KR860000829B1 - 나일론 6 올리고머로 부터 카프로락탐을 회수하는 방법 - Google Patents
나일론 6 올리고머로 부터 카프로락탐을 회수하는 방법 Download PDFInfo
- Publication number
- KR860000829B1 KR860000829B1 KR1019810003431A KR810003431A KR860000829B1 KR 860000829 B1 KR860000829 B1 KR 860000829B1 KR 1019810003431 A KR1019810003431 A KR 1019810003431A KR 810003431 A KR810003431 A KR 810003431A KR 860000829 B1 KR860000829 B1 KR 860000829B1
- Authority
- KR
- South Korea
- Prior art keywords
- caprolactam
- water
- fed
- wash water
- concentrated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/12—Preparation of lactams by depolymerising polyamides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US187,864 | 1980-09-17 | ||
| US06/187,864 US4311642A (en) | 1980-09-17 | 1980-09-17 | Recovery of caprolactam from nylon 6 oligomers |
| US187864 | 1988-04-29 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR830007546A KR830007546A (ko) | 1983-10-21 |
| KR860000829B1 true KR860000829B1 (ko) | 1986-07-02 |
Family
ID=22690811
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019810003431A Expired KR860000829B1 (ko) | 1980-09-17 | 1981-09-15 | 나일론 6 올리고머로 부터 카프로락탐을 회수하는 방법 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4311642A (cg-RX-API-DMAC7.html) |
| EP (1) | EP0048340B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JPS5781458A (cg-RX-API-DMAC7.html) |
| KR (1) | KR860000829B1 (cg-RX-API-DMAC7.html) |
| CA (1) | CA1157020A (cg-RX-API-DMAC7.html) |
| DE (1) | DE3173977D1 (cg-RX-API-DMAC7.html) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4767503A (en) * | 1983-08-29 | 1988-08-30 | Allied Corporation | Removal of light impurities from caprolactam by distillation with water |
| US5169870A (en) * | 1991-06-21 | 1992-12-08 | Basf Corporation | Reclaiming ε-caprolactam from nylon 6 carpet |
| DE4211609A1 (de) * | 1991-08-30 | 1993-03-04 | Bayer Ag | Gewinnung von caprolactam durch thermische spaltung von polyamid 6 |
| DE4216848A1 (de) * | 1992-05-21 | 1993-11-25 | Basf Ag | Verfahren zur Rückgewinnung von Caprolactam aus Polycaprolactam |
| EP0608454B1 (de) * | 1993-01-28 | 1997-08-13 | POLYMER ENGINEERING GmbH | Verfahren und Vorrichtung zur Herstellung von Polyamid 6 aus Polyamid-Abfällen |
| US5457197A (en) * | 1994-04-08 | 1995-10-10 | Alliedsignal Inc. | Monomer recovery from multi-component materials |
| US5495015A (en) * | 1994-12-12 | 1996-02-27 | Basf Aktiengesellschaft | Process for producing caprolactam through hydrolytic cleavage of molten polycaprolactam |
| US5656757A (en) * | 1995-08-10 | 1997-08-12 | Alliedsignal Inc. | Monomer recovery from multi-component materials |
| DE19648747A1 (de) * | 1996-11-25 | 1998-05-28 | Basf Ag | Verfahren zur Rückgewinnung von Caprolactam und seinen Oligomeren aus wässrigen Polycaprolactam-Extrakten |
| NL1005942C2 (nl) * | 1997-05-01 | 1998-11-03 | Dsm Nv | Depolymeriseren van polyamiden. |
| US5990306A (en) * | 1997-09-03 | 1999-11-23 | Alliedsignal Inc. | Process for the purification of caprolactam obtained from the depolymerization of polyamide-containing carpet |
| ATE539052T1 (de) * | 1999-02-26 | 2012-01-15 | Dsm Ip Assets Bv | Ein verfahren zur wiedergewinnung von caprolactam und wasserdampf |
| DE10251798A1 (de) * | 2002-11-07 | 2004-05-19 | Bayer Ag | Verfahren zur Herstellung von Polyamid 6 mit geringem Dimergehalt |
| US9023903B2 (en) | 2012-09-27 | 2015-05-05 | E I Du Pont De Nemours And Company | Reinforced polyamides having improved anti-delamination |
| US9109114B2 (en) | 2012-09-27 | 2015-08-18 | E I Du Pont De Nemours And Company | Polyamides having improved anti-delamination |
| US9193865B2 (en) | 2012-09-27 | 2015-11-24 | E I Du Pont De Nemours And Company | Polyamides having improved anti-delamination |
| CN107051345A (zh) * | 2017-01-25 | 2017-08-18 | 江苏永通新材料科技有限公司 | 一种用于生产聚酰胺切片的低聚物分离器 |
| JP6902157B2 (ja) * | 2017-08-01 | 2021-07-14 | アドバンシックス・レジンズ・アンド・ケミカルズ・リミテッド・ライアビリティ・カンパニーAdvansix Resins & Chemicals Llc | ポリアミドの環状オリゴマーを重合するための方法 |
| KR20240170935A (ko) * | 2022-04-01 | 2024-12-05 | 바스프 에스이 | 폴리아미드의 가수분해 해중합 공정에서의 불순물 분리 |
| TW202615130A (zh) * | 2024-05-15 | 2026-04-16 | 德商巴斯夫歐洲公司 | 用於從聚醯胺6解聚混合物中分離高沸物之方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD59094A (cg-RX-API-DMAC7.html) * | ||||
| US3245964A (en) * | 1962-11-13 | 1966-04-12 | Allied Chem | Continuous extraction of poly-e-caproamide |
| US3182055A (en) * | 1963-02-18 | 1965-05-04 | Allied Chem | Regeneration of e-caprolactam from polyamides |
