MX2018000198A - Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida. - Google Patents

Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida.

Info

Publication number
MX2018000198A
MX2018000198A MX2018000198A MX2018000198A MX2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A
Authority
MX
Mexico
Prior art keywords
reaction mixture
acid reaction
furfural derivative
neutralizing
chemical formula
Prior art date
Application number
MX2018000198A
Other languages
English (en)
Inventor
Johannes Maria Gruter Gerardus
Sofia Vagueiro De Sousa Dias Ana
Maria Franciscus Sijben Johannes
Mazoyer Etienne
Original Assignee
Synvina C V
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Synvina C V filed Critical Synvina C V
Publication of MX2018000198A publication Critical patent/MX2018000198A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Un derivado de furfural que tiene la fórmula química (1), en donde R representa hidrógeno, un grupo alquilo o un grupo acilo, se prepara en un procedimiento, tal procedimiento comprende hacer reaccionar un material de partida que contiene fructosa y/o glucosa con un compuesto que contiene un grupo hidroxilo líquido de fórmula R-OH en presencia de un catalizador ácido a una temperatura de reacción en el intervalo de 150 a 300 °C para producir una mezcla de reacción ácida primaria que comprende el derivado de furfural de fórmula química (1); separar parte del compuesto que contiene un grupo hidroxilo líquido de la mezcla de reacción ácida primaria para producir una mezcla de reacción ácida secundaria; neutralizar la mezcla de reacción ácida secundaria a un valor de pH de al menos 3 para obtener una mezcla de reacción neutralizada; y purificar la mezcla de reacción neutralizada para recuperar el derivado de furfural de la fórmula química (1).
MX2018000198A 2015-07-01 2016-07-01 Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida. MX2018000198A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL2015066 2015-07-01
PCT/NL2016/050470 WO2017003294A1 (en) 2015-07-01 2016-07-01 Process for the preparation of a furfural derivative comprising neutralizing an acid reaction mixture

Publications (1)

Publication Number Publication Date
MX2018000198A true MX2018000198A (es) 2018-04-11

Family

ID=53783874

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2018000198A MX2018000198A (es) 2015-07-01 2016-07-01 Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida.

Country Status (8)

Country Link
US (1) US10266508B2 (es)
EP (1) EP3317262B1 (es)
CN (1) CN107848996B (es)
BR (1) BR112017028433B1 (es)
CA (1) CA2990588C (es)
ES (1) ES2806988T3 (es)
MX (1) MX2018000198A (es)
WO (1) WO2017003294A1 (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107912039B (zh) * 2015-07-01 2021-11-05 福兰尼克斯科技公司 用于制备糠醛衍生物的方法
WO2023066577A1 (en) 2021-10-21 2023-04-27 Furanix Technologies B.V. Process for the preparation of a furfural derivative

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3290263A (en) * 1962-08-02 1966-12-06 Colonial Sugar Refining Co Process of reacting sugars with reagents wherein the sugar is dissolved in monohydric alcohols containing grouping
DE3601281A1 (de) * 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
US7317116B2 (en) * 2004-12-10 2008-01-08 Archer-Daniels-Midland-Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
EP1834950A1 (en) * 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of 5-alkoxymethylfurfural ethers and their use
EP2050742B1 (en) * 2006-03-10 2010-07-07 Furanix Technologies B.V Use of an organic acid esters of 5-hydroxymethylfurfural
WO2009030506A2 (en) 2007-09-07 2009-03-12 Furanix Technologies B.V. Hydroxymethylfurfural ethers from sugars or hmf and branched alcohols
NL2005928C2 (en) * 2010-12-28 2012-07-02 Furanix Technologies Bv Process for the conversion of a carbohydrate-containing feedstock.
CN103857664B (zh) * 2011-09-23 2016-08-24 新加坡科技研究局 由碳水化合物制备5-羟甲基糠醛的方法
CN103159707A (zh) 2011-12-09 2013-06-19 中国科学院大连化学物理研究所 一种生物质催化转化制备呋喃衍生物的方法
WO2016207025A1 (de) * 2015-06-24 2016-12-29 Basf Se Verfahren zum herstellen und abtrennen von hmf
CN107912039B (zh) * 2015-07-01 2021-11-05 福兰尼克斯科技公司 用于制备糠醛衍生物的方法

Also Published As

Publication number Publication date
EP3317262B1 (en) 2020-04-22
BR112017028433B1 (pt) 2022-02-08
US20180186761A1 (en) 2018-07-05
CN107848996B (zh) 2021-07-27
BR112017028433A2 (pt) 2018-08-28
CA2990588A1 (en) 2017-01-05
WO2017003294A1 (en) 2017-01-05
US10266508B2 (en) 2019-04-23
CN107848996A (zh) 2018-03-27
EP3317262A1 (en) 2018-05-09
CA2990588C (en) 2020-04-14
ES2806988T3 (es) 2021-02-19

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