KR20230102330A - Detox cosmetic composition using clay mineral material and sulfur and manufacturing method thereof - Google Patents

Abstract

A detox cosmetic composition using a clay mineral material and sulfur is disclosed.
The detox cosmetic composition using the disclosed clay mineral material and sulfur includes zeolite; with bentonite; with diatomaceous earth; with elvan; germanium; And including refined sulfur powder,
The refined sulfur powder is a mixture of 10 to 15% fermented sulfur, 6 to 7% chelating agent, and 70 to 80% purified water, and has a size of 0.7 μm to 0.8 μm.

Description

Detox cosmetic composition using clay mineral material and sulfur and manufacturing method thereof

The present invention relates to a detox cosmetic composition using sulfur and a clay mineral material containing a large amount of useful minerals contained in a clay mineral having a high far-infrared emissivity, anti-inflammatory and antioxidant effects, and excellent adsorption of wastes including sebum, and a method for manufacturing the same. .

In recent years, ‘functional soap’ with various functions besides the cleansing function of soap is increasingly being used, and various soaps containing whitening ingredients and prevention of skin diseases such as acne and troubles are being released.

In general, sulfur detoxifies harmful substances deposited in the epidermal tissue of the skin, maintains the elasticity of the dermal tissue, helps to improve skin whitening and wrinkle removal, and as pentathionic acid is formed, the skin It is known to have a sterilizing effect by dissolving dead skin cells to remove various bacteria that cause acne, eczema, dandruff, and athlete's foot.

As sulfur has various effects on the skin, it is receiving a lot of attention and spotlight from modern people who value skin health. Accordingly, in recent years, in order to easily obtain various effects of sulfur hot springs without going to hot springs, a technology for commercializing sulfur into soaps has been developed.

Korean Patent No. 1006606 discloses a method for manufacturing medicinal soap using a sulfur solution dissolved in a nonionic surfactant, and Korean Patent No. 1113928 discloses a method for manufacturing natural soap using a nano-legislated sulfur dispersion liquid phase. However, it is different from the detox cosmetic composition and manufacturing method using the clay mineral material and sulfur of the present invention.

Registered Patent Publication No. 10-1006606 (2010.12.30) Registered Patent Publication No. 10-1113928 (2012.02.01)

The present invention was derived from the above needs, and an object of the present invention is to analyze the stability and quality of a cosmetic composition mixed with wet nanosulfur and ceramic mineral materials such as anti-inflammatory activity, antioxidant activity, harmful bacteria test and cytotoxicity evaluation The purpose is to provide a detox cosmetic composition using clay mineral materials and sulfur that has excellent effects on skin regeneration, detoxification, antibacterial and skin beauty without irritation to the skin.

In order to solve the above problems, the detox cosmetic composition using the clay mineral material and sulfur according to the present invention is zeolite; with bentonite; with diatomaceous earth; with elvan; germanium; and purified sulfur powder, wherein the purified sulfur powder is a mixture of 10 to 15% fermented sulfur, 6 to 7% chelating agent, and 70 to 80% purified water, and may have a size of 0.7 μm to 0.8 μm.

In addition, the method for manufacturing a detox cosmetic composition using clay mineral materials and sulfur according to the present invention is (1) a mineral water separation process step through zeolite, bentonite, diatomaceous earth, elvan and germanium-containing ceramic powder and clay mineral water purification. ; (2) obtaining refined sulfur having a size of 0.7 μm to 0.8 μm through a wet nano system after chelation of mineral sulfur; and (3) mixing the mineral water of step (1) with the purified sulfur of step (2) to form a complex.

