KR101113928B1 - Method for fabricating detoxication sulfur nano power emulsion and method for fabricating natural soap using the same - Google Patents

Abstract

The present invention relates to a method for producing a nano- legal sulfur dispersion phase and a method for producing a natural soap using the same, (a) removing the toxicity of the sulfur powder; (b) a dry purification step of sequentially removing the toxic sulfur powder through a vibration sieve and strainer of 100 to 150 mesh to remove the organic matter and other impurities; (c) a wet refining step of mixing the sulfur powder having undergone the dry refining step with purified water and passing it through a shaker of 300 to 350 mesh; (d) coarse pulverizing step of forming the primary dispersion liquid by adding the sulfur powder, which has been subjected to the wet refining step, to the ball-mill having a bead particle size of 4 to 6 mm together with purified water; (e) finely pulverized to prepare a secondary dispersion liquid phase of 0.1 ~ 0.5㎛ by injecting the first dispersion liquid phase subjected to the coarse grinding step into a basket-mill having a bead particle size of 0.5 ~ 0.65mm step; And (f) inputting the secondary dispersion liquid obtained through the pulverization step into a bead mill or nano-mill having a bead particle size of 0.1 mm or less, thereby preparing an ultrafine grinding step of producing a legal sulfur dispersion liquid having a thickness of 20 to 50 nm. By performing a nano-prepared sulfur dispersion, and by using it to prepare a natural soap, the present invention relates to an invention for producing an environmentally friendly natural soap that can improve atopic dermatitis.

Description

METHOD FOR FABRICATING DETOXICATION SULFUR NANO POWER EMULSION AND METHOD FOR FABRICATING NATURAL SOAP USING THE SAME}

The present invention relates to a method for producing a nano-prepared sulfur dispersion liquid phase and a method for producing a natural soap using the same, by preparing a sulfur in the form of a dispersion or emulsion (Dispersion) having a size of 20 to 50nm The present invention relates to a technique for improving skin penetration ability and waste removal ability and improving atopic dermatitis improvement effect.

Atopic dermatitis is a chronic, recurrent inflammatory skin disease that usually begins in infancy or childhood, accompanied by pruritus (itch), dry skin, and characteristic eczema. In infancy, it begins with eczema on the flanks of the face and limbs, but as it grows, it is characteristic of eczema on the bends of the arms and behind the knees, and in many cases it tends to improve naturally as it grows. .

In adults, the skin becomes thicker in lichenification when the skin is folded, and eczema is more common on the face than in infants. Atopic dermatitis is on the rise worldwide, with a prevalence rate of 20% of the population.

The cause of atopic dermatitis is not yet known. Because clinical symptoms also appear in various cases such as dry skin and eczema, the cause of the disease cannot be explained by any one, but environmental factors, genetic predisposition, immunological reactions and abnormal skin barriers are considered as the main causes.

Environmental factors include allergens (allergens) such as environmental pollution such as soot from industrialization, increased use of food additives, increased use of carpets, beds, and sofas due to Western-style dwellings, and house dust mites due to increased room temperature. ) Increase.

In addition, as pets grow more indoors, exposure to causative agents is also a cause. Atopic dermatitis is genetically affected by the fact that many patients with atopic dermatitis have a family history.

The main symptoms of atopic dermatitis are severe pruritus (itch), dry skin, and skin lesions.

Dry skin causes and worsens itching. Itching intermittently during the day, usually worsening in the early evening or midnight. Itching and scratching leads to eczema skin lesions (pathological changes), and as these lesions progress, a vicious cycle leads to more severe itching.

The distribution and response patterns of skin lesions vary somewhat with the age of the patient. Infants often have acute eczema with a sore or scab, usually on the face and head, rough and dry on the outside of the limbs.

In children between 2 and 10 years of age, they often appear on the folds of the limbs and on the folds of the neck rather than on the face and appear in the form of dry eczema. Asians, on the other hand, may have severe nipple eczema that does not heal well after teens.

