KR900017945A - Glass lining method by sol-gel method Repairing method and repairing device for the damaged part of the lining glass layer - Google Patents

Glass lining method by sol-gel method Repairing method and repairing device for the damaged part of the lining glass layer Download PDF

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KR900017945A
KR900017945A KR1019900007592A KR900007592A KR900017945A KR 900017945 A KR900017945 A KR 900017945A KR 1019900007592 A KR1019900007592 A KR 1019900007592A KR 900007592 A KR900007592 A KR 900007592A KR 900017945 A KR900017945 A KR 900017945A
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glass
agent
repair
sol
layer
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KR930006323B1 (en
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다쓰오 하라
고오이치 와다
시게오 우에가키
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가와구치 다다시
신코오판텍 가부시키가이샤
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C27/00Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
    • C03C27/06Joining glass to glass by processes other than fusing
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23DENAMELLING OF, OR APPLYING A VITREOUS LAYER TO, METALS
    • C23D13/00After-treatment of the enamelled articles
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/02Surface treatment of glass, not in the form of fibres or filaments, by coating with glass
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208Oxides, e.g. ceramics
    • C23C18/1212Zeolites, glasses
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/122Inorganic polymers, e.g. silanes, polysilazanes, polysiloxanes
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1225Deposition of multilayers of inorganic material
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229Composition of the substrate
    • C23C18/1241Metallic substrates
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125Process of deposition of the inorganic material
    • C23C18/1254Sol or sol-gel processing
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125Process of deposition of the inorganic material
    • C23C18/1262Process of deposition of the inorganic material involving particles, e.g. carbon nanotubes [CNT], flakes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/49718Repairing
    • Y10T29/49746Repairing by applying fluent material, e.g., coating, casting

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Ceramic Engineering (AREA)
  • Nanotechnology (AREA)
  • Dispersion Chemistry (AREA)
  • Laminated Bodies (AREA)
  • Glass Compositions (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Resistance Heating (AREA)
  • Joining Of Glass To Other Materials (AREA)

Abstract

내용 없음No content

Description

졸-겔법에 의한 글래스 라이닝 강철제 기기의 라이닝 유리층의 파손부분의 보수방법 및 보수장치Repairing method and repairing device for broken part of lining glass layer of glass-lined steel machine by sol-gel method

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

제1도는 만곡 보수부분의 보수상황을 나타내는 종단 측면도이다. 제2도는 소지강과 라이닝 유리 각각의 온도(횡축)에 대한 재료 신장율(종축)의 관계를 나타내는 열팽창 곡선도이다. 제3도는 보수층의 중첩 형성에 의한 라이닝 유리층을 보수, 완료했을 때의 상태를 나타내는 종단 측면도이다.1 is a longitudinal side view showing the repair status of the curved repair portion. 2 is a thermal expansion curve showing the relationship between the material elongation (vertical axis) with respect to the temperature (horizontal axis) of each of the base steel and the lining glass. 3 is a longitudinal side view showing the state when the lining glass layer by the overlap formation of the repair layer is repaired and completed.

Claims (12)

