KR860000751B1 - 시클로 헥실아민의 제조 방법 - Google Patents

시클로 헥실아민의 제조 방법 Download PDF

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Publication number
KR860000751B1
KR860000751B1 KR8202554A KR820002554A KR860000751B1 KR 860000751 B1 KR860000751 B1 KR 860000751B1 KR 8202554 A KR8202554 A KR 8202554A KR 820002554 A KR820002554 A KR 820002554A KR 860000751 B1 KR860000751 B1 KR 860000751B1
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South Korea
Prior art keywords
reaction
catalyst
parts
weight
aniline
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Expired
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KR8202554A
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English (en)
Korean (ko)
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KR840000472A (ko
Inventor
루드비히 머턴 헬무트
레이 와일더 진
Original Assignee
존 엘머 마우터
몬산토 캄파니
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Publication of KR840000472A publication Critical patent/KR840000472A/ko
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C07C209/70—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
    • C07C209/72—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines by reduction of six-membered aromatic rings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/46—Ruthenium, rhodium, osmium or iridium
    • B01J23/462—Ruthenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/26—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an unsaturated carbon skeleton containing at least one six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/06—Systems containing only non-condensed rings with a five-membered ring
    • C07C2601/08—Systems containing only non-condensed rings with a five-membered ring the ring being saturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
KR8202554A 1981-06-09 1982-06-08 시클로 헥실아민의 제조 방법 Expired KR860000751B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US271869 1981-06-09
US06/271,869 US4384142A (en) 1981-06-09 1981-06-09 Production of cyclohexylamine

Publications (2)

Publication Number Publication Date
KR840000472A KR840000472A (ko) 1984-02-22
KR860000751B1 true KR860000751B1 (ko) 1986-06-18

Family

ID=23037431

Family Applications (1)

Application Number Title Priority Date Filing Date
KR8202554A Expired KR860000751B1 (ko) 1981-06-09 1982-06-08 시클로 헥실아민의 제조 방법

Country Status (12)

