KR950002804B1 - Process for manufacturing polyester fiber - Google Patents

Process for manufacturing polyester fiber Download PDF

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KR950002804B1
KR950002804B1 KR1019920008150A KR920008150A KR950002804B1 KR 950002804 B1 KR950002804 B1 KR 950002804B1 KR 1019920008150 A KR1019920008150 A KR 1019920008150A KR 920008150 A KR920008150 A KR 920008150A KR 950002804 B1 KR950002804 B1 KR 950002804B1
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roller
heat
temperature
speed
cooling chamber
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KR1019920008150A
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Korean (ko)
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KR930023498A (en
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하명직
주도홍
김덕환
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주식회사코오롱
하기주
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Abstract

spinning polyester yarn at a below 5000 m/min spinning speed; cooling in cooling bath of 400-500 mm length; heat-treating a heat pipe of 200-300≰C; passing ever the first godet roller; and heat-stabilizing in the second godet roller at the same speed as the of 1st godet roll at 100-200≰C. The process, the production reduces cost.

Description

폴리에스테르 섬유의 제조방법Method for producing polyester fiber

제1도는 본 발명의 공정개략도.1 is a process schematic diagram of the present invention.

본 발명은 폴리에스테르의 섬유를 5000m/min 이하의 방사속도로 제조함에 있어서, 별도로 연신을 하지않더라도 우수한 연신사의 물성을 얻을 수 있는 폴리에스테르 섬유의 제조방법에 관한 것이다.The present invention relates to a method for producing a polyester fiber that can obtain excellent properties of the drawn yarn even when not drawn separately in the production of polyester fibers at a spinning speed of 5000 m / min or less.

5000m/min 이하의 방사속도로 폴리에스테르 섬유를 제조하는 종래의 방법은 방사→냉각→오일링→제1고뎃롤러와 제2고뎃롤러사이에서 연신→권취하는 공정순서로 제조하는 것이었다.The conventional method for producing polyester fibers at a spinning speed of 5000 m / min or less has been made in the process sequence of spinning → cooling → stretching → winding between the first high speed roller and the second high speed roller.

상기 방법은 제1고뎃롤러와 제2고뎃롤러사이에서 연신을 하여야만 의류용에 적합한 원사물성을 얻을 수 있다.In this method, the yarn property suitable for clothing can be obtained only by stretching between the first roller and the second roller.

만약 연신을 하지 않으면 결정화 및 배향의 불균일로 인해 신도의 상승 및 U%(균제도)불량, 물성편차증대, 염반발생등의 문제를 일으킨다.If it is not stretched, it may cause problems such as increase of elongation, U% (evenness) defect, increase of property deviation, and occurrence of plaque due to non-uniformity of crystallization and orientation.

그러므로 연신은 필수불가결의 조건이며 이와같은 연신을 원활하게 하기 위해서는 제1고뎃롤러와 제2고뎃롤러의 속도차이를 두어 제1고뎃롤러의 온도를 폴리에스테르의 Tg 온도이상으로 유지시켜야만 한다.Therefore, the stretching is an indispensable condition, and in order to facilitate such stretching, the temperature difference between the first gourd roller and the second gourd roller should be kept above the Tg temperature of the polyester by the speed difference between the first gourd roller and the second gourd roller.

따라서, 종래의 방법은 제1고뎃롤러와 제2고뎃롤러간의 연신으로 인하여 설치면적이 증대되며, 생산성의 합리화를 이룰 수 없는 문제점을 갖고 있었다.Therefore, the conventional method has a problem that the installation area is increased due to the stretching between the first high roller and the second high roller, and the productivity cannot be rationalized.

본 발명은 5000m/min 이하의 방사속도로 폴리에스테르 섬유를 제조할 때 별도의 연신을 하지 않으므로서 설치면적을 줄일 수 있으며 우수한 연신사의 물성을 얻을 수 있고, 에너지절감과 생산성의 합리화를 이룰 수 있는 제조방법을 제공하는데 목적이 있는 바, 예시도면에 의하여 상세히 설명하면 다음과 같다.The present invention can reduce the installation area without obtaining a separate stretch when producing polyester fibers at a spinning speed of 5000m / min or less, obtain excellent stretched yarn properties, can achieve energy saving and rationalization of productivity It is an object of the present invention to provide a manufacturing method, which will be described in detail by way of example drawings.