In addition, the (1) mineral water separation step may include (1-1) mixing 20 to 30 parts by weight of the ceramic powder and clay mineral with 70 to 80 parts by weight of purified water; (1-2) primary stirring for 2 to 3 hours in 200 L; (1-3) mixing and stirring the ceramic powder and clay mineral in distilled water and separating the mixed mineral from water by passing it through a filtering net (screen 325 mesh) for water purification; (1-4) secondary stirring for 30 to 60 minutes; (1-5) recovering the supernatant to separate the precipitate; (1-6) heating the supernatant at 100 ° C for 24 to 48 hours for sterilization and disinfection after settling in a 1.5-ton settling tank; and (1-7) cooling to room temperature and aging for 3 to 4 days to obtain mineral active water.

In addition, the (2) step of obtaining purified sulfur includes (2-1) mixing 10 to 15% of fermented sulfur, 6 to 7% of a chelating agent, and 70 to 80% of purified water; (2-2) primary crushing; (2-3) chelation detoxification; (2-4) washing and purifying; (2-5) secondary crushing; and (2-6) recovering the supernatant to separate the precipitate.

As a result of the cytotoxicity evaluation, the detox cosmetic composition using clay mineral material and sulfur and its manufacturing method according to the present invention showed a survival rate of 90% or more compared to the untreated control group, and in the case of antioxidant, 174% or more compared to the control group, and anti-inflammation of the control group 57 As it achieves more than %, it is non-toxic and has effects of skin purification, cationic effect, far-infrared rays, ultraviolet rays blocking, antioxidant and deodorizing effects on ceramic clay minerals.

In addition, the detox cosmetic composition using clay mineral material and sulfur and its manufacturing method according to the present invention increase the functional components of each raw material by using wet nano-sulfur, bioceramic powder, and non-heated water purification of clay minerals, fine deposited on the skin It is possible to apply technology that maximizes the effectiveness of dust removal, skin inflammation, and trouble improvement, and can be applied to quasi-drugs for animals and household chemical safety products in addition to functional soaps and shampoos, so it has the advantage of expanding the product field.

1 is a photograph showing a detox cosmetic composition using a clay mineral material and sulfur according to the present invention and a step of (1) mineral water separation process in a manufacturing method thereof.
Figure 2 is a photograph showing the step of obtaining (2) refined sulfur in a detox cosmetic composition using a clay mineral material and sulfur and a manufacturing method thereof according to the present invention.
Figure 3 is a picture of shampoo and soap prepared with a detox cosmetic composition using a clay mineral material and sulfur according to the present invention.
4 is a product (shampoo) harmful bacteria test result report according to an embodiment of the present invention.
5 is a product (soap) harmful bacteria test result report according to an embodiment of the present invention.

Hereinafter, the composition of a detox cosmetic composition using a clay mineral material and sulfur according to an embodiment of the present invention will be described in detail with reference to the accompanying drawings.

The clay mineral material in the present invention may include zeolite, bentonite, diatomaceous earth, elvan, germanium, and refined sulfur powder. Five types of ceramic powders were tested for physical properties. Bentonite has the characteristics of pale off-white color, pH 10.5±0.5, high absorption rate, but slow absorption rate and insoluble in water. Zeolite is light gray, has a pH of 5.72±0.5, and has a high absorption rate and is easily dissolved in water. Diatomaceous earth is brown, pH 8.65±0.5, very rapidly absorbed and readily soluble in water. Elvan is light brown, pH 10.12±0.5, very rapidly absorbed and well soluble in water. Germanium is white, pH 6.22±0.5, poorly absorbed and insoluble in water.

Component analysis of 7 types of ceramic mineral water and refining composites was requested in terms of SiO3, Al2O3, Fe2O3, Ti)2, CaO, MgO, Na2O, K2O, ignition loss, moisture, arsenic, mercury, cadmium, and water-soluble S and S. It was conducted by requesting the Vito Analysis Center.

