MX2010010765A - Metodo continuo para producir amidas de acidos carboxilicos aromaticos. - Google Patents

Metodo continuo para producir amidas de acidos carboxilicos aromaticos.

Info

Publication number
MX2010010765A
MX2010010765A MX2010010765A MX2010010765A MX2010010765A MX 2010010765 A MX2010010765 A MX 2010010765A MX 2010010765 A MX2010010765 A MX 2010010765A MX 2010010765 A MX2010010765 A MX 2010010765A MX 2010010765 A MX2010010765 A MX 2010010765A
Authority
MX
Mexico
Prior art keywords
aromatic carboxylic
carboxylic acids
continuous method
producing amides
reacted
Prior art date
Application number
MX2010010765A
Other languages
English (en)
Inventor
Christoph Kayser
Roman Morschhaeuser
Matthias Krull
Michael Seebach
Ralf Bierbaum
Original Assignee
Clariant Finance Bvi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Clariant Finance Bvi Ltd filed Critical Clariant Finance Bvi Ltd
Publication of MX2010010765A publication Critical patent/MX2010010765A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122—Incoherent waves
    • B01J19/126—Microwaves
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/81—Amides; Imides
    • C07D213/82—Amides; Imides in position 3

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La invención se refiere a un método continuo para producir amidas de ácidos carboxílicos aromáticos, mediante el cual por lo menos un ácido carboxílico aromático de fórmula (I), Ar-COOH, en donde Ar es un radical alquilo opcionalmente sustituido que comprende entre 5 y 20 átomos, por lo menos con una amina de la fórmula (II), HNR1R2, en donde R1 y R2 son independientemente hidrógeno o un grupo hidrocarburo que comprende entre 1 y 100 átomos de carbono, para formar una sal de amonio, y se hace reaccionar luego dicha sal de amonio para formar una carboxamida, bajo irradiación de microondas en un tubo de reacción, el eje longitudinal del tubo estando orientado en la dirección de propagación de las microondas de un aplicador de microondas de modo único.
MX2010010765A 2008-04-04 2009-03-18 Metodo continuo para producir amidas de acidos carboxilicos aromaticos. MX2010010765A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102008017217A DE102008017217A1 (de) 2008-04-04 2008-04-04 Kontinuierliches Verfahren zur Herstellung von Amiden aromatischer Carbonsäuren
PCT/EP2009/001984 WO2009121484A1 (de) 2008-04-04 2009-03-18 Kontinuierliches verfahren zur herstellung von amiden aromatischer carbonsäuren

Publications (1)

Publication Number Publication Date
MX2010010765A true MX2010010765A (es) 2010-10-26

Family

ID=40651444

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2010010765A MX2010010765A (es) 2008-04-04 2009-03-18 Metodo continuo para producir amidas de acidos carboxilicos aromaticos.

Country Status (11)

Country Link
US (1) US20110089019A1 (es)
EP (1) EP2274269A1 (es)
KR (1) KR20100135721A (es)
CN (1) CN101918355B (es)
AU (1) AU2009231119A1 (es)
BR (1) BRPI0907793A2 (es)
CA (1) CA2720319A1 (es)
DE (1) DE102008017217A1 (es)
EA (1) EA018345B1 (es)
MX (1) MX2010010765A (es)
WO (1) WO2009121484A1 (es)

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DE102008017218B4 (de) * 2008-04-04 2011-09-22 Clariant International Ltd. Kontinuierliches Verfahren zur Herstellung von Amiden niederer aliphatischer Carbonsäuren
DE102008017216B4 (de) * 2008-04-04 2013-08-14 Clariant International Ltd. Kontinuierliches Verfahren zur Herstellung von Fettsäureamiden
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DE102008017213B4 (de) * 2008-04-04 2012-08-09 Clariant International Limited Kontinuierliches Verfahren zur Herstellung von Amiden aliphatischer Hydroxycarbonsäuren
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CN109456214A (zh) * 2018-11-29 2019-03-12 福建医科大学 一种在水相中微波条件下苯甲酰胺类化合物的方法
CN111320553A (zh) * 2018-12-17 2020-06-23 潘伟 一种n,n-二甲基苯甲酰胺提纯装置
CN110405933A (zh) * 2019-08-31 2019-11-05 乌鲁木齐益好天成新型节能材料有限公司 微波、近红外双辐射sg外墙防火保温板生产流水线
WO2021252123A2 (en) * 2020-05-19 2021-12-16 Purdue Research Foundation Continuous flow sonogashira coupling synthesis method
CN113277956B (zh) * 2021-06-03 2022-11-04 浙江树人学院（浙江树人大学） 一种使用无污染性耦合剂合成酰胺类化合物的方法

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Also Published As

Publication number Publication date
AU2009231119A1 (en) 2009-10-08
DE102008017217A1 (de) 2009-10-08
US20110089019A1 (en) 2011-04-21
EP2274269A1 (de) 2011-01-19
CN101918355B (zh) 2013-07-17
BRPI0907793A2 (pt) 2015-07-14
CN101918355A (zh) 2010-12-15
WO2009121484A1 (de) 2009-10-08
EA201001113A1 (ru) 2010-12-30
EA018345B1 (ru) 2013-07-30
KR20100135721A (ko) 2010-12-27
CA2720319A1 (en) 2009-10-08

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