KR20220163544A - A cosmetic composition comprising Lac pigment extract - Google Patents
A cosmetic composition comprising Lac pigment extract Download PDFInfo
- Publication number
- KR20220163544A KR20220163544A KR1020210071300A KR20210071300A KR20220163544A KR 20220163544 A KR20220163544 A KR 20220163544A KR 1020210071300 A KR1020210071300 A KR 1020210071300A KR 20210071300 A KR20210071300 A KR 20210071300A KR 20220163544 A KR20220163544 A KR 20220163544A
- Authority
- KR
- South Korea
- Prior art keywords
- extract
- lac pigment
- cosmetic composition
- weight
- skin
- Prior art date
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
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Abstract
Description
본 발명은 Lac 색소 추출물을 포함하는 화장료 조성물 및 이를 포함하는 화장품에 관한 것으로, 보다 상세하게는 유효성분의 피부흡수력이 우수하고, 피부의 주름 및 피부트러블을 개선하는 동시에 항산화 효과, 항노화 효과, 피부 노폐물 제거는 물론 보습, 미백 및 피부 개선에 탁월한 효과를 나타낼 수 있는 Lac 색소 추출물을 포함하는 화장료 조성물 및 이를 포함하는 화장품에 관한 것이다.The present invention relates to a cosmetic composition containing a Lac pigment extract and to a cosmetic product containing the same, and more particularly, the active ingredient has excellent skin absorption, improves skin wrinkles and skin troubles, and at the same time has antioxidant effects, anti-aging effects, It relates to a cosmetic composition containing a Lac pigment extract capable of exhibiting excellent effects in moisturizing, whitening and skin improvement as well as removing skin wastes, and cosmetics containing the same.
미세먼지, 황사 등의 기후 또는 환경적 요인으로 인해 아토피 등의 피부 질환이 증가하고 있다. 또한 건조한 생활환경 변화로 인해 피부에 대한 충분한 보습, 자외선에 의한 피부 손상 방지, 피부 노화 방지 등 다양한 피부 개선 및 미용에 대한 소비자의 요구가 증대되고 있는 추세이다. Skin diseases such as atopy are increasing due to climate or environmental factors such as fine dust and yellow dust. In addition, due to changes in the dry living environment, consumer demand for various skin improvement and beauty care, such as sufficient moisturizing of the skin, prevention of skin damage caused by ultraviolet rays, and prevention of skin aging, is increasing.
각종 피부 미용 관련 제품들은 주로 가공된 화학물질을 사용하고 있어 피부에 자극적이며, 오히려 피부를 손상시키는 부작용을 유발하는 문제점이 있다. Various skin beauty products mainly use processed chemicals, which are irritating to the skin and cause side effects that damage the skin.
이에 따라 화학물질의 사용을 최소화할 수 있고, 천연재료를 이용하여 피부에 친화적이면서 피부 개선에 도움이 되는 화장료 조성물에 대한 기술 연구가 활발히 진행되고 있다. Accordingly, technical research on a cosmetic composition that can minimize the use of chemicals and is friendly to the skin using natural materials and helps to improve the skin is being actively conducted.
그동안 천연 추출물을 화장료 조성물에 적용하고자 하는 시도가 있어 왔으나, 피부에 발림성이 좋지 않아 사용감이 떨어지며 자체 향이 피부 미용에 적합하지 않아 선호도가 낮은 편이였다. 또한, 천연 추출물의 유용 성분이 피부에 흡수되는 것이 쉽지 않아 이를 이용한 피부 개선 또는 미용 효과가 거의 나타나지 않아 상용화에 어려움이 있어 왔다. In the meantime, attempts have been made to apply natural extracts to cosmetic compositions. In addition, since it is not easy for useful components of natural extracts to be absorbed into the skin, there is little improvement in skin or cosmetic effects using them, so there has been difficulty in commercialization.
