KR860001913A - Wax-free stock composition based on polyvinyl alcohol - Google Patents

Wax-free stock composition based on polyvinyl alcohol Download PDF

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KR860001913A
KR860001913A KR1019850005963A KR850005963A KR860001913A KR 860001913 A KR860001913 A KR 860001913A KR 1019850005963 A KR1019850005963 A KR 1019850005963A KR 850005963 A KR850005963 A KR 850005963A KR 860001913 A KR860001913 A KR 860001913A
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ethylene oxide
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alcohol
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KR920009254B1 (en
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아아서 배슬로우 도널드 (외 1)
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도늘드 에이 호우즈
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
    • D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

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폴리비닐알콜을 기제로 하는 왁스-비함유 호제 조성물Wax-free stock composition based on polyvinyl alcohol

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음As this is a public information case, the full text was not included.

Claims (20)

필수적으로 하기 (a)-(f)로 구성되는 조성물:(a) 폴리비닐알콜, 비닐알콜/메타크릴산 메틸 공중합체 및 메타크릴산메틸 이외의 용해 공단량체를 함유하는 폴리비닐알콜로 이루어지는 군에서 선택되며, 비누화 값이 약 1-160이고 4% 용액점도가 20℃하에 약 3-70m㎩.s인 비닐알콜 중합체 약 45.5-99.9중량%, (b) 산화에틸렌의 평균 함량이 약 1-7단위이고 알콜의 평균 탄소함량이 약 8-18(탄소원자)인, 측쇄 알콜 또는 측쇄 알콜 혼합물의 액상 비이온성 저-산화에틸렌 부가물 약 0.1-3중량%; (c) 전분 0-49.9중량%; (d) 분자량(평균수)이 약 200-800인 산화에틸렌 올리고모 0-약 5중량%; (e) 카르복시메틸 셀룰로오즈 0-약 49.9중량%; (f) 선형 알콜 또는 선형 알콜 혼합물(평균 탄소함량; 약8-18단위)의 저-산화에틸렌 부가물(산화에틸렌의 평균 함량:약1-7단위) 및 선형 또는 측쇄 알콜(평균 탄소 함량:약8-18단위)의 중-내지 고-산화에틸렌 부가물(산화에틸렌의 평균 함량:약3-40단위)로 이루어지는 군에서 선택되는 적어도 1개의 보조 산화에틸렌 부가물 0-약 1중량%(여기서, 전분과 카르복시메틸 셀룰로 오즈의 중량의 합은 비닐알콜 중합체의 중량을 초과하지 않아야 한다.)A composition consisting essentially of the following (a)-(f): (a) A group consisting of polyvinyl alcohol, vinyl alcohol / methyl methacrylate copolymer, and polyvinyl alcohol containing a dissolved comonomer other than methyl methacrylate About 45.5-99.9% by weight of a vinyl alcohol polymer having a saponification value of about 1-160 and a 4% solution viscosity of about 3-70 mPa.s at 20 ° C., (b) an average content of ethylene oxide of about 1- About 0.1-3% by weight of a liquid nonionic low-ethylene oxide adduct of a branched alcohol or branched alcohol mixture, which is 7 units and has an average carbon content of alcohol of about 8-18 (carbon atoms); (c) 0-49.9% by weight starch; (d) 0- about 5% by weight ethylene oxide oligomo having a molecular weight (average number) of about 200-800; (e) 0-about 49.9 weight percent of carboxymethyl cellulose; (f) low-ethylene oxide adducts (average carbon content: about 1-7 units) of linear alcohols or linear alcohol mixtures (average carbon content; about 8-18 units) and linear or branched alcohols (average carbon content: 0-about 1% by weight of at least one secondary ethylene oxide adduct selected from the group consisting of about 8-18 units) of medium to high-ethylene oxide adducts (average content of ethylene oxide: about 3-40 units) Here, the sum of the weight of starch and carboxymethyl cellulose should not exceed the weight of the vinyl alcohol polymer.) 