MX2021012680A - Metodos para la produccion de monohidrato de l-glufosinato de amonio cristalino. - Google Patents

Metodos para la produccion de monohidrato de l-glufosinato de amonio cristalino.

Info

Publication number
MX2021012680A
MX2021012680A MX2021012680A MX2021012680A MX2021012680A MX 2021012680 A MX2021012680 A MX 2021012680A MX 2021012680 A MX2021012680 A MX 2021012680A MX 2021012680 A MX2021012680 A MX 2021012680A MX 2021012680 A MX2021012680 A MX 2021012680A
Authority
MX
Mexico
Prior art keywords
glufosinate ammonium
methods
glufosinate
monohydrate
ammonium monohydrate
Prior art date
Application number
MX2021012680A
Other languages
English (en)
Inventor
Matthew Richard Oberholzer
Brian Michael Green
Rachel Melissa Witek
Nadejda Pavlova
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2021012680A publication Critical patent/MX2021012680A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N9/00—Enzymes; Proenzymes; Compositions thereof; Processes for preparing, activating, inhibiting, separating or purifying enzymes
    • C12N9/0004—Oxidoreductases (1.)
    • C12N9/0012—Oxidoreductases (1.) acting on nitrogen containing compounds as donors (1.4, 1.5, 1.6, 1.7)
    • C12N9/0014—Oxidoreductases (1.) acting on nitrogen containing compounds as donors (1.4, 1.5, 1.6, 1.7) acting on the CH-NH2 group of donors (1.4)
    • C12N9/0022—Oxidoreductases (1.) acting on nitrogen containing compounds as donors (1.4, 1.5, 1.6, 1.7) acting on the CH-NH2 group of donors (1.4) with oxygen as acceptor (1.4.3)
    • C12N9/0024—D-Amino acid oxidase (1.4.3.3)
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12Y—ENZYMES
    • C12Y104/00—Oxidoreductases acting on the CH-NH2 group of donors (1.4)
    • C12Y104/03—Oxidoreductases acting on the CH-NH2 group of donors (1.4) with oxygen as acceptor (1.4.3)
    • C12Y104/03003—D-Amino-acid oxidase (1.4.3.3)
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N9/00—Enzymes; Proenzymes; Compositions thereof; Processes for preparing, activating, inhibiting, separating or purifying enzymes
    • C12N9/10—Transferases (2.)
    • C12N9/1096—Transferases (2.) transferring nitrogenous groups (2.6)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Genetics & Genomics (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Wood Science & Technology (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • General Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Biomedical Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Enzymes And Modification Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Saccharide Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

Se divulgan métodos para preparar monohidrato de L-glufosinato de amonio cristalino. Los métodos incluyen formar una mezcla que comprende agua, un solvente orgánico miscible en agua, hidróxido de amonio y un material de inicio de glufosinato que contiene L-glufosinato de amonio y D-glufosinato de amonio. El monohidrato de L-glufosinato de amonio se cristaliza y se separa de la mezcla, lo que proporciona la Forma B de monohidrato de L-glufosinato de amonio. También se describen composiciones y métodos que emplean el monohidrato de L-glufosinato de amonio cristalino.
MX2021012680A 2019-04-16 2020-04-15 Metodos para la produccion de monohidrato de l-glufosinato de amonio cristalino. MX2021012680A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201962834675P 2019-04-16 2019-04-16
US202062978005P 2020-02-18 2020-02-18
PCT/US2020/028191 WO2020214631A1 (en) 2019-04-16 2020-04-15 Methods for producing crystalline l-glufosinate ammonium monohydrate

Publications (1)

Publication Number Publication Date
MX2021012680A true MX2021012680A (es) 2021-11-12

Family

ID=70554206

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2021012680A MX2021012680A (es) 2019-04-16 2020-04-15 Metodos para la produccion de monohidrato de l-glufosinato de amonio cristalino.