Atopic dermatitis often improves or disappears with age, but even when it improves, it tends to easily itch or inflammatory by specific substances or stimuli, and hand eczema often appears in adulthood.

If atopic dermatitis remains until adulthood, the skin symptoms of the body improve, while erythema, redness, and eczema tend to appear on the face, and the folding area has a long rubbing skin, which shows the appearance of thickened skin.

In adulthood, not only chronic eczema is present, but acute lesions with scabs and scabs on chronic eczema occur repeatedly over a period of time.

This atopic dermatitis is a problem that is called modern incurable disease, and suffers not only atopy patients themselves, but also their families.

In order to prevent atopic dermatitis caused by skin contamination among the above-mentioned problems, it is possible to treat atopy with natural soap, but by preparing a nano-size legal sulfur dispersion phase under strict process control and adding it to natural soap In order to prevent the entanglement of additives at the point of trace, soap production can be facilitated, and the process of nano-sulfur dispersing liquid to improve the elimination of waste and skin protection by allowing the sulfur to penetrate deep into the skin It is an object of the present invention to provide a production method and a production method of natural soap using the same.

Method for producing a nano- legal sulfur dispersion phase according to the present invention comprises the steps of (a) removing the toxicity of the sulfur powder; (b) a dry purification step of sequentially removing the toxic sulfur powder through a vibration sieve and strainer of 100 to 150 mesh to remove the organic matter and other impurities; (c) a wet refining step of mixing the sulfur powder that has undergone the dry refining step with purified water and then passing it through a shaker of 300 to 350 mesh; (d) coarse pulverizing step of forming the primary dispersion liquid by adding the sulfur powder, which has been subjected to the wet refining step, to the ball-mill having a bead particle size of 4 to 6 mm together with purified water; (e) finely pulverized to prepare a secondary dispersion liquid phase of 0.1 ~ 0.5㎛ by injecting the first dispersion liquid phase subjected to the coarse grinding step into a basket-mill having a bead particle size of 0.5 ~ 0.65mm step; And (f) adding the secondary dispersion obtained by the pulverization step into a bead-mill or nano-mill having a bead particle size of 0.1 mm or less, and having a legal sulfur of 20 to 50 nm. It is characterized in that it comprises an ultra fine grinding step of producing a dispersion phase.

Here, (a) prior to the step of removing the toxicity of the sulfur powder, (a-1) is selected from sulfur or silver of more than 90% purity and put in any one of the silver bowl, copper bowl and earthenware bowl, and heated to 710 ~ 900 ℃ Then, the step of performing the cooling step to 110 ~ 120 ℃ 8 to 10 times and (a-2) characterized by further comprising the step of pulverizing and dispersing, neutralizing the cooled sulfur.

Next, the step of removing the toxicity of the sulfur powder (a) is impregnated with one or more of purified radish juice, rye juice, rye water, barley water, pine leaf extract water, orchardia extract water, taro extract water and soybean water After aging, or impregnated with calcium (Ca) -enriched Jijangsu, or aged, or impregnated with calcium (Ca) -enriched mineral extract water, or aged or impregnated with medicinal herb extracts It features.

Next, the mixing ratio of the purified water to the sulfur powder in the step (c) is characterized in that 90: 1 ~ 100: 1 by weight.

Next, the mixing ratio of the purified water to the sulfur powder in the step (d) is 4: 1 ~ 6: 1 by weight ratio, in the step (d) of the ball-mill (Ball-Mill) The rotation speed is 80 ~ 100RPM, the operating time is characterized in that 20 to 28 hours.

Next, in the step (e), the number of revolutions of the basket-mill is 80 to 100 RPM, and the operation time is 20 to 28 hours.

