KR970025674A - 질소 생성을 위한 공기 분리방법 및 장치 - Google Patents

질소 생성을 위한 공기 분리방법 및 장치 Download PDF

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KR970025674A
KR970025674A KR1019960052443A KR19960052443A KR970025674A KR 970025674 A KR970025674 A KR 970025674A KR 1019960052443 A KR1019960052443 A KR 1019960052443A KR 19960052443 A KR19960052443 A KR 19960052443A KR 970025674 A KR970025674 A KR 970025674A
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nitrogen
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coolant
distillation column
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이윤석
요셉 피 노모비츠
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이윤석
카셋트 래리 알
더 비오씨 그룹, 인코포레이티드
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/044—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a single pressure main column system only
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    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
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    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04048—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams
    • F25J3/04066—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams of oxygen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
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    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04321—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of oxygen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/72—Refluxing the column with at least a part of the totally condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
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    • F25J2230/52—Processes or apparatus involving steps for increasing the pressure of gaseous process streams the fluid being oxygen enriched compared to air, e.g. "crude oxygen"
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    • F25J2250/00—Details related to the use of reboiler-condensers
    • F25J2250/02—Bath type boiler-condenser using thermo-siphon effect, e.g. with natural or forced circulation or pool boiling, i.e. core-in-kettle heat exchanger
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Abstract

질소를 생성하는 방법은 제1 및 제2냉각제 스트림이 증류칼럼에 역류를 제공하기 위해 질소가 풍부한 최상부를 응축하는데 사용되는 단일 칼럼 질소 발생기이다. 냉각제 스트림 중의 하나는 증류칼럼의 기부영역 중에서 생성되는 산소가 풍부한 액체보다 더 높은 질소함량을 갖는 액체로 구성된다. 이 냉각제 스트림은 질소 재생을 증가시키기 위해 증류칼럼의 기부에서 압축, 냉각 및 재순환된다.

Description

질소 생성을 위한 공기 분리방법 및 장치
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명의 장치에서 공기를 분리하는 방법을 도시한다.

Claims (8)