| US3294756A (en) * | 1963-05-01 | 1966-12-27 | Allied Chem | Continuous polymerization of epsilon-caprolactam |
| US3266165A (en) * | 1964-10-01 | 1966-08-16 | Allied Chem | Process and apparatus for segregative drying of nylon-6 |
| NL135959C (cg-RX-API-DMAC7.html) * | 1964-12-23 | |||
| US3373145A (en) * | 1965-04-29 | 1968-03-12 | Allied Chem | Washing of polymer particulates by regular periodic ebb and flow of aqueous solvent |
| US3600381A (en) * | 1968-05-09 | 1971-08-17 | Teijin Ltd | Caprolactam purification process |
| AU434985B2 (en) * | 1969-12-15 | 1973-04-18 | Tevin Limited | Process for obtaining purified caprolactam bythe purification of oligomer-containing impure epsilon caprolactam |
| DE2135085C3 (de) * | 1971-07-14 | 1981-12-03 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Wiedergewinnung von Caprolactam aus einem Gemisch, das Caprolactam und dessen Oligomere enthält |
| US4107160A (en) * | 1977-08-24 | 1978-08-15 | Zimmer Aktiengesellschaft | Continuous process for the recovery of caprolactam |
-
1980
- 1980-09-17 US US06/187,864 patent/US4311642A/en not_active Expired - Lifetime
-
1981
- 1981-08-17 EP EP81106355A patent/EP0048340B1/en not_active Expired
- 1981-08-17 DE DE8181106355T patent/DE3173977D1/de not_active Expired
- 1981-09-14 CA CA000385778A patent/CA1157020A/en not_active Expired
- 1981-09-15 KR KR1019810003431A patent/KR860000829B1/ko not_active Expired
- 1981-09-17 JP JP56146995A patent/JPS5781458A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0148894B2 (cg-RX-API-DMAC7.html) | 1989-10-20 |
| CA1157020A (en) | 1983-11-15 |
| JPS5781458A (en) | 1982-05-21 |
| DE3173977D1 (en) | 1986-04-10 |
| EP0048340B1 (en) | 1986-03-05 |
| US4311642A (en) | 1982-01-19 |
| EP0048340A1 (en) | 1982-03-31 |
| KR830007546A (ko) | 1983-10-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1157020A (en) | Recovery of caprolactam from nylon 6 oligomers | |
| US5656757A (en) | Monomer recovery from multi-component materials | |
| CN102076471B (zh) | 一种萃取聚酰胺-6的连续方法 | |
| US3449220A (en) | Method of separating low-molecular weight components from high-polymeric compounds by thin film vacuum distillation | |
| US4107160A (en) | Continuous process for the recovery of caprolactam | |
| US8231765B2 (en) | Process for the purification of lactams | |
| US6332949B1 (en) | Method for upgrading used sulfuric acids | |
| US2813858A (en) | Process for purifying epsilon-caprolactam | |
| US4088660A (en) | Method for the separation and recovery of furfural and organic volatile acids, such as acetic acid and formic acid, from the process of preparation of furfural | |
| EP0270953B1 (en) | Preparation of anhydrous alkanesulfonic acid | |
| US6093788A (en) | Process of recovering ε-caprolactam from PA-6 synthesis extract water | |
| KR100497833B1 (ko) | 락탐의 정제 방법 | |
| US4935555A (en) | Purification of neopentyl glycol | |
| US4665205A (en) | Process for preparing tetrahydrofuran | |
| US4582642A (en) | Recovery of caprolactam from process residues | |
| US3459640A (en) | Process for the purification of lactams | |
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| US4014903A (en) | Recovery of dicarboxylic acids from aqueous solution containing nitric acid | |
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| US5705040A (en) | Process for preparing a substantially pure aqueous solution of hydrogen peroxide | |
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| US2960499A (en) | Preparing a lactam containing lactam oligomers | |
| WO2004113288A1 (en) | Method for making caprolactam |
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| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
St.27 status event code: A-0-1-A10-A12-nap-PA0109 |
|
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
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| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
|
| PA0201 | Request for examination |
St.27 status event code: A-1-2-D10-D11-exm-PA0201 |
|
| PG1501 | Laying open of application |
St.27 status event code: A-1-1-Q10-Q12-nap-PG1501 |
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| PG1605 | Publication of application before grant of patent |
St.27 status event code: A-2-2-Q10-Q13-nap-PG1605 |
|
| PE0701 | Decision of registration |
St.27 status event code: A-1-2-D10-D22-exm-PE0701 |
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| PR0701 | Registration of establishment |
St.27 status event code: A-2-4-F10-F11-exm-PR0701 |
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