Next, in the step (f), the number of revolutions of the bead-mill or nano-mill (Bead-Mill or Nano-Mill) is 80 to 100 RPM, characterized in that the operating time is 20 to 28 hours, (F) further comprises the step of adding a dispersant to the legal sulfur dispersion liquid.

In this case, the dispersant is characterized in that it comprises at least one of Arabic Gum, Xanthan Cum and Carboxy Methyl Cellulose (CMC), wherein the dispersing agent is 0.5 to 1% by weight of the sulfur dispersion phase weight It is characterized in that it is added at a ratio of.

In addition, the method for producing a natural soap according to the present invention is characterized in that the nano-prepared sulfur dispersion liquid prepared by the method described above is prepared by adding to the vegetable oil and the compound of caustic soda.

Here, the vegetable oil is characterized in that at least one of olive oil, coconut oil, palm oil, camellia oil and grape seed oil, characterized in that the nano legal sulfur is used in combination with herbs, herbs and natural minerals.

Using the manufacturing method of the nano-prepared sulfur dispersion liquid phase and the manufacturing method of the natural soap using the same according to this invention can prevent atopy by skin contamination.

In particular, by producing a legal sulfur dispersion phase of 20 ~ 50nm nanosize by strict process control, it provides the effect that legal sulfur can penetrate deep into the skin, and active mineral supply and exchange of intercellular materials.

Therefore, it is possible to increase the anti-aging and skin elasticity of the skin, and provide an effect of reducing acne, eczema blemish and freckles and the like.

In addition, the nano- legal sulfur dispersion phase according to the present invention activates the physiology of cells, generates heat energy to decompose harmful substances, and provides a far-infrared effect for improving the ability to release stress and waste.

In addition, the nano- legal sulfur dispersion phase according to the present invention can improve the anion effect, including blood purification, cell activation, immune resistance increase action, autonomic nervous system regulation action, harmful bacteria removal effect and odor removal effect.

In addition, by adding the nano- legal sulfur dispersion phase according to the present invention to natural soap, it increases the skin anti-aging material such as cystine protein, forms a skin antiseptic component such as pentathiic acid to prevent skin contamination, It provides an effect that can be maintained.

In addition, by using the natural soap according to the present invention, it can treat athlete's foot, eczema, acne, dandruff, keratin, sweat bands and atopic dermatitis, and provides an effect that can increase the elasticity of the skin.

Therefore, the manufacturing method of the nano- legal sulfur dispersion phase according to the present invention and a method for producing a natural soap using the same, can meet the needs of modern people pursuing well-being (LOHAS), natural By increasing the use of soap, it provides an effect that can also prevent environmental pollution.

1 is a flow chart showing a method for producing a nano- legal sulfur dispersion phase according to the present invention.

Hereinafter, with reference to the accompanying drawings it will be described in detail the manufacturing method of the nano-prepared sulfur dispersion phase according to the present invention and a method for producing a natural soap using the same.

BRIEF DESCRIPTION OF THE DRAWINGS The advantages and features of the present invention, and how to accomplish them, will become apparent with reference to the embodiments and drawings described in detail below. However, it is to be understood that the present invention is not limited to the disclosed embodiments, but may be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. It is intended that the disclosure of the present invention be limited only by the terms of the appended claims.

In particular, in the present invention, the dispersion liquid phase is to define an emulsion state or a dispersion state. Therefore, it is preferable that the term "dispersion liquid phase" used below is basically understood to include a nano powder.

1 is a flow chart showing a method for producing a nano- legal sulfur dispersion phase according to the present invention.

Referring to Figure 1, first to perform a step (S10) of removing the toxicity of sulfur powder.

Here, before removing the toxicity of the sulfur powder, sulfur having a purity of 90% or more is selected and placed in any one of a silver bowl, a copper bowl, and an earthenware bowl, heated to 710 to 900 ° C, and then cooled to 110 to 120 ° C. The process of performing 8 to 10 times and the step of pulverizing the cooled sulfur to powder, and further performing the step of neutralizing to prepare a raw sulfur powder.

