MX2015007372A - Proceso mejorado para la preparacion de [n-ciano-s-[1-(piridin-3-i l) etil]-s-metilsulfiliminas. - Google Patents

Proceso mejorado para la preparacion de [n-ciano-s-[1-(piridin-3-i l) etil]-s-metilsulfiliminas.

Info

Publication number
MX2015007372A
MX2015007372A MX2015007372A MX2015007372A MX2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A
Authority
MX
Mexico
Prior art keywords
cyano
methylsulfilimines
pyridin
ethyl
preparation
Prior art date
Application number
MX2015007372A
Other languages
English (en)
Inventor
Michael A Gonzalez
Chad Meece
Xiaoyun Chen
Florin Dan
Original Assignee
Dow Agrosciences Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Agrosciences Llc filed Critical Dow Agrosciences Llc
Publication of MX2015007372A publication Critical patent/MX2015007372A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/57—Nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/28—Radicals substituted by singly-bound oxygen or sulphur atoms
    • C07D213/32—Sulfur atoms
    • C07D213/34—Sulfur atoms to which a second hetero atom is attached

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyridine Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Las sulfiliminas ciano-substituidas se producen de forma eficaz y con alto rendimiento a partir de los correspondientes sulfuros, cianamida e hipoclorito mediante la adición del sulfuro a una solución de la cianamida e hipoclorito en presencia de un solvente de nitrilo mientras mantiene el pH de aproximadamente 8 a aproximadamente 12.
MX2015007372A 2012-12-11 2013-12-10 Proceso mejorado para la preparacion de [n-ciano-s-[1-(piridin-3-i l) etil]-s-metilsulfiliminas. MX2015007372A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201261735573P 2012-12-11 2012-12-11
US201261735612P 2012-12-11 2012-12-11
PCT/US2013/074006 WO2014093276A1 (en) 2012-12-11 2013-12-10 Improved process for the preparation of|n-cyano-s-[1 -(pyridin-3-yl)ethyl]-s-methylsulfilimines

Publications (1)

Publication Number Publication Date
MX2015007372A true MX2015007372A (es) 2015-09-23

Family

ID=49877060

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2015007372A MX2015007372A (es) 2012-12-11 2013-12-10 Proceso mejorado para la preparacion de [n-ciano-s-[1-(piridin-3-i l) etil]-s-metilsulfiliminas.

Country Status (14)

Country Link
US (2) US20140163236A1 (es)
EP (1) EP2931706A1 (es)
JP (1) JP2016504304A (es)
KR (1) KR20150092762A (es)
CN (1) CN105324365A (es)
AR (1) AR093901A1 (es)
AU (1) AU2013359564A1 (es)
CA (1) CA2894667A1 (es)
HK (1) HK1214825A1 (es)
IL (1) IL239228A0 (es)
MX (1) MX2015007372A (es)
RU (1) RU2015128003A (es)
WO (1) WO2014093276A1 (es)
ZA (1) ZA201503835B (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2863994C (en) * 2012-02-16 2020-06-16 Dow Agrosciences Llc Methods of producing sulfilimine compounds
TWI735573B (zh) * 2016-06-21 2021-08-11 美商陶氏農業科學公司 生產某些經取代硫亞胺之方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2558647C (en) * 2004-04-08 2013-05-28 Dow Agrosciences Llc Insecticidal n-substituted sulfoximines
TW201309635A (zh) 2006-02-10 2013-03-01 Dow Agrosciences Llc 殺蟲性之ｎ-取代（６-鹵烷基吡啶-３-基）烷基磺醯亞胺（二）
TWI381811B (zh) * 2006-06-23 2013-01-11 Dow Agrosciences Llc 用以防治可抵抗一般殺蟲劑之昆蟲的方法
JP5302221B2 (ja) 2007-02-26 2013-10-02 ダウ アグロサイエンシィズ エルエルシー ある種の置換スルフィルイミン類の調製方法
CA2863994C (en) * 2012-02-16 2020-06-16 Dow Agrosciences Llc Methods of producing sulfilimine compounds

Also Published As

Publication number Publication date
EP2931706A1 (en) 2015-10-21
US20140163236A1 (en) 2014-06-12
AR093901A1 (es) 2015-06-24
KR20150092762A (ko) 2015-08-13
US20160137603A1 (en) 2016-05-19
JP2016504304A (ja) 2016-02-12
ZA201503835B (en) 2016-08-31
IL239228A0 (en) 2015-07-30
WO2014093276A1 (en) 2014-06-19
CA2894667A1 (en) 2014-06-19
CN105324365A (zh) 2016-02-10
AU2013359564A1 (en) 2015-06-11
RU2015128003A (ru) 2017-01-16
HK1214825A1 (zh) 2016-08-05

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