제1항에 있어서, 약 3-70m㎩.s의 점도를 갖는 완전 가수분해된 폴리비닐알콜, 약 3-60m㎩.s의 점도를 갖고 약 3.5-6중량%의 공중합 메타크릴산메틸 공단량체를 함유하는 완전가수분해된 비닐알콜/메타크릴산메틸 공중합체, 약 3-60m㎩.s의 점도를 갖고 약 4-12몰%의 초산비닐을 함유하는 부분 가수분해된 폴리비닐 알콜, 약3-70m㎩.s의 점도를 갖고 메틸아크릴레이트 및 메틸 히드로겐 말레이트로 부터 선정되는 용해 공단량체를 함유하는 폴리비닐알콜 및 상기한 비닐알콜 중합체의 혼합물로 이루어지는 군에서 비늘알콜 중합체가 선택되는 조성물.The fully hydrolyzed polyvinyl alcohol having a viscosity of about 3-70 mPa.s, the copolymer of methyl methacrylate comonomer having a viscosity of about 3-60 mPa.s and about 3.5-6% by weight. Fully hydrolyzed vinyl alcohol / methyl methacrylate copolymer containing, partially hydrolyzed polyvinyl alcohol having a viscosity of about 3-60 mPa.s and containing about 4-12 mole percent vinyl acetate, about 3 A composition wherein the scale alcohol polymer is selected from the group consisting of a mixture of the above-described vinyl alcohol polymer and polyvinyl alcohol having a viscosity of -70 mPa.s and containing a dissolving comonomer selected from methyl acrylate and methyl hydrogen malate. . 제1항에 있어서, 비닐 알콜 중합체의 양이 약 63-99.8중량%, 산화에틸렌 부가물의 양이 약 0.2-1중량%, 전분의 양이 0-약 33중량%, 산화에틸렌 올리고머의 양이 0-약 3중량%, 카르복시 메틸 셀룰로오지의 양이 0-약 33중량%이고 상기 산화에틸렌 부가물의 산화에틸렌 평균 함량이 약 2-5이며 알콜의 평균 탄소 함량이 약 10-15(탄소원자)인 조성물.The method of claim 1, wherein the amount of vinyl alcohol polymer is about 63-99.8% by weight, the amount of ethylene oxide adduct is about 0.2-1% by weight, the amount of starch is 0-about 33% by weight, and the amount of ethylene oxide oligomer is 0 About 3% by weight, the amount of carboxy methyl cellulose is 0- about 33% by weight, the average ethylene oxide content of the ethylene oxide adduct is about 2-5, and the average carbon content of the alcohol is about 10-15 (carbon atoms) Phosphorus composition. 제1항에 있어서, 비닐알콜 중합체의 양이 약 72.7-99.6중량%, 산화에틸렌 부가물의 양이 약 0.4-0.8중량%, 전분의 양이 0-약 25중량%, 산화에틸렌 올리고머의 양이 0-약 1.5중량%, 카르복시메틸 셀룰로오즈의 양이 0-약 25중량%이고, 상기 산화에틸렌 부가물의 산화에틸렌 평균 함량이 약 3이며, 알콜의 평균 탄소 함량이 약 13(탄소원자)인 조성물.The method of claim 1, wherein the amount of vinyl alcohol polymer is about 72.7-99.6 wt%, the amount of ethylene oxide adduct is about 0.4-0.8 wt%, the amount of starch is 0-about 25 wt%, the amount of ethylene oxide oligomer is 0 About 1.5% by weight, the amount of carboxymethyl cellulose is from 0 to about 25% by weight, the average ethylene oxide content of the ethylene oxide adduct is about 3, and the average carbon content of the alcohol is about 13 (carbon atoms). 필수적으로 하기 (a)-(f)로 구성되는 조성물:(a) 폴리비닐알콜 및 비닐알콜/메타크릴산 메틸 공중합체 및 메타크릴산메틸 이외의 용해 공단량체를 함유하는 폴리비닐 알콜로 이루어지는 군에서 선택되며, 비누화값이 약 1-160이고 20℃에서의 4% 용액점도가 약 3-70m㎩.s인 비닐알콜 중합체 약 45-90중량%; (b) 산화에틸렌의 평균 함량이 약 2-7단위이고 알콜의 평균 탄소함량이 약 8-18(탄소원자)인, 측쇄 알콜 또는 측쇄 알콜 혼합물의 액상 비이온성 저-산화에틸렌 부가물 약 10-55중량%; (c) 전분 약 0-45중량%; (d) 분자량(평균수)이 약 200-800인 산화에틸렌 올리고머 0-약 45중량%; (e) 카르복시메틸 셀룰로오즈 0-약 45%중량%; (f) 선형 알콜 또는 선형 알콜 혼합물(평균 탄소함량: 약 8-18단위)의 저-산화에틸렌 부가물(산화에틸렌의 평균 함량; 약 1-7단위) 및 선형 또는 측쇄 알콜(평균 탄소 함량; 약 8-18단위)의 중-내지 고-산화에틸렌 부가물(산화에틸렌의 평균 함량: 약 8-40단위)로 이루어지는 군에서 선택된 보조 산화에틸렌 부가물 0-약 45중량%.A composition consisting essentially of the following (a)-(f): (a) A group consisting of polyvinyl alcohol and a vinyl alcohol / methyl methacrylate copolymer and polyvinyl alcohol containing a dissolved comonomer other than methyl methacrylate Selected from about 45-90 weight percent vinyl alcohol polymer having a saponification value of about 1-160 and a 4% solution viscosity at 20 ° C. of about 3-70 mPa · s; (b) liquid nonionic low-ethylene oxide adducts of branched or branched alcohol mixtures having an average content of ethylene oxide of about 2-7 units and an average carbon content of alcohol of about 8-18 carbon atoms. 