본 발명은 5000m/min 히아의 방사속도로 폴리에스테르 섬유를 제조하는 통상의 방법에 있어서, 폴리에스테르 폴리머를 용융방사하고 길이가 400∼500mm인 냉각실에서 냉각시키고(온도 17℃, 풍속 초당 0.45m), 오일링한 후에 온도가 200∼300℃인 열파이프에서 열처리하며, 이어서 상온의 제1고뎃롤러를 통과시킨 다음에 제1고뎃롤러와 동일한 속도의 제2고뎃롤러에서 열고정시킴을 특징으로 한다.(제1도 참조)The present invention relates to a conventional method for producing polyester fibers at a spinning speed of 5000 m / min HIA, wherein the polyester polymer is melt spun and cooled in a cooling chamber of 400 to 500 mm in length (temperature 17 ° C., 0.45 m per second wind speed). After the oiling, heat treatment is performed in a heat pipe having a temperature of 200 to 300 ° C., followed by passing the first high roller in a room temperature, and then heat-setting the second high roller in the same speed as the first high roller. (See Figure 1.)

본 발명에서는 냉각실을 짧게 해서 급냉각을 시킨 다음 열파이프를 통과시킴으로서 결정화를 일정비율로 생성시키고 속도가 동일한 상온의 제1고뎃롤러와 100∼200℃의 제2고뎃롤러에서 열고정을 시켜서 안정한 폴리에스테르 연신사의 물성을 발현시켰다.In the present invention, the cooling chamber is shortened and quenched, and then passed through a heat pipe to produce crystallization at a constant rate. Physical properties of the polyester drawn yarn were expressed.

본 발명에서 냉각실의 길이를 통상의 냉각실의 길이인 760∼1000mm 보다 짧게 400∼500mm로 한 이유는 냉각실의 길이를 짧게 하여야만 급냉각이 되어 고화가 방지되며, 제1고뎃롤러의 속도(3,300∼4,800m/min)에 의하여 균일한 배향이 일어날 수 있도록 하기 위함이다.In the present invention, the length of the cooling chamber is shorter than 760 to 1000 mm, which is the length of a normal cooling chamber, to 400 to 500 mm. The reason for the cooling chamber is that the cooling chamber is shortened and the solidification is prevented. 3,300 to 4,800 m / min) to achieve a uniform orientation.

만일 냉각실의 길이가 400mm 미만이면 고화가 구금직하부에서 일어나 절사가 많이 일어나는 원인이 되며, 500mm를 초과하면 고화가 너무 많이 되어서 연신이 균일하게 이루어지지 않는다.If the length of the cooling chamber is less than 400mm, the solidification occurs in the lower portion of the detention, causing a lot of cutting occurs. If it exceeds 500mm, the solidification is too much, the stretching is not uniform.

본 발명에서 종래처럼 제1고뎃롤러를 고온으로 하지 않고 상온의 제l고뎃롤러를 사용하고 열파이프를 쓰는 이유는 고온의 제1고뎃롤러를 쓰면 순간적인 열처리로 인하여 열처리가 불균일하게 되어서 최종원사의 물성이 불균일해지기 때문이며, 열파이프로 인하여 열처리를 균일하게 할 수가 있고 상온의 제1고뎃롤러로 인하여 열처리의 안정화를 꾀할 수 있기 때이다.In the present invention, the reason for using the first high-pressure roller at room temperature without using the first high-pressure roller as the conventional one and using a heat pipe is that the high temperature of the first high-pressure roller causes the heat treatment to be uneven due to the instantaneous heat treatment. This is because it becomes uneven, and heat treatment can be made uniform by the heat pipe, and stabilization of heat treatment can be achieved by the first high heat roller at room temperature.

