KR970058715A - Methods for the preparation of water-soluble pearlescent liquids using physical, chemical and biochemical methods - Google Patents
Methods for the preparation of water-soluble pearlescent liquids using physical, chemical and biochemical methods Download PDFInfo
- Publication number
- KR970058715A KR970058715A KR1019960000873A KR19960000873A KR970058715A KR 970058715 A KR970058715 A KR 970058715A KR 1019960000873 A KR1019960000873 A KR 1019960000873A KR 19960000873 A KR19960000873 A KR 19960000873A KR 970058715 A KR970058715 A KR 970058715A
- Authority
- KR
- South Korea
- Prior art keywords
- supernatant
- pearl
- precipitate
- water
- liquid
- Prior art date
Links
- 239000007788 liquid Substances 0.000 title claims abstract 11
- 238000002306 biochemical method Methods 0.000 title claims abstract 4
- 239000000126 substance Substances 0.000 title claims abstract 4
- 238000000034 method Methods 0.000 title claims 9
- 238000002360 preparation method Methods 0.000 title claims 2
- 239000006228 supernatant Substances 0.000 claims abstract 17
- 239000007787 solid Substances 0.000 claims abstract 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract 6
- 239000002244 precipitate Substances 0.000 claims abstract 6
- 239000000243 solution Substances 0.000 claims abstract 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract 4
- 229960000583 acetic acid Drugs 0.000 claims abstract 3
- 239000012362 glacial acetic acid Substances 0.000 claims abstract 3
- 102000035195 Peptidases Human genes 0.000 claims abstract 2
- 108091005804 Peptidases Proteins 0.000 claims abstract 2
- 239000007853 buffer solution Substances 0.000 claims abstract 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract 2
- 239000001569 carbon dioxide Substances 0.000 claims abstract 2
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract 2
- 230000003472 neutralizing effect Effects 0.000 claims abstract 2
- 239000011541 reaction mixture Substances 0.000 claims abstract 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract 2
- 239000011049 pearl Substances 0.000 claims 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 239000013505 freshwater Substances 0.000 claims 1
- 239000011050 natural pearl Substances 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 230000001376 precipitating effect Effects 0.000 claims 1
- 210000002966 serum Anatomy 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract 3
- 235000012489 doughnuts Nutrition 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/02—Antioxidant
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Nutrition Science (AREA)
- Inorganic Chemistry (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Zoology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Peptides Or Proteins (AREA)
- Cosmetics (AREA)
Abstract
본 발명은 물리, 화학 및 생화학적 방법을 이용한 수용성 진주액의 제조방법에 관한 것으로, 좀 더 상세하게는 외피를 제거한 진주를 10~20메쉬의 입자크기로 분쇄시킨 후, 1 내지 4배의 물을 첨가하여 밀봉시킨 다음, 100 내지 125℃, 1내지 1.5기압에서 15분 이상 반응시키고, 상기 반응물을 상온에서 충분히 정치시켜 고형분을 침전시킨후, 제1상등액을 분리시키는 제1단계; 상기 제1단계의 침전된 고형분에 식용빙초산액을 첨가하여 이산화탄소가 발생되지 않을때까지 반응시킨 다음, 고형분을 침전시키고 제2상등액을 분리시키는 제2단께; 상기 제2단계의 침전도니 고형물과 염산을 반응시켜 탄산칼슘을 제거하고 세정한 다음. 최종액의 pH를 중성으로 전환시켜 침전물을 얻는 단계; 상기 침전물을 탄산나트륨 완충용액으로 분산시킨 후, 단백질분해효소를 첨가하여 반응시킨 다음, 염산으로 중화시켜 제3상등애을 분리시키는 제3단계; 및 상기 제1상등액, 제2상등액 및 제3상등액을 적당한 비율로 혼합시키는 단계로 이루어지는 물리, 화학 및 생화학적 방법을 이용한 수용성 진주액의 제조방법에 관한 것이다.The present invention relates to a method for producing a water-soluble pearl liquid by physical, chemical and biochemical methods, and more particularly, to a method for producing a water-soluble pearl liquid by pulverizing a pearl with a shell of 10 to 20 mesh, The reaction is carried out at a temperature of 100 to 125 DEG C and 1 to 1.5 atm for 15 minutes or more, and the reaction is allowed to stand at room temperature to precipitate solid components, followed by separation of the first supernatant liquid; To the second stage where the edible glacial acetic acid solution is added to the precipitated solid content of the first step to react until the carbon dioxide is not generated and then the solid content is precipitated and the second supernatant liquid is separated; The precipitated donut solids in the second step are reacted with hydrochloric acid to remove calcium carbonate and then washed. Converting the pH of the final solution to neutrality to obtain a precipitate; A third step of dispersing the precipitate in a sodium carbonate buffer solution, adding a proteolytic enzyme to the reaction mixture, and neutralizing the precipitate with hydrochloric acid to separate a third phylum; And mixing the first supernatant, the second supernatant, and the third supernatant at an appropriate ratio. The present invention also relates to a method for producing a water-soluble pearl liquid using physical, chemical and biochemical methods.
