IE33907L - Preparation of trichloromethane sulphenyl chloride - Google Patents
Preparation of trichloromethane sulphenyl chlorideInfo
- Publication number
- IE33907L IE33907L IE173069A IE173069A IE33907L IE 33907 L IE33907 L IE 33907L IE 173069 A IE173069 A IE 173069A IE 173069 A IE173069 A IE 173069A IE 33907 L IE33907 L IE 33907L
- Authority
- IE
- Ireland
- Prior art keywords
- chloride
- sulphur
- reaction
- charcoal
- preparation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C313/00—Sulfinic acids; Sulfenic acids; Halides, esters or anhydrides thereof; Amides of sulfinic or sulfenic acids, i.e. compounds having singly-bound oxygen atoms of sulfinic or sulfenic groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C313/08—Sulfenic acids; Derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
1,244,898. Sulphur chloride; sulphur di- Chloride. GLANZSTOFF A.G. 12 Dec., 1969 [8 Jan., 1969], No. 60722/69. Heading C1A. [Also in Division C2] Sulphur chloride and sulphur dichloride are obtained in the preparation of trichloromethyl sulphenyl chloride by reaction of carbon disulphide with chlorine in the presence of active charcoal. The charcoal has preferably been treated to remove iron impurities, and desirably has high abrasion resistance, a particle size of 2À5 to 4 mm. and a surface area of 1200 to 1500 m.<SP>2</SP>/g. Reaction temperatures of -5 to 100 C. are specified. Reaction may be continuous or batchwise over granular charcoal packed in a reaction column containing a cooling coil, the reagents being introduced either in countercurrent or together at the top of the column. The chlorination mixture may be separated by distillation into a low boiling fraction containing sulphur dichloride and carbon tetrachloride, and a high boiling fraction containing trichloromethyl sulphenyl chloride and sulphur chloride, which may be further purified by steam distillation.
[GB1244898A]
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691900659 DE1900659C3 (en) | 1969-01-08 | 1969-01-08 | Process for the preparation of trichloromethane sulfenyl chloride |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IE33907L true IE33907L (en) | 1970-07-08 |
| IE33907B1 IE33907B1 (en) | 1974-12-11 |
Family
ID=5721887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IE173069A IE33907B1 (en) | 1969-01-08 | 1969-12-30 | Process for the preparation of trichloromethanesulphenyl chloride |
Country Status (19)
| Country | Link |
|---|---|
| AT (1) | AT291957B (en) |
| BE (1) | BE743941A (en) |
| BG (1) | BG17555A3 (en) |
| CH (1) | CH517716A (en) |
| CS (1) | CS157080B2 (en) |
| DE (1) | DE1900659C3 (en) |
| DK (1) | DK125393B (en) |
| ES (1) | ES375204A1 (en) |
| FI (1) | FI50118C (en) |
| FR (1) | FR2031084A5 (en) |
| GB (1) | GB1244898A (en) |
| IE (1) | IE33907B1 (en) |
| LU (1) | LU60140A1 (en) |
| NL (1) | NL7000150A (en) |
| NO (1) | NO128820B (en) |
| PL (1) | PL80428B1 (en) |
| RO (1) | RO58248A (en) |
| SE (1) | SE351629B (en) |
| YU (1) | YU32476B (en) |
-
1969
- 1969-01-08 DE DE19691900659 patent/DE1900659C3/en not_active Expired
- 1969-12-10 NO NO487969A patent/NO128820B/no unknown
- 1969-12-11 SE SE1713069A patent/SE351629B/xx unknown
- 1969-12-12 GB GB6072269A patent/GB1244898A/en not_active Expired
- 1969-12-12 DK DK658169A patent/DK125393B/en unknown
- 1969-12-17 FI FI365969A patent/FI50118C/en active
- 1969-12-19 CH CH1890469A patent/CH517716A/en not_active IP Right Cessation
- 1969-12-20 RO RO6192769A patent/RO58248A/ro unknown
- 1969-12-22 YU YU320269A patent/YU32476B/en unknown
- 1969-12-25 BG BG013618A patent/BG17555A3/en unknown
- 1969-12-30 IE IE173069A patent/IE33907B1/en unknown
- 1969-12-31 BE BE743941D patent/BE743941A/xx unknown
-
1970
- 1970-01-06 LU LU60140D patent/LU60140A1/xx unknown
- 1970-01-07 PL PL13803570A patent/PL80428B1/xx unknown
- 1970-01-07 NL NL7000150A patent/NL7000150A/xx not_active Application Discontinuation
- 1970-01-07 ES ES375204A patent/ES375204A1/en not_active Expired
- 1970-01-07 FR FR7000421A patent/FR2031084A5/fr not_active Expired
- 1970-01-08 AT AT15170A patent/AT291957B/en not_active IP Right Cessation
- 1970-01-08 CS CS15770A patent/CS157080B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR2031084A5 (en) | 1970-11-13 |
| DE1900659A1 (en) | 1970-09-24 |
| FI50118C (en) | 1975-12-10 |
| NO128820B (en) | 1974-01-14 |
| YU32476B (en) | 1974-12-31 |
| YU320269A (en) | 1974-06-30 |
| CS157080B2 (en) | 1974-08-23 |
| BG17555A3 (en) | 1973-11-10 |
| RO58248A (en) | 1975-09-15 |
| LU60140A1 (en) | 1970-03-06 |
| NL7000150A (en) | 1970-07-10 |
| CH517716A (en) | 1972-01-15 |
| AT291957B (en) | 1971-08-10 |
| DK125393B (en) | 1973-02-12 |
| BE743941A (en) | 1970-05-28 |
| FI50118B (en) | 1975-09-01 |
| DE1900659B2 (en) | 1973-09-06 |
| DE1900659C3 (en) | 1974-04-04 |
| ES375204A1 (en) | 1972-03-01 |
| IE33907B1 (en) | 1974-12-11 |
| GB1244898A (en) | 1971-09-02 |
| PL80428B1 (en) | 1975-08-30 |
| SE351629B (en) | 1972-12-04 |
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