At this time, when the heating temperature of the sulfur is less than 710 ℃ may fall purity, if the heating temperature exceeds 900 ℃ because it is outside the sufficient temperature range for sulfur liquefaction, rather it may result in energy waste, 900 ℃ It is preferable to adjust heating temperature below.

In addition, since the melting point of sulfur is about 113 ° C., the cooling temperature is preferably set to 110 to 120 ° C. in consideration of an error range. In the case of carrying out the above, since the advantages of powdering due to the increase in the number of repetitions are insufficient, it may be a waste.

At this time, the particle size of the sulfur powder is preferably to be 100 ~ 200㎛, the neutralization process is preferably adjusted to pH 7 by repeating the alkali and acid treatment of the method of adding vinegar acid to natural calcium carbonate.

Next, there may be various embodiments of removing the toxicity of the sulfur powder.

In the first embodiment, impregnated with at least one organic substance of purified radish juice, rye juice, rye water, barley water, pine leaf extract water, underwear extract water, taro extract water and soybean water for 40 to 60 hours, There is a method to perform impregnation aging 3-4 times.

As a second embodiment, there is a method of impregnating aging for about 40 to 60 hours in jijangsu, which is fortified with calcium (Ca). At this time, as a method of strengthening calcium (Ca), it is preferable to use a method of mixing the boiled water and pearl powder, or boiled crab shell and shrimp shell.

As a third embodiment, there is a method of impregnating and aging impregnated mineral extracted water with calcium (Ca). At this time, the mineral extract is activated by heat treatment of natural zeolite, Sepiorite, Attapulgite, Germanium powder, white jade powder, mica powder, mica powder, or murky powder, and then extract water is formed. For example, it is desirable to adjust the pH to 7 to remove the toxicity.

As a fourth embodiment, there is a method for detoxification by impregnating and ripening herbal extracts such as rich, licorice, triticale, pogongyoung, machihyeon, earth and ginseng.

The method of preparing sulfur powder according to the present invention may be performed by one or more methods selected from the above embodiments. However, the present invention is not always limited thereto, and any method may be used as long as there is a method of increasing sulfur decontamination rate.

Next, the toxic removal sulfur powder is sequentially passed through a vibration sieve and strainer of 100 ~ 150 mesh (Mesh) to perform a dry purification step (S20) to remove the organic matter and other impurities.

Next, the wet refining step is performed by mixing the sulfur powder passed through the purified water with purified water (S30) to pass through a shaker of 300 ~ 350 mesh (Mesh).

At this time, the mixing ratio of purified water to the sulfur powder is preferably adjusted to be 90: 1 to 100: 1 by weight ratio. If the weight of the purified water is not more than 90 times compared to the sulfur powder, the purification effect may be reduced.

In addition, in the wet purification process, it is preferable to perform separate collection as needed, or to further enhance the purification effect by performing a stepped defensive purification process.

Then, the coarse pulverization step (S40) of preparing the first dispersion liquid phase by adding the sulfur powder having undergone the wet refining step to a ball-mill having a bead particle size of 4 to 6 mm together with purified water. Perform.

Herein, the mixing ratio of the purified water to the sulfur powder is 4: 1 to 6: 1 by weight, and the rotation speed of the ball-mill is 80 to 100 RPM and the operating time is 20 to 28 hours. It is characterized by.

At this time, the size of the pulverized sulfur powder is preferably to have a particle size of about 5㎛, if the rotation speed of the ball-mill is less than 80 RPM, or the operating time is less than 20 hours, the particle size of the sulfur powder is 5㎛ or more It is often formed, and its uniformity may not appear evenly. On the other hand, when the rotation speed exceeds 100 RPM and the operating time exceeds 28 hours, the effect on the uniformity and refinement of the particle size is insufficient, and thus the optimum coarse grinding condition appears within the rotation speed and the operating time range.