본 발명은 유효성분의 피부흡수력이 우수하고, 피부의 주름 및 피부트러블을 개선하는 동시에 항산화 효과, 항노화 효과, 피부 노폐물 제거는 물론 보습, 미백 및 피부 개선에 탁월한 효과를 나타낼 수 있는 Lac 색소 추출물을 포함하는 화장료 조성물 및 이를 포함하는 화장품을 제공하는 것을 목적으로 한다. The present invention is a Lac pigment extract that has excellent skin absorption of active ingredients, improves skin wrinkles and skin troubles, and at the same time has antioxidant effects, anti-aging effects, removal of skin wastes, as well as excellent effects in moisturizing, whitening and skin improvement. It is an object to provide a cosmetic composition comprising a cosmetic composition and a cosmetic comprising the same.
상기와 같은 목적을 달성하기 위하여, 본 발명은 물, Lac 색소 추출물, 보습제, 점증제 및 계면활성제를 포함하는 화장료 조성물을 제공한다. In order to achieve the above object, the present invention provides a cosmetic composition comprising water, a Lac pigment extract, a moisturizer, a thickening agent and a surfactant.
본 발명의 일실시예에 있어서, 상기 화장료 조성물은 Lac 색소 추출물 0.1~2중량%, 보습제 1~10중량%, 점증제 0.1~1중량%, 계면활성제 0.1~1중량 및 잔량의 물을 포함하는 것을 특징으로 한다. In one embodiment of the present invention, the cosmetic composition comprises 0.1 to 2% by weight of Lac pigment extract, 1 to 10% by weight moisturizer, 0.1 to 1% by weight thickener, 0.1 to 1% surfactant by weight and the remaining amount of water characterized by
본 발명의 일실시예에 있어서, 상기 Lac 색소 추출물은 Lac 색소 열수 추출물 및 Lac 색소 알코올 추출물을 포함하고, 상기 Lac 색소 열수 추출물 및 Lac 색소 알코올 추출물의 중량비는 20~40:60~80 인 것을 특징으로 한다. In one embodiment of the present invention, the Lac pigment extract includes a Lac pigment hot water extract and a Lac pigment alcohol extract, and the weight ratio of the Lac pigment hot water extract and the Lac pigment alcohol extract is 20 to 40:60 to 80. to be
본 발명의 일실시예에 있어서, 상기 화장료 조성물은 측백엽 추출물 0.1~1중량%를 추가로 포함하는 것을 특징으로 한다. In one embodiment of the present invention, the cosmetic composition is characterized in that it further comprises 0.1 to 1% by weight of the extract of cypress japonica.
본 발명의 일실시예에 있어서, 상기 화장료 조성물은 물봉선 추출물 0.1~1중량%를 추가로 포함하는 것을 특징으로 한다. In one embodiment of the present invention, the cosmetic composition is characterized in that it further comprises 0.1 to 1% by weight of water bongseon extract.
또한 본 발명은 상기 화장료 조성물을 포함하는 화장품을 제공한다. In addition, the present invention provides a cosmetic comprising the cosmetic composition.
본 발명은 유효성분의 피부흡수력이 우수하고, 피부의 주름 및 피부트러블을 개선하는 동시에 항산화 효과, 항노화 효과, 피부 노폐물 제거는 물론 보습, 미백 및 피부 개선에 탁월한 효과를 나타낼 수 있는 Lac 색소 추출물을 포함하는 화장료 조성물 및 이를 포함하는 화장품을 제공할 수 있다. The present invention is a Lac pigment extract that has excellent skin absorption of active ingredients, improves skin wrinkles and skin troubles, and at the same time has antioxidant effects, anti-aging effects, removal of skin wastes, as well as excellent effects in moisturizing, whitening and skin improvement. It is possible to provide a cosmetic composition comprising a cosmetic composition and a cosmetic comprising the same.