55 wt%; (c) about 0-45 weight percent starch; (d) 0-about 45 weight percent of an ethylene oxide oligomer having a molecular weight (average number) of about 200-800; (e) 0-about 45% by weight carboxymethyl cellulose; (f) low-ethylene oxide adducts (average content of ethylene oxide; about 1-7 units) and linear or branched chain alcohols (average carbon content) of linear alcohols or linear alcohol mixtures (average carbon content: about 8-18 units); 0 to about 45 weight percent secondary ethylene oxide adduct selected from the group consisting of about 8-18 units) of medium to high ethylene oxide adducts (average content of ethylene oxide: about 8-40 units). 제5항에 있어서, 약 3-70m㎩.s의 점도를 갖는 완전 가수분해된 폴리비닐알콜, 약 3-60m㎩.s의 점도를 갖고 약 3.5-6중량%의 공중합 메타크릴산 메틸 공단량체를 함유하는 완전 가수분해된 비닐알콜/메타크릴산메틸 공중합체, 약 3-60m㎩.s의 점도를 갖고 약 4-12몰%의 초산비닐을 함유하는 부분 가수분해된 폴리비닐알콜, 약 3-70m㎩.s의 점도를 가지며 메틸아크릴레이트 및 메틸 히드로겐말레이트로 부터 선정되는 용해 공단량체를 함유하는 폴리비닐알콜 및 상기 비닐알콜 중합체의 혼합물로 이루어지는 군으로 부터 비닐알콜 중합체가 선택되는 조성물.6. The fully hydrolyzed polyvinyl alcohol having a viscosity of about 3-70 mPa.s, the copolymer of methyl methacrylate comonomer having a viscosity of about 3-60 mPa.s and about 3.5-6% by weight. Fully hydrolyzed vinyl alcohol / methyl methacrylate copolymer containing, partially hydrolyzed polyvinyl alcohol having a viscosity of about 3-60 mPa.s and containing about 4-12 mol% vinyl acetate, about 3 A vinyl alcohol polymer is selected from the group consisting of polyvinyl alcohol and a mixture of said vinyl alcohol polymers having a viscosity of -70 mPa.s and containing a dissolving comonomer selected from methyl acrylate and methyl hydrogen maleate. 제5항에 있어서, 비닐 알콜 중합체의 양이 약 45-70중량%, 산화에틸렌 부가물의 양이 약 30-55중량%, 전분의 양이 0-약25중량%, 산화에틸렌 올리고머의 양이 0-약25중량%, 카르복시메틸 셀룰로오즈의 양이 0-약 25중량%이고, 상기 산화에틸렌 부가물의 산화에틸렌 평균함량이 약 3-5이며 알콜의 평균 탄소 함량이 약 10-19(탄소원자)인 조성물.The method of claim 5, wherein the amount of vinyl alcohol polymer is about 45-70% by weight, the amount of ethylene oxide adduct is about 30-55% by weight, the amount of starch is 0-about 25% by weight, and the amount of ethylene oxide oligomer is 0 About 25% by weight, the amount of carboxymethyl cellulose is from 0 to about 25% by weight, the average ethylene oxide content of the ethylene oxide adduct is about 3-5 and the average carbon content of alcohol is about 10-19 (carbon atoms) Composition. 제5항에 있어서, 비닐알콜 중합체의 양이 약 50-60중량%, 산화에틸렌 부가물의 양이 약 40-50중량%, 전분의 양이 0-약 5중량%, 산화에틸렌 올리고머의 양이 0-약 5중량%, 카르복시메틸 셀룰로오즈의 양이 0-약 5중량%이고, 상기 산화에틸렌 부가물의 산화에틸렌 평균 함량이 약 3이며 알콜의 평균 탄소함량이 약 13(탄소원자)인 조성물.The method of claim 5, wherein the amount of vinyl alcohol polymer is about 50-60% by weight, the amount of ethylene oxide adduct is about 40-50% by weight, the amount of starch is 0-about 5% by weight, and the amount of ethylene oxide oligomer is 0 About 5% by weight, the amount of carboxymethyl cellulose is from 0 to about 5% by weight, the average ethylene oxide content of the ethylene oxide adduct is about 3 and the average carbon content of the alcohol is about 13 (carbon atoms). 약 2-20중량%의 고체함량을 갖는, 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물로 구성되는 왁스-비함유 수성 호제 용액.A wax-free aqueous appeal solution consisting of the composition of claims 1, 2, 3 or 4 having a solids content of about 2-20% by weight. 