Next, the primary dispersion liquid obtained through the coarse grinding step is introduced into a basket-mill having a bead particle size of 0.5 to 0.65 mm to prepare a secondary dispersion liquid phase of 0.1 to 0.5 μm. The grinding step (S50) is performed.

At this time, it is preferable that the operation conditions of the basket-mill also follow the coarse grinding conditions. Therefore, it is preferable that rotation speed is 80-100 RPM, and operation time is 20-28 hours.

Subsequently, the secondary dispersion obtained through the pulverization step is introduced into a bead-mill or nano-mill having a bead particle size of 0.1 mm or less, and legal sulfur of 20 to 50 nm. The ultra fine grinding step (S60) of preparing a dispersion liquid phase is performed.

At this time, the operating conditions of the bead-mill or nano-mill (Bead-Mill or Nano-Mill) is also adjusted to the number of revolutions 80 ~ 100RPM, operating time 20 ~ 28 hours, nano formulation having a final particle size of 20 ~ 50nm Preference is given to producing a sulfur dispersion liquid phase.

In the present invention, even when only one of the coarse grinding step, the fine grinding step, and the ultra fine grinding step is in violation of the conditions, it was not possible to obtain a nano legal sulfur dispersion phase having a size of 20 to 50 nm.

In addition, in order to utilize the nano-prepared sulfur dispersion liquid phase prepared as described above, it should be kept in a mostly dispersed state, it is preferable to further perform the dispersion step (S70) of adding a dispersant used in food additives.

In this case, the dispersant is characterized in that it comprises at least one of Arabic Gum, Xanthan Cum and Carboxy Methyl Cellulose (CMC), wherein the dispersing agent is 0.5 to 1% by weight of the sulfur dispersion phase weight It is preferable to add in the ratio of.

If the dispersing agent is added in less than 0.5% by weight of the emulsion dispersion phase, the dispersion effect of the nano-prepared sulfur powder may be inferior, and when added in an amount exceeding 1% by weight, the purity of the nano-law sulfur dispersion phase is deteriorated. May be of poor use.

The effect of such dispersion is an important factor, especially in producing functional products such as soaps.

Hereinafter, the atopic dermatitis prevention effect and its utility which can be obtained by demonstrating the method of manufacturing a natural soap using the nano legal process sulfur dispersion liquid phase which concerns on this invention are demonstrated.

To prepare a natural soap, first, caustic soda is added to vegetable oils such as olive oil, coconut oil, palm oil, camellia oil, grape seed oil, and the saponification reaction is induced.

In addition, in the present invention, the nano-dispersion sulfur dispersion phase of the size of 20-50 nm described above in the saponification reaction is added.

At this time, in order for the legal sulfur soap according to the present invention to achieve the purpose and efficacy for improving atopic dermatitis, the nano legal sulfur concentration of the liquid phase relative to the total weight of the soap composition should be added in an amount of 0.1 to 10% by weight.

When the weight ratio of the legal sulfur dispersion is less than 0.1% by weight, the pharmacological efficacy of the legal sulfur is insignificant, and the effect is reduced, and even if it is added in an amount exceeding 10% by weight, the soap cannot have the function of the present application. 1 weight% is added, More preferably, it is added at a ratio of 0.5-5 weight%.

In addition, in the present invention, supplementary additives such as herbs, herbal medicines, natural minerals, and the like may be further added to supplement the functions of soap in addition to the basic sulfur and soap components.

In particular, in the present invention, as well as the cleaning action as described above, it is possible to diversify the function of the soap by adding an additive that can supplement a variety of functions, such as skin disease prevention treatment, antibacterial function, antioxidant properties, skin nutrition supplements. As an additive to supplement the function, ginseng, milk, mugwort, cucumber, elvan powder, bamboo salt powder may be included.