도 1은 15개 표준물질(페놀계 화합물 및 플라보노이드 화합물)의 HPLC 크로마토그래피(위), Lac 색소 열수 추출물의 HPLC 크로마토그래피(가운데) 및 Lac 색소 메탄올 추출물의 HPLC 크로마토그래피(아래)를 나타낸다: 1. Gallic, 2. Protocatechuic, 3. Chlorogenic, 4. 4-Hydroxybenzoic, 5. Caffeic, 6. Isovanillic, 7. Rutin, 8. p-Coumaric, 9. Ferulic, 10. Taxifolin, 11. Trans-Coumaric, 12. Rosmarinic, 13. Quecertin, 14. Tans-Cinnamic, 15. Kaempferol. Figure 1 shows HPLC chromatography of 15 standards (phenolic compounds and flavonoid compounds) (top), HPLC chromatography of Lac pigment hot water extract (middle) and HPLC chromatography of Lac pigment methanol extract (bottom): 1 .Gallic, 2. Protocatechuic, 3. Chlorogenic, 4. 4-Hydroxybenzoic, 5. Caffeic, 6. Isovanillic, 7. Rutin, 8. p -Coumaric, 9. Ferulic, 10. Taxifolin, 11. Trans -Coumaric, 12 .Rosmarinic, 13. Quecertin, 14. Tans -Cinnamic, 15. Kaempferol.
이하 실시예를 바탕으로 본 발명을 상세히 설명한다. 본 발명에 사용된 용어, 실시예 등은 본 발명을 보다 구체적으로 설명하고 통상의 기술자의 이해를 돕기 위하여 예시된 것에 불과할 뿐이며, 본 발명의 권리범위 등이 이에 한정되어 해석되어서는 안 된다.The present invention will be described in detail based on the following examples. The terms, examples, etc. used in the present invention are merely exemplified to explain the present invention in more detail and help the understanding of those skilled in the art, and the scope of the present invention should not be construed as being limited thereto.
본 발명에 사용되는 기술 용어 및 과학 용어는 다른 정의가 없다면 이 발명이 속하는 기술 분야에서 통상의 지식을 가진 자가 통상적으로 이해하고 있는 의미를 나타낸다.Technical terms and scientific terms used in the present invention represent meanings commonly understood by those of ordinary skill in the art to which this invention belongs, unless otherwise defined.
본 발명은 물, Lac 색소 추출물, 보습제, 점증제 및 계면활성제를 포함하는 화장료 조성물에 관한 것이다. The present invention relates to a cosmetic composition comprising water, a Lac pigment extract, a moisturizer, a thickening agent and a surfactant.
상기 화장료 조성물은 Lac 색소 추출물 0.1~2중량%, 보습제 1~10중량%, 점증제 0.1~1중량%, 계면활성제 0.1~1중량 및 잔량의 물을 포함할 수 있다. The cosmetic composition may include 0.1 to 2% by weight of Lac pigment extract, 1 to 10% by weight of a moisturizer, 0.1 to 1% by weight of a thickening agent, 0.1 to 1% by weight of a surfactant, and the remaining amount of water.
상기 Lac 색소 추출물은 Lac 색소를 물, 알코올(에탄올, 메탄올, 주정, 발효주정 등), 아세톤 등의 용매로 가열 추출하고 감압 농축하여 수득할 수 있다. The Lac pigment extract can be obtained by heat-extracting the Lac pigment with a solvent such as water, alcohol (ethanol, methanol, alcohol, fermented alcohol, etc.), acetone, and concentrated under reduced pressure.
상기 Lac 색소는 연지벌레 유충이 분비하는 수지상 물질에서 추출된 것으로서, 락카인산을 주성분으로 하고 내열성, 내광성 및 열안정성이 우수하며 섬유 및 모발의 염색에 활용되고 있다. The Lac pigment is extracted from a dendritic substance secreted by cochineal larvae, has laccaic acid as a main component, has excellent heat resistance, light resistance and heat stability, and is used for dyeing of fibers and hair.