  1. 공기의 정류를 위해 적합한 온도로 압축되고 정화된 공급공기를 냉각하고; 질소가 풍부한 수증기 최상부 및 칼럼 기부로서 산소가 풍부한 액체를 생성하기 위해 증류칼럼내에 상기 압축되고 정화된 공급공기를 도입하고; 상기 질소가 풍부한 수증기 최상부로 구성되는 질소가 풍부한 스트림의 일부이상을 응축하고 역류로서 상기 증류칼럼내에 생성된 응축물의 일부이상을 도입하고; 상기 산소가 풍부한 액체의 함량보다 더 큰 질소함량을 갖는 질소-함유 액체를 상기 증류칼럼으로부터 추출하고; 상기 산소가 풍부한 액체 및 질소-함유 액체로 구성되는 제1 및 제2냉각제 스트림을 각각 팽창시키고; 상기 제1 및 제2냉각제 스트림으로 상기 일부 이상의 상기 질소가 풍부한 스트림을 응축하여 증발된 제1 및 제2냉각제 스트림을 형성하고; 상기 질소가 풍부한 스트림의 또다른 부분으로부터 질소 생성물을 추출하고; 냉동제 스트림을 형성하기 위해 작동의 수행으로 상기 제1증발된 냉각제 스트림을 부분적으로 가온 및 팽창시키고; 상기 냉동제 스트림과 상기 압축되고 정화된 공기 사이에서 간접적으로 열을 교환하고; 및 상기 제2증발된 냉각제 스트림을 압축하고, 상기 온도로 상기 제2증발된 냉각제 스트림을 냉각하고, 상기 증류칼럼의 기부영역으로 상기 제2증발된 냉각제 스트림을 도입하여 상기 질소 생성물의 재생을 중가시키는 것을 포함하는 질소 생성방법.
  2. 제1항에 있어서, 상기 질소 생성물이 기체 질소 생성물 스트림으로서 추출되는 방법.
  3. 제1항에 있어서, 상기 제1압축되고 정화된 공급공기가 상기 증류칼럼의 중간위치로 도입되는 방법.
  4. 제1항 또는 제3항에 있어서, 상기 제2증발된 냉각제 스트림이 필수적으로 상기 온도에서 압축되는 방법.
  5. 제4항에 있어서, 상기 제1 및 제2냉각제 스트림이 팽창되기에 앞서 보조 냉각되는 방법.
  6. 제5항에 있어서, 상기 질소 생성물이 기체 질소 생성물 스트림으로서 추출되고; 상기 기체 질소 생성물스트림, 상기 냉동제 스트림, 및 상기 제1증발된 냉각제 스트림이 상기 제1 및 제2냉각제 스트림으로 간접적으로 열 교환되어 상기 제1 및 제2냉각제 스트림을 보조 냉각하는 방법.
  7. 제6항에 있어서, 상기 압축되고 정화된 공급공기 및 상기 제2증발된 냉각제 스트림으로의 간접 열 교환을 통하여 상기 기체 생성물 질소 스트림 및 상기 냉동제 스트림을 완전히 가온하고, 상기 제1증발된 냉각제 스트림을 부분적으로 가온하는 방법.
  8. 정류를 위한 적합한 온도로 압축되고 정화된 공급공기를 냉각하고, 제1증발된 냉각제 스트림을 부분적으로 가온하고, 제2증발된 냉각제 스트림을 상기 온도로 완전히 냉각하고, 압축되고 정화된 공급공기로부터 냉동제 스트림까지 간접적인 열이동을 위한 주요 열 교환수단; 상기 압축되고 정화된 공급공기를 수취하여, 질소가 풍부한 최상부 및 칼럼기부로서 산소가 풍부한 액체를 생성하는, 상기 주요 열 교환수단에 연결된 증류칼럼; 상기 질소가 풍부한 최상부로 구성되는 일부 이상의 질소가 풍부한 스트림을 응축시키고, 역류로서 상기 증류칼럼내에 생성된 일부 이상의 응축물을 도입하고, 제1 및 제2냉각제 스트림을 증발시켜 상기 제1 및 제2증발된 냉각재 스트림을 형성하기 위한 응축수단; 상기 증류칼럼에 연결되어 상기 제1냉각제 스트림이 상기 산소가 풍부한 액체로 구성되고 상기 제2냉각제 스트림이 상기 산소가 풍부한 액체의 함량보다 더 큰 질소 함량을 갖는 질소-함유 액체로 구성되는 상기 응축수단; 상기 주요 열 교환수단에 또한 연결되어 상기 제1증발된 냉각제 스트림이 그 내부에서 부분적으로 가온되는 상기 응축수단; 상기 제1 및 제2냉각제 스트림을 팽창시키는 밸브를 위해 상기 응축수단과 상기 증류칼럼 사이에 각각 위치한 제1 및 제2팽창밸브; 상기 질소가 풍부한 스트림의 또다른 부분으로부터 질소 생성물을 추출하기 위한 수단; 상기 냉동제 스트림을 형성하기 위해 작동의 수행으로 상기 제1증발된 냉각제 스트림을 팽창시키기 위한 상기 열 교환수단에 연결되는 팽창수단; 상기 팽창수단에 연결되어 상기 압축되고 정화된 공기가 상기 냉동제 스트림에 간접적으로 열 교환되는 상기 주요 열 교환수단; 상기 제2증발된 냉각제 스트림을 압축하기 위한 상기 응축수단에 연결된 압축기; 상기 주요 열 교환수단에 또한 연결되어 상기 제2증발된 냉각제 스트림이 그 내부에서 냉각되는 상기 압축기; 및 상기 제2증발된 냉각제 스트림을 상기 증류칼럼으로 수취한다음 상기 은도로 완전히 냉각하여 상기 질소 생성물의 재생을 증가시키기 위해 상기 기부 영역에서 상기 주요 열 교환수단에 또한 연결되는 상기 증류칼럼을 포함하는 질소를 생성하기 위한 장치.
    ※ 참고사항:최초출원 내용에 의하여 공개하는 것임.
KR1019960052443A 1995-11-07 1996-11-06 질소 생성을 위한 공기 분리방법 및 장치 KR100198352B1 (ko)

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US5582034A (en) 1996-12-10
AU6430596A (en) 1997-05-15
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CA2183511A1 (en) 1997-05-08
TR199600708A2 (tr) 1997-05-21
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AU704118B2 (en) 1999-04-15
CA2183511C (en) 1999-10-12
IL119056A0 (en) 1996-11-14
JP4057668B2 (ja) 2008-03-05
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TW360618B (en) 1999-06-11
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IL119056A (en) 2000-07-16
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CN1103438C (zh) 2003-03-19
ZA967298B (en) 1997-05-22
EP0773417A2 (en) 1997-05-14
CN1152108A (zh) 1997-06-18

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