Description
내용없음No content
Claims (7)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019960000873A KR0173429B1 (en) | 1996-01-17 | 1996-01-17 | Process for preparation of pearl solution with physical, chemical and biochemical method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019960000873A KR0173429B1 (en) | 1996-01-17 | 1996-01-17 | Process for preparation of pearl solution with physical, chemical and biochemical method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR970058715A true KR970058715A (en) | 1997-08-12 |
| KR0173429B1 KR0173429B1 (en) | 1999-02-01 |
Family
ID=19449592
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019960000873A KR0173429B1 (en) | 1996-01-17 | 1996-01-17 | Process for preparation of pearl solution with physical, chemical and biochemical method |
Country Status (1)
| Country | Link |
|---|---|
| KR (1) | KR0173429B1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100397682B1 (en) * | 2001-02-26 | 2003-09-13 | 송선자 | Ionized calcium and ionized calcium water made of pearl shell and preparation method of the same |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100549399B1 (en) * | 2002-07-09 | 2006-02-03 | (주) 진주본 | The method of preparing water-soluble pearl powder using acid hydrolysis in normal temperature |
| KR20040006092A (en) * | 2002-07-09 | 2004-01-24 | 서숙 | Dermis-accelerant Including the Fine Pure Pearl Powder |
| KR101313266B1 (en) * | 2010-10-11 | 2013-09-30 | 양승필 | High-calcium soybean curd containing pearl material and Making method thereof |
| CN104905242B (en) * | 2014-03-14 | 2017-06-13 | 浙江欧诗漫生物股份有限公司 | It is a kind of that the method for preparing the solvable edible calcium of pearl and pearl composite whitening factor solutions is separated from pearl |
| KR102259686B1 (en) * | 2019-11-06 | 2021-06-02 | 안은영 | Manufacturing method of food, health functional food and cosmetic composition using water-soluble pearl Fermentation capsule |
-
1996
- 1996-01-17 KR KR1019960000873A patent/KR0173429B1/en not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100397682B1 (en) * | 2001-02-26 | 2003-09-13 | 송선자 | Ionized calcium and ionized calcium water made of pearl shell and preparation method of the same |
Also Published As
| Publication number | Publication date |
|---|---|
| KR0173429B1 (en) | 1999-02-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH07502416A (en) | Purification of zein from corn gluten meal | |
| CN103497535A (en) | Animal melanin extraction method and application of extraction product thereof | |
| KR970058715A (en) | Methods for the preparation of water-soluble pearlescent liquids using physical, chemical and biochemical methods | |
| CN110643665A (en) | Method for extracting selenoprotein from selenium-enriched yeast by double-enzyme coupling method | |
| KR970068894A (en) | Health food composition containing minerals, herbal medicine extracts and amino acids | |
| AU2002364492A1 (en) | Process for the production of alginate having a high mannuronic acid-content | |
| JPH01275512A (en) | Production of soluble shell membrane | |
| KR100549399B1 (en) | The method of preparing water-soluble pearl powder using acid hydrolysis in normal temperature | |
| JP3450383B2 (en) | Active oxygen inhibitor | |
| JPH0515684B2 (en) | ||
| JP2002037742A (en) | Skin care preparation | |
| GB2046235A (en) | Removing dissolved organic impurities from waste water | |
| RU2233104C1 (en) | Method for complex reprocessing of brown algae for producing of iodine-containing and polysaccharide products | |
| JP2004083451A (en) | Skin lotion | |
| RU2122414C1 (en) | Method of preparing a preparation based on himatomelanoic acids of low-mineralized silt sulfide dirt for physiotherapy | |
| JPS63126597A (en) | Soluble dye decoloring agent | |
| SU597648A1 (en) | Method of processing excess activated sludge | |
| JPS61277695A (en) | Production of fructooligosaccharide | |
| JPS63126596A (en) | Decoloring method for soluble dye by microorganism | |
| US3848812A (en) | Process for extracting protein from microorganisms | |
| JPH07255418A (en) | Diet food | |
| KR850000867B1 (en) | Method for extracting protein from red worm | |
| WO1994004551A1 (en) | Method of obtaining sodium salt of native dna | |
| SU1117037A1 (en) | Method of obtaining food additive from production waste water of meat-packing plant | |
| SU546648A1 (en) | The method of obtaining the complex of proteolytic enzymes |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination | ||
| E902 | Notification of reason for refusal | ||
| E701 | Decision to grant or registration of patent right | ||
| GRNT | Written decision to grant | ||
| FPAY | Annual fee payment |
Payment date: 20041101 Year of fee payment: 7 |
|
| LAPS | Lapse due to unpaid annual fee |