상기 Lac 색소 추출물은 Lac 색소를 물로 가열 추출하고 감압 농축하여 수득한 Lac 색소 열수 추출물인 것이 바람직하다. The Lac pigment extract is preferably a Lac pigment hot-water extract obtained by heat-extracting the Lac pigment with water and concentrating under reduced pressure.
또한 상기 Lac 색소를 알코올로 가열 추출하고 감압 농축하여 수득한 Lac 색소 알코올 추출물인 것이 바람직하다. It is also preferable to be an alcohol extract of the Lac pigment obtained by heat-extracting the Lac pigment with alcohol and concentrating under reduced pressure.
아울러 상기 Lac 색소를 알코올로 가열 추출하고 감압 농축하여 알코올을 제거한 후, 정제수로 수용화한 Lac 색소 수용성 추출물을 사용할 수 있다. In addition, after heat-extracting the Lac pigment with alcohol, concentrating under reduced pressure to remove the alcohol, and water-soluble Lac pigment-soluble extract with purified water can be used.
상기 Lac 색소 수용성 추출물은 물에 잘 녹고 점도가 낮아 가공이 간편하고, 상기 수용화 과정을 거치면서 일부 유효성분의 함량이 증가할 수 있다. The Lac pigment water-soluble extract is easy to process because it is well soluble in water and has low viscosity, and the content of some active ingredients may increase through the water-solubility process.
가열 추출은 Lac 색소 100중량부에 대하여 용매 100~3,000중량부를 가하고 40~120℃에서 1~12시간 가열하여 추출할 수 있으며, 용매로 1~3시간씩 1~5번 반복해서 가열 추출하는 것이 바람직하다. Heat extraction can be performed by adding 100 to 3,000 parts by weight of solvent to 100 parts by weight of Lac pigment and heating at 40 to 120 ° C for 1 to 12 hours. desirable.
가열 추출한 후 감압 농축하여 Lac 색소 추출물을 수득할 수 있다. After extraction with heat, concentrated under reduced pressure to obtain a Lac pigment extract.
또한 Lac 색소를 알코올로 가열 추출하고 감압 농축하여 알코올을 제거한 후, 이를 다시 정제수로 수용화함으로써, Lac 색소 수용성 추출물을 제조할 수 있다. In addition, a water-soluble extract of Lac pigment can be prepared by heat-extracting Lac pigment with alcohol, concentrating under reduced pressure to remove alcohol, and then resolving the Lac pigment in purified water.
상기 Lac 색소 수용성 추출물은 그대로 사용하거나 감압 농축하여 정제수를 제거하여 사용할 수도 있다. The Lac pigment water-soluble extract may be used as it is or concentrated under reduced pressure to remove purified water.
상기 Lac 색소 열수 추출물은 포스포세린(phosphoserine), γ-아미노부티르산(γ-aminobutyric acid), 페룰산(ferulic acid), p-쿠마르산(p-coumaric acid) 등을 포함할 수 있다. The Lac dye hot water extract may include phosphoserine, γ-aminobutyric acid, ferulic acid, p-coumaric acid, and the like.
또한 상기 Lac 색소 알코올 추출물은 포스포세린(phosphoserine), γ-아미노부티르산(γ-aminobutyric acid), 타우린(taurine), 페룰산(ferulic acid), p-쿠마르산(p-coumaric acid), 4-하이드록시벤조산(4-hydroxybenzoic acid), 로즈마린산(rosmarinic acid), t-시나믹산(t-cinnamic acid), 루틴(rutin), 탁시폴린(taxifolin) 등을 포함할 수 있다. In addition, the Lac pigment alcohol extract is phosphoserine, γ-aminobutyric acid, taurine, ferulic acid, p-coumaric acid, 4-hydroxy It may include 4-hydroxybenzoic acid, rosmarinic acid, t-cinnamic acid, rutin, taxifolin, and the like.
