KR940019250A - Process for preparing oil-soluble antioxidants from degreasing rice bran - Google Patents

Process for preparing oil-soluble antioxidants from degreasing rice bran Download PDF

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Publication number
KR940019250A
KR940019250A KR1019930001779A KR930001779A KR940019250A KR 940019250 A KR940019250 A KR 940019250A KR 1019930001779 A KR1019930001779 A KR 1019930001779A KR 930001779 A KR930001779 A KR 930001779A KR 940019250 A KR940019250 A KR 940019250A
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South Korea
Prior art keywords
degreasing rice
emulsifier
extract
filtrate
parts
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KR1019930001779A
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Korean (ko)
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KR950010536B1 (en
Inventor
신재익
최수복
강우석
정성욱
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신춘호
주식회사 농심
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Priority to KR1019930001779A priority Critical patent/KR950010536B1/en
Publication of KR940019250A publication Critical patent/KR940019250A/en
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Publication of KR950010536B1 publication Critical patent/KR950010536B1/en

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B5/00Preserving by using additives, e.g. anti-oxidants
    • C11B5/0085Substances of natural origin of unknown constitution, f.i. plant extracts
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3472Compounds of undetermined constitution obtained from animals or plants
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2200/00Function of food ingredients
    • A23V2200/02Antioxidant
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2200/00Function of food ingredients
    • A23V2200/20Ingredients acting on or related to the structure
    • A23V2200/222Emulsifier

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Polymers & Plastics (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Edible Oils And Fats (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
  • Fats And Perfumes (AREA)

Abstract

본 발명은 a)탈지미강을 물과 에탄올의 혼합용매와 접촉시켜 추출을 행하여 탈지미강의 추출액을 얻은다음 이 추출액으로부터 잔사를 분리해내고 그 여액을 얻는 단계 ; b)상기 a)단계에서 얻은 탈지미강의 추출여액을 농축하는 단계로 이루어지는 항산화제의 제조방법에 있어서, 상기 a)단계에서의 혼합용매는 물0∼10용량%와 에탄올 90∼100용량%로 이루어진 것이며 ; 또한 상기 b)단계에서 얻은 농축된 탈지미강의 추출여액에 제1유화제를 첨가하고 이어 유화 안정보조제를 첨가하고 다음에 제2유화제를 첨가하여 유화하는 단계를 더욱 포함하는 것을 특징으로 하는 항산화제의 제조방법을 제공한다.The present invention comprises the steps of: a) extracting by contacting a degreasing rice steel with a mixed solvent of water and ethanol to obtain an extract of degreasing rice steel, and then separating the residue from the extract and obtaining the filtrate; b) In the method of producing an antioxidant comprising the step of concentrating the extraction filtrate of degreasing rice bran obtained in step a), the mixed solvent in step a) is 0 to 10% by volume of water and 90 to 100% by volume of ethanol It is done; In addition, the step of adding the first emulsifier to the extract filtrate of the concentrated degreasing rice obtained in step b), followed by adding an emulsifying eye aid, and then adding a second emulsifier to emulsify the antioxidant It provides a manufacturing method.

본 발명의 방법에 따라 제조되는 항산화제는 유화안정성 및 유용성이 우수하여 유지에 직접 첨가하여 사용할 수 있다.The antioxidant prepared according to the method of the present invention can be used by adding it directly to fats and oils with excellent emulsion stability and usability.

Description

탈지미강으로부터의 유용성 항산화제 제조방법Process for preparing oil-soluble antioxidants from degreasing rice bran

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

Claims (8)