본 발명에서 유제처리는 오일링롤러 대신에 오일분사장치로 하는 것이 좋으며 2단계로 하는 것이 좋다. 본 발명에서, 상·하 오일분사장치의 간격을 30∼50mm로 하면 더욱 좋은 결과를 얻을 수 있다.In the present invention, the tanning treatment is preferably an oil spraying device instead of an oil ring roller, and is preferably two stages. In the present invention, better results can be obtained by setting the interval between the upper and lower oil injectors to 30 to 50 mm.

실시예 1Example 1

고유점도 0.65인 폴리에틸렌 테레프탈레이트 폴리머를 방사속도 3800m/min으로 방사하고 길이가 400mm인 냉각실에서 냉각시킨 후 오일분사방식으로 2단계에 걸쳐서 유제를 부여하고 온도가 280℃인 열파이프에서 열처리한 후 속도가 3800m/min으로 동일한 상온의 제1고뎃롤러와 120℃의 제2고뎃롤러에서 열고정시킨후 권취한 원사의 물성을 측정하여 표1에 나타내었다.After spinning a polyethylene terephthalate polymer with an intrinsic viscosity of 0.65 at a spinning speed of 3800 m / min and cooling it in a cooling chamber of 400 mm in length, impart an emulsion in two stages by oil spraying and heat treatment in a heat pipe with a temperature of 280 ° C. The physical properties of the wound yarn after heat-setting in the first gourd roller and the second gourd roller at 120 ° C. at the same temperature at 3800 m / min were measured and shown in Table 1.

실시예 2∼3, 비교예 1∼3Examples 2-3 and Comparative Examples 1-3

실시예 1과 동일한 방법으로 제조하되 방사속도, 냉각실의 길이, 열파이프온도, 제2고뎃롤러의 온도등을 표1과 같이 변경하여 제조하였다.Manufactured in the same manner as in Example 1, but was changed by changing the spinning speed, the length of the cooling chamber, the heat pipe temperature, the temperature of the second gourd roller as shown in Table 1.

비교예 4Comparative Example 4

고유점도 0.65인 폴리에틸렌 테레프탈레이트 폴리머를 방사속도 1350m/min으로 방사하고 길이가 800mm인 냉각실에서 냉각시킨후 오일링하고 속도가 1350m/min이고 온도가 89℃인 제1고뎃롤러와 속도가 4300m/min이고 온도가 120℃인 제2고뎃롤러에서 연신한 후 권취하였다.A polyethylene terephthalate polymer with an intrinsic viscosity of 0.65 was spun at a spinning speed of 1350 m / min, cooled in a cooling chamber of 800 mm in length, then oiled, a first gourd roller with a speed of 1350 m / min, and a temperature of 89 ° C. After stretching in a second roller roller having a min and a temperature of 120 ° C., it was wound up.

그 결과는 표1과 같다.The results are shown in Table 1.

[표 1]TABLE 1

* 강도편차는 시료를 20회 측정하여 그 편차가,* The intensity deviation is measured 20 times of the sample and the deviation is

0.10미만이면 : ○If less than 0.10: ○

0,10∼0.15이면 : △If 0,10 to 0.15: △

0.15이상이떤 : ×0.15 or more

Claims (1)

폴리에스테르사를 5000m/min 이하의 방사속도로 제조함에 있어서, 길이가 400∼500mm인 냉각실에서 냉각시키며, 온도가 200∼300℃인 열파이프에서 열처리하고, 이어서 상온의 제1고뎃롤러에 통과시긴 다음 제1고뎃롤러와 동일한 속도의 100∼200℃의 제 2고뎃롤러에서 열고정시킴을 특징으로 하는 폴리에스테르사의 제조방법.In producing polyester yarn at a spinning speed of 5000 m / min or less, it is cooled in a cooling chamber having a length of 400 to 500 mm, heat treated in a heat pipe having a temperature of 200 to 300 ° C., and then passed through a first gourd roller at room temperature. A process for producing polyester yarns characterized by heat setting in a second high speed roller at 100-200 ° C. at the same speed as the first high speed roller.
KR1019920008150A 1992-05-14 1992-05-14 Process for manufacturing polyester fiber KR950002804B1 (en)

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KR1019920008150A KR950002804B1 (en) 1992-05-14 1992-05-14 Process for manufacturing polyester fiber

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KR950002804B1 true KR950002804B1 (en) 1995-03-27

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