본 발명은 상기 Lac 색소 추출물로서 Lac 색소 열수 추출물 및 Lac 색소 알코올 추출물을 동시에 사용할 수 있고, 이때 Lac 색소 열수 추출물 및 Lac 색소 알코올 추출물의 중량비는 20~40:60~80 인 것이 바람직하다. 상기 열수 추출물 및 알코올 추출물의 중량비가 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. In the present invention, as the Lac pigment extract, a Lac pigment hot water extract and a Lac pigment alcohol extract may be simultaneously used. When the weight ratio of the hot water extract and the alcohol extract satisfies the above numerical range, the antioxidant effect, anti-aging effect, and skin improvement effect can be maximized.
또한 본 발명은 상기 Lac 색소 추출물로서 Lac 색소 알코올 추출물, Lac 색소 열수 추출물 및 Lac 색소 수용성 추출물을 동시에 사용할 수 있고, 이때 Lac 색소 알코올 추출물, Lac 색소 열수 추출물 및 Lac 색소 수용성 추출물의 중량비는 100:20~40:10~30 인 것이 바람직하다. 중량비가 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. In addition, in the present invention, as the Lac pigment extract, a Lac pigment alcohol extract, a Lac pigment hot water extract, and a Lac pigment water-soluble extract may be simultaneously used, wherein the weight ratio of the Lac pigment alcohol extract, the Lac pigment hot water extract, and the Lac pigment water-soluble extract is 100:20. It is preferably ~40:10~30. When the weight ratio satisfies the above numerical range, antioxidant effect, anti-aging effect, and skin improvement effect can be maximized.
상기 Lac 색소 추출물은 0.1~2중량% 사용되는 것이 바람직하고, Lac 색소 추출물의 함량이 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. The Lac pigment extract is preferably used in an amount of 0.1 to 2% by weight, and when the content of the Lac pigment extract satisfies the above numerical range, the antioxidant effect, anti-aging effect, and skin improvement effect can be maximized.
상기 보습제는 디프로필렌글리콜, 프로필렌글리콜, 부틸렌글리콜, 글리세린, 베타인, 글리세레스-26(Glycereth-26), 솔비톨, 헥실렌글리콜, 디글리세린 및 판테놀에서 선택되는 하나 이상이 사용될 수 있으며, 디프로필렌글리콜, 부틸렌글리콜 및 글리세린이 사용되는 것이 바람직하다. The humectant may be at least one selected from dipropylene glycol, propylene glycol, butylene glycol, glycerin, betaine, glycereth-26, sorbitol, hexylene glycol, diglycerin, and panthenol. Propylene glycol, butylene glycol and glycerin are preferably used.
상기 보습제의 함량은 1~10중량% 인 것이 바람직하며, 함량이 1중량% 미만이면 보습효과가 미미하고, 함량이 10중량%를 초과하면 피부 개선효과가 저하된다. The content of the humectant is preferably 1 to 10% by weight, and when the content is less than 1% by weight, the moisturizing effect is insignificant, and when the content exceeds 10% by weight, the skin improvement effect is reduced.
상기 점증제는 카보머(carbomer), 셀룰로오스, 메틸셀룰로오스, 하이드록시에틸셀룰로오스, 잔탐검(xanthan gum), 젤란검(gellan gum) 및 폴리아크릴산나트륨(sodium polyacrylate)에서 선택되는 하나 이상이 사용될 수 있다. The thickener may be one or more selected from carbomer, cellulose, methylcellulose, hydroxyethylcellulose, xanthan gum, gellan gum, and sodium polyacrylate. .
상기 점증제의 함량은 0.1~1중량% 인 것이 바람직하며, 함량이 0.1중량% 미만이면 안정성이 저하되고, 함량이 1중량%를 초과하면 피부흡수력이 저하된다. The content of the thickener is preferably 0.1 to 1% by weight, and when the content is less than 0.1% by weight, stability is lowered, and when the content exceeds 1% by weight, skin absorption is lowered.