a)탈지미강을 물과 에탄올의 혼합용매와 접촉시켜 추출을 행하여 탈지미강의 추출액을 얻은 다음 이추출액으로부터 잔사를 분리해내고 그 여액을 얻은 단계 ; b)상기 a)단계에서 얻은 탈지미강의 추출여액을농축하는 단계로 이루어지는 항산화제의 제조방법에 있어서, 상기 a)단계에서의 혼합용매는 물 0∼10용량%와 에탄올 90∼100용량%로 이루어진 것이며 ; 또한 상기 b)단계에서 얻은 농축된 탈지미강의 추출여액에 제1유화제를 첨가하고 이어 유화 안정보조제를 첨가하고 다음에 제2유화제를 첨가하여 유화하는 단계를 더욱 포함하는 것을 특징으로 하는 항산화제의 제조방법.a) extracting by contacting degreasing rice with a mixed solvent of water and ethanol to obtain an extract of degreasing rice, separating the residue from the extract and obtaining the filtrate; b) In the method of producing an antioxidant comprising the step of concentrating the extraction filtrate of degreasing rice bran obtained in step a), the mixed solvent in step a) is 0 to 10% by volume of water and 90 to 100% by volume of ethanol It is done; In addition, the step of adding the first emulsifier to the extract filtrate of the concentrated degreasing rice obtained in step b), followed by adding an emulsifying eye aid, and then adding a second emulsifier to emulsify the antioxidant Manufacturing method. 제 1 항에 있어서, 제 1 유화제는 HLB 값이 4.0 내지 10.5이며 ; 지방산기로는 올레산기를 갖는 모노 또는 폴리글리세린 지방산에스테르인 것을 특징으로 하는 방법.The method of claim 1, wherein the first emulsifier has an HLB value of 4.0 to 10.5; The fatty acid group is a mono or polyglycerol fatty acid ester having an oleic acid group. 제 1 항 또는 제 2 항에 있어서, 제 1 유화제는 상기의 농축된 탈지미강의 추출여액 100중량부에 대하여150 내지 200중량부가 첨가되는 것을 특징으로 하는 방법.The method according to claim 1 or 2, wherein the first emulsifier is added in an amount of 150 to 200 parts by weight based on 100 parts by weight of the extract filtrate of the concentrated degreasing rice bran. 제 1 항에 있어서, 유화안정보조제는 프로플렌 글리콜, 소르비톨, 에탄올, 엠시티인 것을 특징으로 하는 방법.The method according to claim 1, wherein the emulsion stabilizer is propene glycol, sorbitol, ethanol, emcity. 제 1 항 또는 제 4 항에 있어서, 유와안정보조제는 상기의 농축된 탈지미강의 추출여액의 100중량부에 대하여 100 내지 200중량부가 첨가되는 것을 특징으로 하는 방법.5. The method according to claim 1 or 4, wherein the oil and ophthalmic preparation is added in an amount of 100 to 200 parts by weight based on 100 parts by weight of the extract filtrate of the concentrated degreasing rice bran. 제 1 항에 있어서, 제2 유화제는 HLB 값이 1 내지 2이고 ; 지방산기로는 리시놀레산기를 가지며 ; 지방산의 축합도는 4∼8인 폴리글리세린 축합 지방산 에스테르인 것을 특징으로 하는 방법.The method of claim 1, wherein the second emulsifier has an HLB value of 1 to 2; Fatty acid group has a ricinoleic acid group; The degree of condensation of fatty acids is 4 to 8 polyglycerin condensed fatty acid esters. 제 6 항에 있어서, 상기 플리글리세린 축합 지방산 에스테르의 지방산기의 축합도는 6인 것을 특징으로하는 방법.7. The method according to claim 6, wherein the degree of condensation of the fatty acid groups of the polyglycerol condensed fatty acid ester is six. 제 1 항, 제 6 항 또는 제 7 항에 있어서, 제 2 유화제는 상기의 농축된 탈지미강의 추출여액 100중량부에 대하여 150 내지 200중량부가 첨가되는 것을 특징으로 하는 방법.8. The method according to claim 1, 6 or 7, wherein the second emulsifier is added in an amount of 150 to 200 parts by weight based on 100 parts by weight of the extract filtrate of the concentrated degreasing rice. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019930001779A 1993-02-10 1993-02-10 Antioxidant making method from fat-removed rice shell KR950010536B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019930001779A KR950010536B1 (en) 1993-02-10 1993-02-10 Antioxidant making method from fat-removed rice shell

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Application Number Priority Date Filing Date Title
KR1019930001779A KR950010536B1 (en) 1993-02-10 1993-02-10 Antioxidant making method from fat-removed rice shell

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KR940019250A true KR940019250A (en) 1994-09-14
KR950010536B1 KR950010536B1 (en) 1995-09-19

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