KR970027175A - 펌프가능하고 안정한 범용 폴리디오가노실록산-실리카 혼합물의 제조방법 및 실온 경화성 실런트 - Google Patents

펌프가능하고 안정한 범용 폴리디오가노실록산-실리카 혼합물의 제조방법 및 실온 경화성 실런트 Download PDF

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KR970027175A
KR970027175A KR1019960058836A KR19960058836A KR970027175A KR 970027175 A KR970027175 A KR 970027175A KR 1019960058836 A KR1019960058836 A KR 1019960058836A KR 19960058836 A KR19960058836 A KR 19960058836A KR 970027175 A KR970027175 A KR 970027175A
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South Korea
Prior art keywords
weight
polydiorganosiloxane
mixture
amount
silica filler
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KR1019960058836A
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English (en)
Inventor
토마스 뷘쉬
리아 크레스
베르너 로크
아우구스트 레네르
알베르트 코올
노르베르트 쉬나이더
우베 부르크하르트
다까히로 아다찌
도시아끼 다까따
리차드 마크 스코트
로버트 윌리암 쇼
마크 데이비드 피셔
로렌 데일 로우어
셔우드 스펠스
Original Assignee
트리쉬만, 덴케
바스프 마그네틱스 게엠베하
오히라 아끼라
미쓰비시 가스 가가꾸 가부시끼가이샤
알베르투스 빌헬무스 요아네스 쩨스트라텐
셀 인터나쵸나아레 레사아치 마아츠샤피 비이.브이.
루이스 노만 에드워드
다우 코닝 코포레이션
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Application filed by 트리쉬만, 덴케, 바스프 마그네틱스 게엠베하, 오히라 아끼라, 미쓰비시 가스 가가꾸 가부시끼가이샤, 알베르투스 빌헬무스 요아네스 쩨스트라텐, 셀 인터나쵸나아레 레사아치 마아츠샤피 비이.브이., 루이스 노만 에드워드, 다우 코닝 코포레이션 filed Critical 트리쉬만, 덴케
Publication of KR970027175A publication Critical patent/KR970027175A/ko

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Abstract

본 발명은 실리카 1중량부당 디올 0.05 내지 0.5중량부를 이용하여, 50 내지 180℃에서 폴리디오가노실록산, 강화 실리카 충전제 및 디올 표면 개질제를 혼합하고 가열하여 펌프가능하고 안정한 범용 폴리디오가노실록산-실리카 혼합물을 제조하는 방법에 관한 것이다.
당해 혼합물을 사용하여 새깅되지 않은 RTV 실리콘 실런트 조성물을 제조한다.

Description

펌프가능하고 안정한 범용 폴리디오가노실록산-실리카 혼합물의 제조방법 및 실온 경화성 실런트
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (4)

