KR970042574A - 피콜린산크롬의 제조방법 - Google Patents
피콜린산크롬의 제조방법 Download PDFInfo
- Publication number
- KR970042574A KR970042574A KR1019950051991A KR19950051991A KR970042574A KR 970042574 A KR970042574 A KR 970042574A KR 1019950051991 A KR1019950051991 A KR 1019950051991A KR 19950051991 A KR19950051991 A KR 19950051991A KR 970042574 A KR970042574 A KR 970042574A
- Authority
- KR
- South Korea
- Prior art keywords
- acid
- chromium
- minutes
- reaction solution
- carbonate
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- SIOXPEMLGUPBBT-UHFFFAOYSA-M picolinate Chemical compound [O-]C(=O)C1=CC=CC=N1 SIOXPEMLGUPBBT-UHFFFAOYSA-M 0.000 title abstract 2
- 239000011651 chromium Substances 0.000 claims abstract 5
- 239000002253 acid Substances 0.000 claims abstract 4
- 239000003513 alkali Substances 0.000 claims abstract 4
- 238000010438 heat treatment Methods 0.000 claims abstract 4
- 238000004519 manufacturing process Methods 0.000 claims abstract 4
- SIOXPEMLGUPBBT-UHFFFAOYSA-N picolinic acid Chemical compound OC(=O)C1=CC=CC=N1 SIOXPEMLGUPBBT-UHFFFAOYSA-N 0.000 claims abstract 4
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract 3
- 229910052804 chromium Inorganic materials 0.000 claims abstract 3
- 229940081066 picolinic acid Drugs 0.000 claims abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 229940046374 chromium picolinate Drugs 0.000 claims 3
- GJYSUGXFENSLOO-UHFFFAOYSA-N chromium;pyridine-2-carboxylic acid Chemical compound [Cr].OC(=O)C1=CC=CC=N1.OC(=O)C1=CC=CC=N1.OC(=O)C1=CC=CC=N1 GJYSUGXFENSLOO-UHFFFAOYSA-N 0.000 claims 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims 2
- PHFQLYPOURZARY-UHFFFAOYSA-N chromium trinitrate Chemical compound [Cr+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O PHFQLYPOURZARY-UHFFFAOYSA-N 0.000 claims 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims 2
- 229910021555 Chromium Chloride Inorganic materials 0.000 claims 1
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims 1
- QSWDMMVNRMROPK-UHFFFAOYSA-K chromium(3+) trichloride Chemical compound [Cl-].[Cl-].[Cl-].[Cr+3] QSWDMMVNRMROPK-UHFFFAOYSA-K 0.000 claims 1
- GRWVQDDAKZFPFI-UHFFFAOYSA-H chromium(III) sulfate Chemical compound [Cr+3].[Cr+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O GRWVQDDAKZFPFI-UHFFFAOYSA-H 0.000 claims 1
- 235000015497 potassium bicarbonate Nutrition 0.000 claims 1
- 229910000027 potassium carbonate Inorganic materials 0.000 claims 1
- 235000011181 potassium carbonates Nutrition 0.000 claims 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 229910000029 sodium carbonate Inorganic materials 0.000 claims 1
- 239000000654 additive Substances 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F11/00—Compounds containing elements of Groups 6 or 16 of the Periodic Table
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/30—Foods, ingredients or supplements having a functional effect on health
- A23V2200/328—Foods, ingredients or supplements having a functional effect on health having effect on glycaemic control and diabetes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/30—Other Organic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
Abstract
본 발명에 따라 식품 또는 동물 사료의 첨가제로서 사용되는 고순도 피콜린산크롬을 고수율로 얻을 수 있는 새로운 제조방법이 제공된다. 본 발명의 방법은 +3가 크롬의 강산염과, 동 당량의 피콜린산을 물에 녹여 70-100℃에서 20분 이상 가열한 후 이 반응에서 생성될 수 있는 산의 전량을 중화시키는데 필요한 알칼리의 50-100%를 반응액의 pH가 3.5 이하가 되도록 유지하면서 반응액에 가한 후 계속 70-100℃에서 20분 이상 가열하는 것으로 이루어진다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (3)
- 염화크롬(CrCl3· xH2O), 황산크롬(Cr2(SO4)3· xH2O) 또는 질산크롬(Cr(NO3)3· xH2O) 중에서 선택된 +3가 크롬의 강산염과 같은 당량의 피콜린산을 물에 녹여 80-100℃에서 20분 이상 가열한 후, 이 반응에서 생성가능한 산의 전량을 중화하는데 필요한 알칼리의 50-100%를 반응액의 pH가 1.5 내지 3.5가 유지되는 범위에서 반응액에 서서히 가한 후 계속 70-100℃에서 20분 이상 가열하는 것으로 되는 피콜린산크롬의 제조방법.
