MX170684B - Procedimiento para la eliminacion de catalizadores de polieterpolioles - Google Patents
Procedimiento para la eliminacion de catalizadores de polieterpoliolesInfo
- Publication number
- MX170684B MX170684B MX019635A MX1963590A MX170684B MX 170684 B MX170684 B MX 170684B MX 019635 A MX019635 A MX 019635A MX 1963590 A MX1963590 A MX 1963590A MX 170684 B MX170684 B MX 170684B
- Authority
- MX
- Mexico
- Prior art keywords
- catalysts
- polyeterpoliol
- elimination
- procedure
- hydrolysis
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 230000008030 elimination Effects 0.000 title 1
- 238000003379 elimination reaction Methods 0.000 title 1
- 239000004721 Polyphenylene oxide Substances 0.000 abstract 2
- 230000007062 hydrolysis Effects 0.000 abstract 2
- 238000006460 hydrolysis reaction Methods 0.000 abstract 2
- 229920000570 polyether Polymers 0.000 abstract 2
- 229920005862 polyol Polymers 0.000 abstract 2
- 150000003077 polyols Chemical class 0.000 abstract 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyethers (AREA)
- Polyesters Or Polycarbonates (AREA)
- Polyurethanes Or Polyureas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente invención se refiere a procedimiento para la eliminación de catalizadores básicos de polieter-polioles con índices de OH de 4 a 250, mediante hidrólisis del alcoholato alcalino y mediante introducción de CO2 y eliminación por filtración del carbonato formado, caracterizado porque la hidrólisis del alcoholato se lleva a cabo con 0,7 a 7 por ciento en peso de agua (referido al polieter-poliol) a 25 hasta 125 grados C y, a continuación, se introduce CO2 en una cantidad de aproximadamente 1 a 2 veces la cantidad estequiometrica a una temperatura de 75 a 120 grados C.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3907911A DE3907911A1 (de) | 1989-03-11 | 1989-03-11 | Verfahren zur entfernung von katalysatoren aus polyether-polyolen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX170684B true MX170684B (es) | 1993-09-07 |
Family
ID=6376087
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX019635A MX170684B (es) | 1989-03-11 | 1990-02-23 | Procedimiento para la eliminacion de catalizadores de polieterpolioles |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5105019A (es) |
| EP (1) | EP0387576B1 (es) |
| JP (1) | JP2976307B2 (es) |
| KR (1) | KR0168429B1 (es) |
| BR (1) | BR9001123A (es) |
| CA (1) | CA2010433C (es) |
| DE (2) | DE3907911A1 (es) |
| ES (1) | ES2045592T3 (es) |
| MX (1) | MX170684B (es) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4408004A1 (de) * | 1994-03-10 | 1995-09-14 | Bayer Ag | Verfahren zur Gewinnung von reinen, fließfähigen Alkali- oder Erdalkalisalzen aus den Salzrückständen der Polyetherpolyolproduktion |
| EP2669312A1 (en) * | 2012-05-29 | 2013-12-04 | Huntsman International Llc | Process for the production of polyether polyols |
| US11572440B2 (en) | 2020-02-18 | 2023-02-07 | Covestro Llc | Methods for purifying polyols containing oxyalkylene units to reduce 2-methyl-2-pentenal content |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3715402A (en) * | 1969-08-08 | 1973-02-06 | Basf Wyandotte Corp | Removal of catalysts from polyols |
| BE795455A (fr) * | 1972-02-24 | 1973-08-16 | Basf Ag | Procede de preparation de polyalkylene-ethers purs |
| DD104806A1 (es) * | 1973-05-30 | 1974-03-20 | ||
| DE2554228A1 (de) * | 1974-12-13 | 1976-06-16 | Basf Wyandotte Corp | Verfahren zur reinigung von hydroxylgruppenhaltigen polyaethern |
| US4029879A (en) * | 1975-11-17 | 1977-06-14 | Basf Wyandotte Corporation | Process for the removal of catalysts from polyether polyols employing water and adsorbent |
| US4137396A (en) * | 1976-09-24 | 1979-01-30 | Basf Wyandotte Corporation | Filtration process for purifying polyols |
| US4129718A (en) * | 1977-12-01 | 1978-12-12 | Basf Wyandotte Corporation | Process for the removal of catalyst from polyether polyol |
| US4137398A (en) * | 1978-06-09 | 1979-01-30 | Basf Wyandotte Corporation | Process for the removal of catalyst from polyether polyol |
-
1989
- 1989-03-11 DE DE3907911A patent/DE3907911A1/de not_active Withdrawn
-
1990
- 1990-02-20 CA CA002010433A patent/CA2010433C/en not_active Expired - Fee Related
- 1990-02-23 MX MX019635A patent/MX170684B/es unknown
- 1990-02-25 DE DE9090103642T patent/DE59000031D1/de not_active Expired - Lifetime
- 1990-02-25 ES ES90103642T patent/ES2045592T3/es not_active Expired - Lifetime
- 1990-02-25 EP EP90103642A patent/EP0387576B1/de not_active Expired - Lifetime
- 1990-03-02 US US07/459,233 patent/US5105019A/en not_active Expired - Fee Related
- 1990-03-09 JP JP2056795A patent/JP2976307B2/ja not_active Expired - Fee Related
- 1990-03-09 BR BR909001123A patent/BR9001123A/pt not_active IP Right Cessation
- 1990-03-09 KR KR1019900003103A patent/KR0168429B1/ko not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| BR9001123A (pt) | 1991-03-05 |
| CA2010433C (en) | 1999-08-17 |
| KR0168429B1 (ko) | 1999-03-20 |
| CA2010433A1 (en) | 1990-09-11 |
| JPH02274727A (ja) | 1990-11-08 |
| US5105019A (en) | 1992-04-14 |
| DE3907911A1 (de) | 1990-09-13 |
| DE59000031D1 (de) | 1992-02-27 |
| EP0387576A1 (de) | 1990-09-19 |
| KR900014464A (ko) | 1990-10-24 |
| EP0387576B1 (de) | 1992-01-15 |
| JP2976307B2 (ja) | 1999-11-10 |
| ES2045592T3 (es) | 1994-01-16 |
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