  1. 25℃에서 측정한 점도가, 0.1 내지 400Paㆍs인 폴리디오가노실록산, 규소 결합된 하이드록실 그룹을 3중량%이상 포함하는 화학식(1)의 디올 표면 개질제 및 표면적이 90 내지 500㎡/g이고 폴리디오가노실록산 전체에 균일하게 분산되는 강화 실리카 충전제를 혼합하여 제1혼합물(여기서, 폴리디오가노실록산, 실리카 충전제 및 디올을 합한 총 100중량부를 기준으로 하여, 폴리디오가노실록산의 양은 전체 혼합물 중에 80 내지 95중량%를 제공하는 데 필요한 양의 50 내지 100중량%이고, 디올의 양은 전체 혼합물 중에 실리카 충전제 1부당 디올 0.05 내지 0.5부를 제공하는 데 필요한 양의 20 내지 100중량%이고, 실리카 충전제의 양은 전체 혼합물 중에 실리카 충전제 5 내지 19.5중량%를 제공하는 데 필요한 양의 0 내지 100중량%이다)을 형성하는 단계(i), 디올 및 실리카 충전제의 하나 이상의 증가물(여기서, 증분은 첨가될 양의 5중량% 이상이다)을 제1혼합물과 혼합하여 제2혼합물(여기서, 폴리디오가노실록산, 실리카 충전제 및 디올을 합한 총 100중량부를 기준으로 하여, 디올의 양은 전체 혼합물 중에 실리카 충전제 1부당 디올 0.05 내지 0.5부를 제공하는 데 필요한 양은 0 내지 80중량%이고, 실리카 충전제의 양은 전체 혼합물 중에 실리카 충전제 5 내지 19.5중량%를 제공하는데 필요한 양의 100중량% 이하이다)을 형성하는 단계(ii), 폴리디오가노실록산의 하나 이상의 증가물(여기서, 증분은 첨가될 양의 5중량% 이상이다)을 제2혼합물과 혼합하여 제3혼합물(여기서, 폴리디오가노실록산의 양은 전체 혼합물 중에 폴리디오가노실록산 80 내지 95중량%를 제공하는 데 필요한 양의 0 내지 50중량%이다)을 형성하는 단계(iii) 및 제3혼합물을 50 내지 180℃의 온도에서 15분 이상 동안 혼합, 가열함으로써 휘발 물질을 제거하여, 폴리디오가노실록산, 실리카 충전제 및 디올을 합한 총 100중량%를 기준으로 하여, 실리카 충전제 5 내지 19.5중량%와 폴리디오가노실록산 80 내지 95중량%로 이루어지고 25℃에서 측정한 플라토 응력이 700dynes/㎠ 이상이며 25℃에서 측정한 50,000dynes/㎠의 전단 응력에서의 전단감점도가 1,000Paㆍs이하인 혼합물을 수득하는 단계(iv)를 포함하여, 펌프가능하고 안정한 범용 폴리디오가노실록산-실리카 혼합물을 제조하는 방법.
    R'O(R2SiO)xR' (1)
    위의 화학식(1)에서 R은 메틸, 에틸, 비닐 또는 3,3,3-트리폴루오로프로필이고, R'는 각각 수소원자, 메틸 라디칼 및 에틸 라디칼로 이루어진 그룹 중에서 선택되는데, R' 그룹 중의 30% 이하는 메틸 라디칼 또는 에틸 라디칼이며, x는 2 내지 18이다.
  2. 25℃에서 측정한 플라토 응력이 1000dynes/㎠ 이상이고 25℃에서 측정한 50,000dynes/㎠의 전단 응력에서의 전단감점도가 600Paㆍs이하인, 제1항에 따르는 방법으로 수득가능한 범용 혼합물.
  3. 제1항에 있어서, 폴리디오가노실록산 말단 그룹의 80% 이상이 규소 결합된 하이드록실 그룹인 방법.
  4. 제2항에 따르는 범용 혼합물을 포함하고 수분 가수분해성 가교결합 실리콘 화합물을 추가로 포함하는 실온 경화성 실리콘 실런트 조성물.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019960058836A 1995-11-02 1996-11-28 펌프가능하고 안정한 범용 폴리디오가노실록산-실리카 혼합물의 제조방법 및 실온 경화성 실런트 KR970027175A (ko)

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DE19540812.8 1995-11-02
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US08/564,775 1995-11-29
US08/564,840 1995-11-29
US08/564,840 US5670560A (en) 1995-11-29 1995-11-29 Method of making a pumpable, stable polydiorganosiloxane-silica foundation mixture and room temperature curing sealant

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US5990223A (en) * 1998-02-17 1999-11-23 Dow Corning Corporation Control of rheological and mechanical properties of silicone elastomers containing silica filler
EP1248819A1 (en) * 1999-12-10 2002-10-16 General Electric Company Room temperature curable silicone sealant
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US2890188A (en) * 1951-12-17 1959-06-09 Dow Corning Siloxane elastomers compounded with hydroxylated silanes
US3274145A (en) 1962-09-04 1966-09-20 Dow Corning Novel siloxane compositions
US4585830A (en) * 1985-05-20 1986-04-29 Dow Corning Corporation Polyorganosiloxane compositions useful for preparing unsupported extruded profiles
US4871827A (en) 1986-03-03 1989-10-03 Dow Corning Corporation Method of improving shelf life of silicone elastomeric sealant
US4657967A (en) 1986-04-07 1987-04-14 Dow Corning Corporation Room temperature curing compositions containing tetrafunctional ethoxy-ketoximo silane crosslinkers
US4724167A (en) * 1986-05-30 1988-02-09 General Electric Company Treated silica fillers and process for making the same
US4973623A (en) 1989-05-26 1990-11-27 Dow Corning Corporation Fast curing oximo-ethoxy functional siloxane sealants
JP3136164B2 (ja) * 1991-01-30 2001-02-19 東レ・ダウコーニング・シリコーン株式会社 室温硬化性オルガノポリシロキサン組成物
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