Country Status (10)

Country Link
US (1) US20220177499A1 (es)
EP (1) EP3956336A1 (es)
JP (1) JP2022529428A (es)
KR (1) KR20210151952A (es)
CN (1) CN113767107A (es)
BR (1) BR112021018995A2 (es)
CA (1) CA3133296A1 (es)
IL (1) IL287204A (es)
MX (1) MX2021012680A (es)
WO (1) WO2020214631A1 (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2019018406A1 (en) 2017-07-18 2019-01-24 Agrimetis, Llc METHODS OF PURIFYING L-GLUFOSINATE
BR112022003519A2 (pt) * 2020-07-31 2023-02-28 Upl Ltd Forma cristalina de sal de l-glufosinato de amônio e processo para a sua produção
US11555046B2 (en) 2020-07-31 2023-01-17 Upl Ltd Crystalline form of L-glufosinate ammonium salt and process for production thereof
CN112760353A (zh) * 2021-03-16 2021-05-07 北京鑫佰利科技发展有限公司 一种l-草铵膦的生产方法
CN114805433B (zh) * 2021-05-13 2023-11-28 永农生物科学有限公司 不含结晶水的l-草铵膦铵盐晶体形式及固体粉末
CN113480573B (zh) * 2021-06-21 2023-08-15 上海七洲紫岳生物科技有限公司 L-草铵膦的晶型及其制备方法和应用
WO2024158883A1 (en) * 2023-01-25 2024-08-02 Vulpes Agricultural Corp. Optically active amino acid salts and method for their preparation

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DE2839087A1 (de) 1978-09-08 1980-03-20 Hoechst Ag Herbizide mittel
JPS59219297A (ja) 1983-05-27 1984-12-10 Meiji Seika Kaisha Ltd 光学活性な〔（３−アミノ−３−カルボキシ）プロピル−１〕−ホスフイン酸誘導体の製造法
GB8421964D0 (en) 1984-08-30 1984-10-03 Beecham Group Plc Chemical process
US5258358A (en) 1991-04-27 1993-11-02 Hoechst Aktiengesellschaft Liquid herbicidal compositions containing glufosinate and an alkyl polyglycoside
IL104056A (en) 1991-12-13 1997-02-18 Hoechst Ag Process for the preparation of L-phosphinothricin and its derivatives
DE4407197A1 (de) 1994-03-04 1995-09-07 Hoechst Schering Agrevo Gmbh Verfahren zur Herstellung von /L/-Homoalanin-4-yl-(methyl)phosphinsäure und deren Salze durch Racematspaltung
EP1917857A1 (en) * 2002-07-24 2008-05-07 Basf Se Synergistically acting herbicidal mixtures
PL1605762T3 (pl) * 2003-03-13 2007-01-31 Basf Se Mieszaniny chwastobójcze działające synergicznie
JP4970249B2 (ja) 2005-03-29 2012-07-04 Ｍｅｉｊｉ Ｓｅｉｋａファルマ株式会社 Ｌ−２−アミノ−４−（ヒドロキシメチルホスフィニル）−ブタン酸の製造法
TWI412533B (zh) 2006-09-04 2013-10-21 Meiji Seika Pharma Co Ltd 光學活性胺基氧膦基丁酸類之製造方法
WO2008035687A1 (fr) 2006-09-20 2008-03-27 Meiji Seika Kaisha Ltd. PROCÉDÉ DE FABRICATION D'UN ACIDE α-AMINÉ CONTENANT DU PHOSPHORE ET INTERMÉDIAIRE DE FABRICATION
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WO2019018406A1 (en) 2017-07-18 2019-01-24 Agrimetis, Llc METHODS OF PURIFYING L-GLUFOSINATE

Also Published As

Publication number Publication date
BR112021018995A2 (pt) 2021-11-30
CA3133296A1 (en) 2020-10-22
CN113767107A (zh) 2021-12-07
JP2022529428A (ja) 2022-06-22
EP3956336A1 (en) 2022-02-23
IL287204A (en) 2021-12-01
WO2020214631A1 (en) 2020-10-22
US20220177499A1 (en) 2022-06-09
KR20210151952A (ko) 2021-12-14

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