상기 계면활성제는 폴리옥시에틸렌세틸올리에이트, 폴리글리세릴-10 올리에이트, 폴리글리세릴-10 라우레이트, 폴리글리세릴-10 미리스테이트, 폴리글리세릴-10 스테아레이트 등이 사용될 수 있다. As the surfactant, polyoxyethylene cetyl oleate, polyglyceryl-10 oleate, polyglyceryl-10 laurate, polyglyceryl-10 myristate, polyglyceryl-10 stearate, and the like may be used.
상기 계면활성제의 함량은 0.1~1중량% 인 것이 바람직하며, 함량이 0.1중량% 미만이면 안정성이 저하되고, 함량이 1중량%를 초과하면 피부흡수력이 저하된다. The content of the surfactant is preferably 0.1 to 1% by weight, and when the content is less than 0.1% by weight, stability is lowered, and when the content exceeds 1% by weight, skin absorption is lowered.
본 발명의 물로는 증류수, 정수, 정제수, 경수, 연수, 천연수, 해양심층수, 전해 알칼리이온수, 전해 산성이온수, 이온수 및 클러스터수가 사용될 수 있다. Distilled water, purified water, purified water, hard water, soft water, natural water, deep sea water, electrolytic alkaline ionized water, electrolytic acid ionized water, ionized water, and cluster water may be used as the water of the present invention.
또한 상기 화장료 조성물은 측백엽 추출물 0.1~1중량%를 추가로 포함할 수 있다. In addition, the cosmetic composition may further include 0.1 to 1% by weight of an extract of cypress japonica.
상기 측백엽 추출물의 함량이 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. When the content of the cypress leaf extract satisfies the above numerical range, the antioxidant effect, anti-aging effect, and skin improvement effect can be maximized.
상기 화장료 조성물은 물봉선 추출물 0.1~1중량%를 추가로 포함할 수 있다. The cosmetic composition may further include 0.1 to 1% by weight of water bongseon extract.
상기 물봉선 추출물의 함량이 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. When the content of the Mulbongseon extract satisfies the above numerical range, the antioxidant effect, anti-aging effect, and skin improvement effect can be maximized.
상기 화장료 조성물은 참당귀 추출물 0.1~1중량%를 추가로 포함할 수 있다. The cosmetic composition may further include 0.1 to 1% by weight of Angelica gigas extract.
상기 참당귀 추출물의 함량이 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. When the content of the Angelica gigas extract satisfies the above numerical range, the antioxidant effect, anti-aging effect, and skin improvement effect can be maximized.
상기 화장료 조성물은 사상자 추출물 0.1~1중량%를 추가로 포함할 수 있다. The cosmetic composition may further include 0.1 to 1% by weight of a casualty extract.
상기 사상자 추출물의 함량이 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. When the content of the casualty extract satisfies the above numerical range, the antioxidant effect, anti-aging effect and skin improvement effect can be maximized.
상기 화장료 조성물은 자초 뿌리 추출물 0.1~1중량%를 추가로 포함할 수 있다. The cosmetic composition may further include 0.1 to 1% by weight of a self-inflicted root extract.
상기 자초 뿌리 추출물의 함량이 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. When the content of the self-injection root extract satisfies the above numerical range, the antioxidant effect, anti-aging effect and skin improvement effect can be maximized.
상기 화장료 조성물은 쑥 추출물 0.1~1중량%를 추가로 포함할 수 있다. The cosmetic composition may further include 0.1 to 1% by weight of mugwort extract.
상기 쑥 추출물의 함량이 상기 수치범위를 만족하는 경우, 항산화 효과, 항노화 효과 및 피부 개선효과가 극대화될 수 있다. When the content of the mugwort extract satisfies the above numerical range, the antioxidant effect, anti-aging effect and skin improvement effect can be maximized.
