdf_load_stackoverflow) | 1970-07-10 |
| DE1900659B2 (de) | 1973-09-06 |
| DE1900659A1 (de) | 1970-09-24 |
| YU320269A (en) | 1974-06-30 |
| FI50118B (enrdf_load_stackoverflow) | 1975-09-01 |
| BG17555A3 (bg) | 1973-11-10 |
| BE743941A (enrdf_load_stackoverflow) | 1970-05-28 |
| FI50118C (fi) | 1975-12-10 |
| RO58248A (enrdf_load_stackoverflow) | 1975-09-15 |
| ES375204A1 (es) | 1972-03-01 |
| SE351629B (enrdf_load_stackoverflow) | 1972-12-04 |
| GB1244898A (en) | 1971-09-02 |
| CH517716A (de) | 1972-01-15 |
| DE1900659C3 (de) | 1974-04-04 |
| IE33907L (en) | 1970-07-08 |
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