졸-겔법에 의해 소지강과 밀착하는 유리를 합성하는 제1보수제를 파손부분에 도포하고, 제1보수제를 가열하여 유리질 제1보수층을 형성하는 제1공정: 졸-겔법에 의해 유리를 합성하는 무기질 충전제를 함유하는 제2보수제를 제1보수층 위에 도포하고, 제2보수제를 가열하여 유리질 제2보수층을 형성하는 제2공정: 및 졸-겔법에 의해 유리를 합성하는 액상 보수제를 제2보수층 위에 도포하고, 액상 보수제를 가열하여 공극이 밀봉된 제2보수층을 형성하는 제3공정을 포함함을 특징으로 하며 글래스 라이닝제 기기의 라이닝 유리층의 파손부분을 보수하는 방법.The first step of applying a first repair agent for synthesizing the glass in close contact with the base steel by the sol-gel method, and heating the first repair agent to form a glassy first repair layer: an inorganic material for synthesizing the glass by the sol-gel method A second step of applying a second repair agent containing a filler on the first repair layer, and heating the second repair agent to form a glassy second repair layer: and applying a liquid repair agent for synthesizing the glass by the sol-gel method onto the second repair layer. And a third step of heating the liquid repair agent to form a second repair layer in which the voids are sealed, and repairing the broken portion of the lining glass layer of the glass lining agent device. 제1항에 있어서, 공극이 밀봉된 유리질 제2보수층 위에 제2보수제를 도포하고, 제2보수제를 가열하여 유리질 보수층을 형성하는 공정 및 졸-겔법에 의해 유리를 합성하는 액상 보수제를 유리질 보수층위에 도포하고, 액상 보수제를 가열하여 공극이 밀봉된 유리질 보수층을 형성하는 공정을 반복하는 공정을 포함하는 방법.The liquid repairing agent according to claim 1, wherein the second repairing agent is applied on the glassy second repairing layer sealed with voids, and the second repairing agent is heated to form a glassy repairing layer, and a liquid repairing agent for synthesizing the glass by the sol-gel method is placed on the glassy repairing layer. Applying, and repeating the step of heating the liquid repair agent to form a glassy repair layer in which the voids are sealed. 제1항에 있어서, 제1보수제가 졸-겔법에 의해 인산염계 유리를 합성하는 방법.The method of claim 1, wherein the first repair agent synthesizes the phosphate-based glass by the sol-gel method. 제1항에 있어서, 제2보수제가 졸-겔법에 의해 규산염계 유리를 합성하는 방법.The method of claim 1, wherein the second repair agent synthesizes the silicate-based glass by the sol-gel method. 제1항에 있어서, 제2보수제가 졸-겔법에 의해 인산염계 유리를 합성하는 방법.The method of claim 1, wherein the second repair agent synthesizes the phosphate-based glass by the sol-gel method. 제1항에 있어서, 제2보수제가 졸-겔법에 의해 Na2O, ZrO2,SiO2계 다성분계 유리를 합성하는 방법.The method of claim 1, wherein the second repair agent synthesizes Na 2 O, ZrO 2 , SiO 2 based multicomponent glass by a sol-gel method. 제1항에 있어서, 제2보수제에 함유된 무기질 충전제가 라이닝 유리와 근사한 열팽창계수를 갖는 무기질분말인 방법.The method of claim 1 wherein the inorganic filler contained in the second repair agent is an inorganic powder having a coefficient of thermal expansion close to that of the lining glass. 제7항에 있어서, 무기질 분말이 라이닝 유리를 구성하는 유리 분말과 동일한 재질인 방법.8. The method of claim 7, wherein the inorganic powder is the same material as the glass powder constituting the lining glass. 제1항에 있어서, 제2공정에 선행하여 라이닝 유리층의 파손부분의형상에 따라 무기질 시트재를 충전시키는 공정을 포함하는 방법.A method according to claim 1, comprising the step of filling the inorganic sheet material in accordance with the shape of the broken portion of the lining glass layer prior to the second step. 제1항에 있어서, 제1보수층 위에 졸-겔법에 의해 유리를 합성하는, 입자 직경이 1㎛ 이하인 무기질 분말을 함유하는 보수제를 도포하고, 입자 직경이 1㎛이하인 무기질 분말을 함유하는 보수제를 가열하는 공정을 포함하는 방법.The water-retaining agent of Claim 1 which apply | coats the water-retaining agent containing the inorganic powder whose particle diameter is 1 micrometer or less, and synthesize | combines glass by the sol-gel method on a 1st water-retaining layer, and heats the water-retaining agent containing the inorganic powder whose particle diameter is 1 micrometer or less Method comprising the step of doing. 제1항에 있어서 졸-겔법에서 가열온도가 300내지 350℃인 방법.The method according to claim 1, wherein the heating temperature is 300 to 350 ° C. in the sol-gel method. 한쪽면에 오목부분을 갖는 유연성 단열재 본체(24,34), 오목부분에 부착된 전기 히터(26), 본체의 오목부분 근처에 부착된 자석(34), 본체 외축을 둘러싸는 석영 유리포(28), 오목부분 속에 위치하는 온도감지기(25)및 감지기(25)와 히터(26)에 접속되어 히터의 온도를 자동조절하는 온도조절기(33)를 포함하는 글래스 라이닝 강철의 라이닝 유리층 파손부분의 가열장치.Flexible heat insulating material bodies 24 and 34 having recesses on one side, electric heaters 26 attached to the recesses, magnets 34 attached near the recesses of the body, and quartz glass cloth 28 surrounding the outer shaft of the body. ), The temperature sensor 25 located in the recessed portion of the glass-lining steel breakage portion of the glass-lining steel, including a temperature controller (25) connected to the sensor (25) and the heater (26) to automatically adjust the temperature of the heater. Heating device. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019900007592A 1989-05-26 1990-05-25 Method and device for repairing damaged part of lining glass layer of glass-lined steel equipment KR930006323B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP134,255 1989-05-26
JP1-134255 1989-05-26
JP1134255A JP2796123B2 (en) 1989-05-26 1989-05-26 Method and apparatus for repairing localized damage to the lining glass layer of glass-lined steel equipment

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KR900017945A true KR900017945A (en) 1990-12-20
KR930006323B1 KR930006323B1 (en) 1993-07-14

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US (1) US5053251A (en)
EP (1) EP0407027B1 (en)
JP (1) JP2796123B2 (en)
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EP0407027B1 (en) 1995-04-19
KR930006323B1 (en) 1993-07-14
JP2796123B2 (en) 1998-09-10
EP0407027A3 (en) 1991-01-30
DE69018715D1 (en) 1995-05-24
DE69018715T2 (en) 1995-09-07
EP0407027A2 (en) 1991-01-09
JPH032386A (en) 1991-01-08
US5053251A (en) 1991-10-01

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