As a result, the ceramic mineral water-refined composite was analyzed to have moisture of 88.94%, Al2O3 0.32%, and Fe2O3 0.14%, and the nano-sulfur composite had water of 89.45%, Al2O3 0.001%, Fe2O3 0.004%, and sulfur ceramic water-purified extract 5% of water 85.79%. %, Al2O3 0.32%, Fe2O3 0.17%, Sulfur Ceramic Sub-purified Extract 10% is Moisture 84.07%, Al2O3 0.26%, Fe2O3 0.11%, Illite Mineral Active Liquid is Moisture 99.69%, Al2O3 not detected, Fe2O3 0.004%, Illite Subi Refined The extract 5% was analyzed as moisture 84.27%, Al2O3 0.32%, Fe2O3 0.48%, and illite sub-purified extract 10% was analyzed as moisture 80.83%, Al2O3 0.43%, Fe2O3 0.78%. Through this, it was confirmed that in the case of the sample to which the hydrorefining process was applied, the water content decreased, but the content of Al2O3, Fe2O3 and other components increased.

The refined sulfur powder is a mixture of 10 to 15% fermented sulfur, 6 to 7% chelating agent, and 70 to 80% purified water, and may have a size of 0.7 μm to 0.8 μm.

The manufacturing method of the detox cosmetic composition using the clay mineral material and sulfur according to the present invention is as follows.

(1) It is a step of separating mineral water through water purification of ceramic powder and clay minerals including zeolite, bentonite, diatomaceous earth, elvan and germanium.

(2) It is a step of obtaining purified sulfur with a size of 0.7㎛ to 0.8㎛ through a wet nano system after mineral sulfur chelation detoxification.

(3) mixing the mineral water in step (1) and purified sulfur in step (2) to form a complex.

1 is a photograph showing the step of (1) mineral water separation process in a detox cosmetic composition using clay mineral material and sulfur and a manufacturing method thereof according to the present invention.

In the manufacturing method of the detox cosmetic composition using clay mineral material and sulfur according to the present invention, the (1) mineral water separation step is (1-1) 20 to 30 parts by weight of the ceramic powder and clay mineral and 70 to 80 parts by weight of purified water Mixing parts by weight. (1-2) a step of primary stirring in 200L for 2 to 3 hours. (1-3) mixing and stirring the ceramic powder and clay mineral in distilled water and separating the mixed mineral from water by passing through a filtering net (screen 325 mesh) for water purification. (1-4) including the step of secondary stirring for 30 to 60 minutes. (1-5) recovering the supernatant and separating the precipitate. (1-6) After settling in a 1.5-ton settling tank, heating the supernatant at 100 degrees Celsius for 24 to 48 hours for sterilization and disinfection. (1-7) cooling to room temperature and aging for 3 to 4 days to obtain mineral active water.

Figure 2 is a photograph showing the step (2) of obtaining purified sulfur in a detox cosmetic composition using a clay mineral material and sulfur and a manufacturing method thereof according to the present invention.

Among the methods for manufacturing a detox cosmetic composition using clay mineral materials and sulfur according to the present invention, the step (2) obtaining purified sulfur includes (2-1) 10-15% fermented sulfur, 6-7% chelating agent, and purified water. Mixing 70-80%. (2-2) primary grinding, (2-3) chelation detoxification, (2-4) washing and purification, (2-5) secondary grinding and (2-6) supernatant It may include recovering and separating the precipitate.

3 is a photograph of shampoo and soap prepared with a detox cosmetic composition using clay mineral material and sulfur according to the present invention.

It was confirmed that the detox cosmetic composition using clay mineral material and sulfur according to the present invention was safe for use on human skin using the cytotoxicity result data for wet nano-sulfur, and based on this, the recipe concentration standard was set at 10% .

It was confirmed that it is safe for human skin use by utilizing the data of antioxidant, anti-inflammatory, cytotoxicity, and harmful bacteria test results for ceramic mineral materials. Based on this, the recipe concentration standards were set to 1,000 ppm for ceramic minerals and 19,321 ppm for extracts.