약 5-15중량%의 고체 함량을 갖는, 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물로 구성되는 왁스-비함유 수성 호제 용액.A wax-free aqueous appeal solution composed of the composition of claims 1, 2, 3 or 4 having a solids content of about 5-15% by weight. 약 7-12중량%의 고체 함량을 갖는, 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물로 구성되는 왁스-비함유 수성 호제 용액.A wax-free aqueous appeal solution consisting of the composition of claims 1, 2, 3 or 4 having a solids content of about 7-12% by weight. 고체함량이 약 2-20중량%이며 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물로 구성되는 왁스-비함유 수용액을 사용하여 방적실에 풀을 먹이는 방법.A method of feeding grass to a spinning chamber using a wax-free aqueous solution comprising about 2-20% by weight of solids and comprising the composition of claims 1, 2, 3 or 4. 고체함량이 약 5-15중량%이며 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물로 구성되는 왁스-비함유 수용액을 사용하여 방적실에 풀을 먹이는 방법.A method of feeding grass to a spinning chamber using a wax-free aqueous solution comprising about 5-15% by weight of solids and comprising the composition of claims 1, 2, 3 or 4. 고체함량이 약 7-12중량%이며 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물로 구성되는 왁스-비함유 수용액을 사용하여 방적실에 풀을 먹이는 방법.A method of feeding grass to a spinning chamber using a wax-free aqueous solution comprising about 7-12% by weight of solids and comprising the composition of claims 1, 2, 3 or 4. 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물의 왁스-비함유 보호용 표면 코우팅을 갖는 방적실로 구성되는 풀먹인 신.A glued sin consisting of a spinning chamber having a wax-free protective surface coating of the composition of claims 1, 2, 3 or 4. 면 및 폴리에스테르/면 방적실로 부터 선택되며 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물의 왁스-비함유 보호용 표면 코우팅을 갖는 방적실로 구성되는 풀먹인 실.A threaded yarn selected from cotton and polyester / cotton yarn and consisting of a yarn having a wax-free protective surface coating of the composition of claims 1, 2, 3 or 4. 65/35,50/50 및 40/60 폴리에스테르/면 방적실로 부터 선택되며 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물의 왁스-비함유 보호용 표면 코우팅을 갖는 방적실로 구성되는 풀먹인 실.Spinning yarns selected from 65 / 35,50 / 50 and 40/60 polyester / cotton spinning yarns having wax-free protective surface coatings of the compositions of claims 1, 2, 3 or 4. A grass fed thread composed of threads. 65/35,50/50 및 40/60 폴리에스테르/면 방적실로 부터 선택되며 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물의 왁스-비함유 보호용 표면 코우팅을 갖는 방적실로 구성되는 풀먹인 실로부터 제조된 직물.Spinning yarns selected from 65 / 35,50 / 50 and 40/60 polyester / cotton spinning yarns having wax-free protective surface coatings of the compositions of claims 1, 2, 3 or 4. Fabrics made from glued yarns consisting of threads. 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물의 왁스-비함유 보호용 표면 코우팅을 갖는 방적실로 구성되는 풀먹인 실로 부터 제조된 직물.A fabric made from glued yarns consisting of yarns having a wax-free protective surface coating of the composition of claims 1, 2, 3 or 4. 면 및 폴리에스테르/면 방적실로 부터 선택되며 청구범위 제1항, 제2항, 제3항 또는 제4항의 조성물의 왁스-비함유 보호용 표면 코우팅을 갖는 방적실로 구성되는 풀먹인 실로 부터 제조된 직물.Selected from cotton and polyester / cotton spun yarn and made from glued yarns consisting of a spun yarn having a wax-free protective surface coating of the composition of claims 1, 2, 3 or 4. textile. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019850005963A 1984-08-20 1985-08-19 Polyvinyl alcohol based wax-free size composition KR920009254B1 (en)

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US4845140A (en) * 1986-07-07 1989-07-04 Air Products And Chemicals, Inc. Waxless polyvinyl alcohol size composition
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