At this time, containing 0.1 to 5% by weight of the above-mentioned auxiliary additives in the soap base including vegetable oil, surfactant, cinnamon powder, relative to the total weight of the soap, the main effect of the nano-prepared sulfur dispersion phase of the present invention It is preferable.

As a method of producing a natural soap by using the raw materials as described above it can be prepared by the melting method (MP), low temperature (CP), high temperature (HP) riveting method and the like.

In the present invention, by adding 5% by weight of the total weight of the soap raw material to the legal sulfur powder phase having a particle size of 150㎛, the ability to remove the waste in the skin based on the soap prepared by the low temperature method.

As a result, when the particle size of the legal sulfur dispersion liquid was 55 nm, the waste removal ability was about 1000 times higher than that of the standard soap, but the entanglement of the additive occurred at the trace point, resulting in a rough surface of the soap.

Thus, the particle size of the nano-dispersion sulfur dispersion phase was adjusted to 50 nm or less. In this case, the soap surface was smoothly formed while exhibiting the ability to remove wastes 1000 times or more, thereby improving soap manufacturing efficiency.

Next, in the case where the particle size of the nano- legal sulfur dispersion phase was less than 20 nm, even when the addition amount of the legal sulfur dispersion phase was more than 10% by weight, only 90 times less waste removal ability than the reference soap was shown.

Therefore, the natural soap manufacturing method using the nano- legal sulfur dispersion phase according to the present invention by adding a nano- legal sulfur dispersion phase having a particle size of 20 ~ 50nm, by setting to less than 0.1 to 10% by weight of the total weight of the soap raw material, As a natural soap for improving atopic dermatitis, it has an optimal function.

As described above, in the case of using the nano legal sulfur according to the present invention, by maximizing the legal function of the legal sulfur dispersion, the nano legal sulfur component can penetrate deep into the skin, and the mineral supply and the exchange of intercellular materials are active. By making it possible to increase the skin's anti-aging and skin elasticity.

In addition, the nano- legal sulfur dispersion phase according to the present invention is utilized as a natural soap, thereby activating the physiology of skin cells, generating heat energy to decompose harmful substances, and provide a far-infrared effect to improve the ability to discharge stress and waste products. Can be.

In addition, blood purification, cell activation, immune resistance increase action, autonomic nervous system regulation action, harmful bacteria removal effect and odor can be removed.

In addition, the nano- legal sulfur dispersion phase according to the present invention increases the skin anti-aging substance such as cystine protein, and forms a skin antiseptic component such as pentathiic acid to prevent skin contamination, athlete's foot, eczema, acne, dandruff, skin It can treat keratin, sweat and atopic dermatitis, and increase the elasticity of the skin.

While the present invention has been described in connection with what is presently considered to be practical exemplary embodiments, it is to be understood that the invention is not limited to the disclosed embodiments, but, on the contrary, It will be understood by those skilled in the art that the present invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. Therefore, it should be understood that the embodiments described above are exemplary in all respects and not restrictive.

Claims (17)

