KR830001367B1 - 티타늄 테트라클로라이드의 산화법 - Google Patents
티타늄 테트라클로라이드의 산화법 Download PDFInfo
- Publication number
- KR830001367B1 KR830001367B1 KR1019790004251A KR790004251A KR830001367B1 KR 830001367 B1 KR830001367 B1 KR 830001367B1 KR 1019790004251 A KR1019790004251 A KR 1019790004251A KR 790004251 A KR790004251 A KR 790004251A KR 830001367 B1 KR830001367 B1 KR 830001367B1
- Authority
- KR
- South Korea
- Prior art keywords
- titanium tetrachloride
- reaction
- ticl
- oxidation
- oxygen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 title claims description 32
- 238000007254 oxidation reaction Methods 0.000 title claims description 19
- 230000003647 oxidation Effects 0.000 title claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 32
- 239000007789 gas Substances 0.000 claims description 24
- 239000001301 oxygen Substances 0.000 claims description 20
- 229910052760 oxygen Inorganic materials 0.000 claims description 20
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 19
- 239000012530 fluid Substances 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 14
- 230000001590 oxidative effect Effects 0.000 claims description 13
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 12
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 239000000049 pigment Substances 0.000 description 9
- 239000012495 reaction gas Substances 0.000 description 7
- 239000011148 porous material Substances 0.000 description 5
- 239000000460 chlorine Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
- 229910003902 SiCl 4 Inorganic materials 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229910001615 alkaline earth metal halide Inorganic materials 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 230000019612 pigmentation Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000007039 two-step reaction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
- C09C1/3607—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US96625678A | 1978-12-04 | 1978-12-04 | |
US966256 | 1992-10-26 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR830001136A KR830001136A (ko) | 1983-04-29 |
KR830001367B1 true KR830001367B1 (ko) | 1983-07-19 |
Family
ID=25511119
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019790004251A Expired KR830001367B1 (ko) | 1978-12-04 | 1979-12-03 | 티타늄 테트라클로라이드의 산화법 |
Country Status (6)
Country | Link |
---|---|
JP (1) | JPS5580721A (enrdf_load_stackoverflow) |
KR (1) | KR830001367B1 (enrdf_load_stackoverflow) |
BR (1) | BR7907852A (enrdf_load_stackoverflow) |
FR (1) | FR2443423B1 (enrdf_load_stackoverflow) |
GB (1) | GB2037266B (enrdf_load_stackoverflow) |
IN (1) | IN152047B (enrdf_load_stackoverflow) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0619071Y2 (ja) * | 1988-05-12 | 1994-05-18 | 矢崎総業株式会社 | 圧力センサ |
US5204083A (en) * | 1988-05-23 | 1993-04-20 | Kerr-Mcgee Chemical Corporation | Process for preparing titanium dioxide |
GB9216933D0 (en) * | 1992-08-10 | 1992-09-23 | Tioxide Group Services Ltd | Oxidation of titanium tetrachloride |
US5536487A (en) * | 1995-02-27 | 1996-07-16 | Kronos, Inc. | Process for the use of rutile promoter and control additives in the manufacture of titanium dioxide by the chloride process |
US5840112A (en) | 1996-07-25 | 1998-11-24 | Kerr Mcgee Chemical Corporation | Method and apparatus for producing titanium dioxide |
PL187022B1 (pl) * | 1996-07-25 | 2004-04-30 | Kerr Mcgee Chemical Llc | Sposób wytwarzania dwutlenku tytanu i reaktor do wytwarzania dwutlenku tytanu |
TWI272251B (en) * | 2000-02-04 | 2007-02-01 | Showa Denko Kk | Process for producing ultrafine mixed-crystal oxide |
US6572964B2 (en) | 2000-02-04 | 2003-06-03 | Showa Denko K.K. | Ultrafine mixed-crystal oxide, production process and use thereof |
US6387347B1 (en) * | 2000-02-14 | 2002-05-14 | Millennium Inorganic Chemicals, Inc. | Controlled vapor phase oxidation of titanium tetrachloride to manufacture titanium dioxide |
US7476378B2 (en) | 2005-10-27 | 2009-01-13 | E.I. Dupont Denemours & Company | Process for producing titanium dioxide |
DE102007049296A1 (de) | 2007-10-12 | 2009-04-16 | Kronos International, Inc. | Mehrstufiges Verfahren zur Herstellung von Titandioxid |
CN114029025A (zh) * | 2021-11-15 | 2022-02-11 | 攀钢集团攀枝花钢铁研究院有限公司 | 一种氯化法钛白氧化反应装置 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL288332A (enrdf_load_stackoverflow) * | 1962-01-30 | |||
DE1592529B2 (de) * | 1967-06-03 | 1971-09-02 | Titangesellschaft mbH, 5090 Leverku sen | Verfahren zur herstellung eines rutil pigmentes durch umsetzung von titantetrachlorid mit sauerstoff in einem heissen gasgemisch |
US4053577A (en) * | 1972-02-18 | 1977-10-11 | Tioxide Group Limited | Process for the gaseous phase production of metal oxide particles |
-
1979
- 1979-10-18 IN IN1086/CAL/79A patent/IN152047B/en unknown
- 1979-12-03 FR FR7929677A patent/FR2443423B1/fr not_active Expired
- 1979-12-03 JP JP15570279A patent/JPS5580721A/ja active Pending
- 1979-12-03 KR KR1019790004251A patent/KR830001367B1/ko not_active Expired
- 1979-12-03 BR BR7907852A patent/BR7907852A/pt unknown
- 1979-12-04 GB GB7941763A patent/GB2037266B/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
GB2037266A (en) | 1980-07-09 |
IN152047B (enrdf_load_stackoverflow) | 1983-10-01 |
JPS5580721A (en) | 1980-06-18 |
FR2443423B1 (fr) | 1986-04-04 |
BR7907852A (pt) | 1980-07-29 |
KR830001136A (ko) | 1983-04-29 |
GB2037266B (en) | 1983-02-16 |
FR2443423A1 (fr) | 1980-07-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19791203 |
|
PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 19830119 Patent event code: PE09021S01D |
|
PG1501 | Laying open of application | ||
PG1605 | Publication of application before grant of patent |
Comment text: Decision on Publication of Application Patent event code: PG16051S01I Patent event date: 19830617 |
|
PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 19830926 |
|
PR0701 | Registration of establishment |
Comment text: Registration of Establishment Patent event date: 19831014 Patent event code: PR07011E01D |
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PR1002 | Payment of registration fee |
Payment date: 19831014 End annual number: 3 Start annual number: 1 |
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PR1001 | Payment of annual fee |
Payment date: 19860607 Start annual number: 4 End annual number: 4 |
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PR1001 | Payment of annual fee |
Payment date: 19870526 Start annual number: 5 End annual number: 5 |
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PR1001 | Payment of annual fee |
Payment date: 19880520 Start annual number: 6 End annual number: 6 |
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PR1001 | Payment of annual fee |
Payment date: 19890523 Start annual number: 7 End annual number: 7 |
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PR1001 | Payment of annual fee |
Payment date: 19900528 Start annual number: 8 End annual number: 8 |
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PR1001 | Payment of annual fee |
Payment date: 19910610 Start annual number: 9 End annual number: 9 |
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PR1001 | Payment of annual fee |
Payment date: 19920601 Start annual number: 10 End annual number: 10 |
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PR1001 | Payment of annual fee |
Payment date: 19930520 Start annual number: 11 End annual number: 11 |
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PR1001 | Payment of annual fee |
Payment date: 19940526 Start annual number: 12 End annual number: 12 |
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PC1801 | Expiration of term |