- 제1항에 있어서, 알칼리가 수산화나트륨, 수산화칼륨, 탄산나트륨, 탄산칼륨, 산성탄산나트륨, 및 산성탄산칼륨 중에서 선택되는 것이 특징인 피콜린산크롬의 제조방법.
- 제1항에 있어서, 생성가능한 산의 전량을 중화하는데 필요한 알칼리의 50-100%를, 한번에 또는 수차례로 나누어 반응액에 첨가하여 중화처리하는 것이 특징인 피콜린산크롬의 제조방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019950051991A KR0184380B1 (ko) | 1995-12-19 | 1995-12-19 | 피콜린산크롬의 제조방법 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019950051991A KR0184380B1 (ko) | 1995-12-19 | 1995-12-19 | 피콜린산크롬의 제조방법 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR970042574A true KR970042574A (ko) | 1997-07-24 |
| KR0184380B1 KR0184380B1 (ko) | 1999-05-15 |
Family
ID=19441408
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019950051991A KR0184380B1 (ko) | 1995-12-19 | 1995-12-19 | 피콜린산크롬의 제조방법 |
Country Status (1)
| Country | Link |
|---|---|
| KR (1) | KR0184380B1 (ko) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20020094622A (ko) * | 2001-06-12 | 2002-12-18 | 주식회사 동우 티엠씨 | 피콜린산 크롬의 제조방법 |
| CN109232404A (zh) * | 2018-08-15 | 2019-01-18 | 四川新美生物科技有限公司 | 一种吡啶甲酸铬的制备方法 |
| CN112174882B (zh) * | 2020-09-29 | 2022-06-10 | 上海沃凯生物技术有限公司 | 一种环保的吡啶甲酸铬制备方法 |
-
1995
- 1995-12-19 KR KR1019950051991A patent/KR0184380B1/ko not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| KR0184380B1 (ko) | 1999-05-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| BR8101848A (pt) | Catalisador que compreende oxido de cobre e oxido de aluminio e processo para sua preparacao | |
| ES2137683T3 (es) | Derivados de hidrotalcita que comprenden niquel y cobalto y con una morfologia en hoja, y procedimiento de produccion. | |
| KR970042574A (ko) | 피콜린산크롬의 제조방법 | |
| GB1077036A (en) | Process for the production of the sodium salt of 3-hydroxy-2-oxo-1(2h)-pyridine sulphonic acid and the production of 2,3-pyridine diol | |
| JPS55122885A (en) | Production of nickel hydroxide compound | |
| KR870008793A (ko) | 구리 수산화물의 제조방법 | |
| KR890003960A (ko) | 고-추출 크롬탄닝 공정 | |
| KR850004444A (ko) | 조절개시에 의한 이산화크롬의 제조방법 | |
| IE38692B1 (en) | Process for the preparation of alkylsulphonate compounds | |
| ES467659A1 (es) | Procedimiento para la obtencion de un curtiente de cromo y sal de glauber. | |
| GB1182513A (en) | Guanosine Derivatives and a process for preparing the same | |
| Mohan | Acid character of octacyanotungstic (IV) acid and isolation of a red product of its photodecomposition | |
| JPS53132499A (en) | Production of chromium hydroxide | |
| US92405A (en) | Gael wandel | |
| GB517455A (en) | Improvements in or relating to the conversion of alkaline earth metal oxalates and the manufacture of alkali metal hydroxides | |
| KR970065501A (ko) | 칼슘 피루베이트 및 이의 수화물의 제조방법 | |
| KR840009301A (ko) | 2-퀴녹살리놀의 제조방법 | |
| US3382233A (en) | Process for producing 5'-guanylic acid | |
| JPS55151554A (en) | Production of dihydroperoxide | |
| GB1311480A (en) | Process for the production of hydrazodicarbonamide and azodi carbonamide | |
| KR850005987A (ko) | 염기성 탄산알루미늄마그네슘의 제조방법 | |
| KR950005864A (ko) | 포름 알데히드 수지중의 유리 포름 알데히드의 제거방법 | |
| GB1440754A (en) | Method for the preparation of aminocarboxylic acid salts | |
| GB1451528A (en) | Process for the preparation of 4-bromonaphthalic acid anhydride | |
| GB1063893A (en) | Process for the manufacture of hydrazine and derivatives thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination | ||
| E902 | Notification of reason for refusal | ||
| E601 | Decision to refuse application | ||
| J201 | Request for trial against refusal decision | ||
| B701 | Decision to grant | ||
| GRNT | Written decision to grant | ||
| FPAY | Annual fee payment |
Payment date: 20091218 Year of fee payment: 12 |
|
| LAPS | Lapse due to unpaid annual fee |