Country Link
US (1) US4384142A (enExample)
EP (1) EP0067058B1 (enExample)
JP (1) JPS57212145A (enExample)
KR (1) KR860000751B1 (enExample)
AU (1) AU546303B2 (enExample)
BR (1) BR8203345A (enExample)
CA (1) CA1175071A (enExample)
DE (1) DE3261126D1 (enExample)
ES (1) ES8304533A1 (enExample)
IN (1) IN155993B (enExample)
MX (1) MX157607A (enExample)
ZA (1) ZA824021B (enExample)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3225879A1 (de) * 1982-07-10 1984-01-12 Basf Ag, 6700 Ludwigshafen Trans-3-(4'-tert.-butylcyclohexyl-1')-2-methyl-1-dialkyl-aminopropane, ihre herstellung und verwendung als arzneimittel
US5214212A (en) * 1992-02-27 1993-05-25 Olin Corporation Promoters for hydrogenation of aromatic amines
DE4207314A1 (de) * 1992-03-07 1993-09-09 Basf Ag Verfahren zur herstellung von cycloaliphatischen aminen
DE19533718A1 (de) * 1995-09-12 1997-03-13 Basf Ag Verfahren zur Hydrierung von aromatischen Verbindungen, in denen mindestens eine Aminogruppe an einen aromatischen Kern gebunden ist
DE59706719D1 (de) * 1996-04-26 2002-05-02 Basf Ag Verfahren zur Umsetzung einer organischen Verbindung in Gegenwart eines in situ gebildeten Ruthenium-katalysators
TW300214B (en) * 1996-06-06 1997-03-11 Sanfu Chemical Co Ltd Method for preparing cyclohexylamine
US6248924B1 (en) 1996-06-19 2001-06-19 Basf Aktiengesellschaft Process for reacting an organic compound in the presence of a supported ruthenium catalyst
DE19641688A1 (de) * 1996-10-10 1998-04-16 Bayer Ag Katalysatoren und Verfahren zur Herstellung von cycloaliphatischen Aminen
DE19651129A1 (de) * 1996-12-09 1998-06-10 Basf Ag Verfahren zur Hydrierung einer aromatischen Verbindung in Gegenwart eines Trägerkatalysators
DE10128242A1 (de) 2001-06-11 2002-12-12 Basf Ag Verfahren zur Hydrierung organischer Verbindungen
US7143462B2 (en) * 2002-09-20 2006-12-05 Colgate-Palmolive Company Oral care implement
DE10225565A1 (de) 2002-06-10 2003-12-18 Oxeno Olefinchemie Gmbh Katalysator und Verfahren zur Hydrierung von aromatischen Verbindungen
DE102004061608A1 (de) * 2004-12-17 2006-07-06 Basf Ag Verfahren zur Herstellung von 1,2-Diamino-3-methylcyclohexan und/oder 1,2-Diamino-4-methylcyclohexan
CN102216254A (zh) * 2008-11-18 2011-10-12 因温斯特技术公司 1,2-二氨基环己烷和化学方法
CN102633649B (zh) * 2012-03-29 2013-08-21 山东潍焦集团有限公司 一种苯胺气相催化加氢合成环己胺的方法
KR102969279B1 (ko) * 2022-05-26 2026-05-26 한국해양과학기술원 바닥 마찰 증대 케이슨
CN118290270A (zh) * 2024-04-02 2024-07-05 大连理工大学 一种纳米多孔钌镍催化剂催化氢化苯胺类化合物的方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2511028A (en) * 1947-12-04 1950-06-13 Du Pont 4-[(para-aminophenyl) alkyl] cyclo-hexylamine
US2606924A (en) * 1949-06-09 1952-08-12 Du Pont Bis (4-aminocyclohexyl)-methane
US2606925A (en) * 1949-12-15 1952-08-12 Du Pont Ruthenium catalyzed hydrogenation process for obtaining aminocyclohexyl compounds
US2822392A (en) * 1954-09-20 1958-02-04 Abbott Lab Process for producing cyclohexylamine
US2955926A (en) * 1954-09-20 1960-10-11 Abbott Lab High pressure chemical apparatus
US3347917A (en) * 1961-12-29 1967-10-17 Du Pont Process for the preparation of di (paraaminocyclohexyl) methane
US3636108A (en) * 1965-12-23 1972-01-18 Du Pont Catalytic hydrogenation of aromatic nitrogen containing compounds over alkali moderated ruthenium
FR1530477A (fr) * 1967-04-14 1968-06-28 Ugine Kuhlmann Procédé de fabrication de cyclohexylamine ou de cyclohexylamine et de dicyclohexylamine par hydrogénation de l'aniline
NL6709040A (enExample) * 1967-06-28 1968-12-30
US3644522A (en) * 1969-04-04 1972-02-22 Du Pont Catalytic hydrogenation of nitrogen containing compounds over supported ruthenium catalysts
US3914307A (en) * 1973-12-27 1975-10-21 Universal Oil Prod Co Hydrogenation of aromatic amines
US4161492A (en) * 1975-01-24 1979-07-17 Bayer Aktiengesellschaft Cycloaliphatic amines and process for preparing same

Also Published As

Publication number Publication date
ES512889A0 (es) 1983-03-01
US4384142A (en) 1983-05-17
BR8203345A (pt) 1984-01-17
JPS57212145A (en) 1982-12-27
JPH05376B2 (enExample) 1993-01-05
AU8467382A (en) 1982-12-16
MX157607A (es) 1988-12-05
EP0067058A1 (en) 1982-12-15
KR840000472A (ko) 1984-02-22
ZA824021B (en) 1983-04-27
CA1175071A (en) 1984-09-25
IN155993B (enExample) 1985-04-20
DE3261126D1 (en) 1984-12-06
AU546303B2 (en) 1985-08-29
EP0067058B1 (en) 1984-10-31
ES8304533A1 (es) 1983-03-01

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