Referring to FIG. 3, the test product users were induced to use products of various routes, and as a first comparative survey, the shampoo bar was selected when comparing the efficacy, detergency, foam, gloss, fragrance, etc. of the liquid shampoo and the solid shampoo bar It was confirmed that the number of subjects was overwhelmingly high at 67%. In addition, as a result of comparing the feeling of use and detergency of 10%, 15%, and 20% ceramic mineral & nanosulfur content of shampoo bars and soaps, it was confirmed that the product with 15% content had a higher preference for both products. On the other hand, 10% and 20% products confirmed that there was no significant difference in preference despite a difference in raw material content of about twice as much, and the content comparison test was confirmed with the 15% product as a prototype.

4 is a product (shampoo) harmful bacteria test result report according to an embodiment of the present invention, and FIG. 5 is a product (soap) harmful bacteria test result report according to an embodiment of the present invention.

4 and 5, it was confirmed that the products according to the embodiment of the present invention showed a survival rate of 90% or more compared to the untreated control group as a result of the cytotoxicity evaluation for wet nanosulfur, and through this, the final development goal (compared to the control group) It was confirmed that more than 80% survival) was achieved. In addition, in the case of antioxidant for ceramic mineral materials, it was confirmed that the final development goal (antioxidation: control group 50% or more, anti-inflammatory: control group 20% or more) was achieved because more than 174% of the control group and anti-inflammation were more than 57% of the control group. Therefore, it can be confirmed that Escherichia coli was not detected in all three types of shampoo, soap, and mist, which are products made of the detox cosmetic composition using the clay mineral material and sulfur of the present invention.

The above embodiments are only exemplary, and various modifications and other equivalent embodiments may be made therefrom by those skilled in the art. Therefore, the true technical protection scope of the present invention should be determined by the technical spirit of the invention described in the claims.

Claims (4)

with zeolite;
with bentonite;
with diatomaceous earth;
with elvan;
germanium; and
Contains refined sulfur powder,
The purified sulfur powder,
A detox cosmetic composition using clay mineral materials and sulfur, characterized in that it has a size of 0.7 μm to 0.8 μm, as a mixture of 10-15% fermented sulfur, 6-7% chelating agent and 70-80% purified water. (1) Mineral water separation process step through water purification of ceramic powder and clay minerals including zeolite, bentonite, diatomaceous earth, elvan and germanium;
(2) obtaining refined sulfur having a size of 0.7 μm to 0.8 μm through a wet nano system after chelation of mineral sulfur; and
(3) A method for producing a detox cosmetic composition using clay mineral materials and sulfur, comprising mixing the mineral water in step (1) and purified sulfur in step (2) to form a complex. According to claim 1,
The (1) mineral water separation process step,
(1-1) mixing 20 to 30 parts by weight of the ceramic powder and clay mineral with 70 to 80 parts by weight of purified water;
(1-2) primary stirring for 2 to 3 hours in 200 L;
(1-3) mixing and stirring the ceramic powder and clay mineral in distilled water and separating the mixed mineral from water by passing it through a filtering net (screen 325 mesh) for water purification;
(1-4) secondary stirring for 30 to 60 minutes;
(1-5) recovering the supernatant to separate the precipitate;
(1-6) heating the supernatant at 100 ° C for 24 to 48 hours for sterilization and disinfection after settling in a 1.5-ton settling tank; and
(1-7) A method of manufacturing a detox cosmetic composition using clay mineral materials and sulfur, comprising obtaining mineral active water by cooling to room temperature and aging for 3 to 4 days. According to claim 1,
The (2) step of obtaining refined sulfur,
(2-1) mixing 10-15% fermented sulfur, 6-7% chelating agent and 70-80% purified water;
(2-2) primary crushing;
(2-3) chelation detoxification;
(2-4) washing and purifying;
(2-5) secondary crushing; and
(2-6) A method for producing a detox cosmetic composition using a clay mineral material and sulfur, comprising the step of recovering the supernatant and separating the precipitate.

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