(a) removing the toxicity of the sulfur powder;
(b) a dry purification step of sequentially removing the toxic sulfur powder through a vibration sieve and strainer of 100 to 150 mesh to remove the organic matter and other impurities;
(c) a wet refining step of mixing the sulfur powder that has undergone the dry refining step with purified water and then passing it through a shaker of 300 to 350 mesh;
(d) coarse pulverizing step of forming the primary dispersion liquid by adding the sulfur powder, which has been subjected to the wet refining step, to the ball-mill having a bead particle size of 4 to 6 mm together with purified water;
(e) finely pulverized to prepare a secondary dispersion liquid phase of 0.1 ~ 0.5㎛ by injecting the first dispersion liquid phase subjected to the coarse grinding step into a basket-mill having a bead particle size of 0.5 ~ 0.65mm step; And
(f) dispersing the sulfuric acid of 20 to 50 nm by injecting the secondary dispersion liquid having undergone the fine grinding step into a bead-mill or nano-mill having a bead particle size of 0.1 mm or less. Ultrafine grinding step of preparing a liquid phase; method of producing a nano- legal sulfur dispersion phase comprising a.
The method of claim 1,
Prior to the step (a) removing the toxicity of the sulfur powder,
(a-1) Selecting sulfur with a purity of 90% or higher and placing it in one of silver, copper, and earthenware bowls, heating to 710 to 900 ° C, and then cooling to 110 to 120 ° C is performed 8 to 10 times. Making; And
(a-2) pulverizing the cooled sulfur to powder, and neutralizing the method of producing a nano-sulfur sulfur dispersion phase further comprising the step of neutralizing.
The method of claim 1,
Removing the toxicity of the sulfur powder (a) step is impregnated after impregnating at least one of purified radish juice, sesame juice, rye water, barley water, pine leaf extract water, orchardia extract water, taro extract water and soy water The manufacturing method of the nano- legal sulfur dispersion liquid phase characterized by the above-mentioned.
The method of claim 1,
The step of removing the toxicity of the sulfur powder (a) is a method for producing a nano-dispersion sulfur dispersion phase, characterized in that the aging after impregnated with calcium (Ca) enhanced jijangsu.
The method of claim 1,
The step of removing the toxicity of the sulfur powder (a) is a method of producing a nano-prepared sulfur dispersion phase, characterized in that the impregnated in the mineral extraction water enhanced calcium (Ca) and then aged.
The method of claim 1,
The step of removing the toxicity of the sulfur powder (a) is a method for producing a nano-prepared sulfur dispersion phase characterized in that the medicinal herbs are impregnated with water and then aged.
The method of claim 1,
The mixing ratio of the purified water to the sulfur powder in the step (c) is 90: 1 ~ 100: 1 by weight ratio of the manufacturing method of nano-sulfur sulfur dispersion phase.
The method of claim 1,
The mixing ratio of the purified water to the sulfur powder in the step (d) is 4: 1 ~ 6: 1 by the weight ratio of the manufacturing method of nano-sulfur sulfur dispersion phase.
The method of claim 1,
In the step (d), the number of revolutions of the ball-mill (Ball-Mill) is 80 ~ 100RPM, the operating time is nano-sulfur sulfur dispersion method characterized in that 20 to 28 hours.
The method of claim 1,
In the step (e), the number of revolutions of the basket-mill is 80 to 100 RPM, and the operating time is nano-producing sulfur dispersion phase, characterized in that 20 to 28 hours.
The method of claim 1,
In the step (f), the number of revolutions of the bead-mill or nano-mill (Bead-Mill or Nano-Mill) is 80 to 100 RPM, and the operating time is 20 to 28 hours. Manufacturing method.
The method of claim 1,
The method of manufacturing a nano-sulfur sulfur dispersion phase characterized in that it further comprises the step of adding a dispersant to the sulfur-sulphuric dispersion solution passed through step (f).
The method of claim 12,
The dispersing agent is a method for producing a nano-dispersed sulfur dispersion phase characterized in that it comprises at least one of Arabic Gum, Xanthan Cum and Carboxy Methyl Cellulose (CMC).
The method of claim 12,
The dispersing agent is a method for producing a nano- legal sulfur dispersion phase, characterized in that added in a proportion of 0.5 to 1% by weight of the sulfur dispersion weight.
A method for producing a natural soap, characterized by adding the nano- legal sulfur dispersion phase prepared by the method of any one of claims 1 to 14 to a vegetable oil and a compound of caustic soda.
The method of claim 15,
The vegetable oil is a method of producing a natural soap, characterized in that at least one of olive oil, coconut oil, palm oil, camellia oil and grape seed oil.
The method of claim 15,
Method of producing a natural soap, characterized in that the nano-sulfur formulation dispersion phase is used by mixing with herbs, herbs and natural minerals.

Images