상기 측백엽 추출물, 물봉선 추출물, 참당귀 추출물, 사상자 추출물, 자초 뿌리 추출물 및 쑥 추출물은 Lac 색소 추출물의 제조방법과 동일한 방법으로 제조될 수 있다. The cypress leaf extract, Mulbongseon extract, Angelica gigas extract, Sagittarius extract, perennial root extract, and mugwort extract may be prepared by the same method as the Lac pigment extract.
또한 본 발명은 상기 화장료 조성물을 포함하는 화장품에 관한 것이다. In addition, the present invention relates to cosmetics comprising the cosmetic composition.
상기 화장료 조성물은 크게 제한되는 것은 아니지만, 유연 화장수, 영양 화장수 등과 같은 화장수; 페이셜 로션, 바디 로션 등과 같은 로션; 핸드 크림, 영양 크림, 수분 크림, 아이 크림 등과 같은 크림; 에센스; 오일; 겔; 세안제; 비누; 스크럽제; 분무제; 패치; 및 팩으로 이루어진 군으로부터 선택되는 어느 하나의 화장품으로 제조될 수 있다. The cosmetic composition is not particularly limited, but lotions such as softening lotion and nutrient lotion; lotions such as facial lotions, body lotions, and the like; creams such as hand creams, nourishing creams, moisture creams, eye creams, and the like; essence; oil; gel; face wash; soap; scrubs; aerosol; patch; And it can be made into any one cosmetic selected from the group consisting of a pack.
이하 구체적인 실시예를 들어 본 발명을 상세히 기술하나, 본 발명의 범위가 이들 실시예에 의해 한정되는 것은 아니다.Hereinafter, the present invention will be described in detail with reference to specific examples, but the scope of the present invention is not limited by these examples.
(실시예 1) Lac 색소 추출물의 제조 (Example 1) Preparation of Lac pigment extract
Lac 색소 1g을 증류수 30㎖로 100℃에서 1시간 환류 추출한 다음 감압 농축하여 추출물을 수득하였다(Lac 색소 열수 추출물). 1 g of Lac pigment was extracted with 30 ml of distilled water under reflux at 100° C. for 1 hour, and then concentrated under reduced pressure to obtain an extract (hot water extract of Lac pigment).
Lac 색소 1g을 95% 메탄올 30㎖로 100℃에서 1시간 환류 추출한 다음 감압 농축하여 추출물을 수득하였다(Lac 색소 메탄올 추출물). 1 g of Lac pigment was extracted under reflux at 100° C. for 1 hour with 30 ml of 95% methanol, and then concentrated under reduced pressure to obtain an extract (Lac pigment methanol extract).
Lac 색소 1g을 95% 메탄올 30㎖로 100℃에서 1시간 환류 추출한 다음 감압 농축하고 용매를 모두 제거한 후, 정제수로 수용화시켜 추출물을 수득하였다(Lac 색소 수용성 추출물). 1 g of Lac pigment was extracted with 30 ml of 95% methanol at 100° C. under reflux for 1 hour, concentrated under reduced pressure, all solvents were removed, and then soluble in purified water to obtain an extract (Lac pigment water-soluble extract).
도 1은 15개 표준물질(페놀계 화합물 및 플라보노이드 화합물)의 HPLC 크로마토그래피(위), Lac 색소 열수 추출물의 HPLC 크로마토그래피(가운데) 및 Lac 색소 메탄올 추출물의 HPLC 크로마토그래피(아래)를 나타내고 있다. Figure 1 shows HPLC chromatography (top) of 15 standard substances (phenolic compounds and flavonoid compounds), HPLC chromatography (middle) of Lac pigment hot water extract, and HPLC chromatography (bottom) of Lac pigment methanol extract.
상기 Lac 색소 열수 추출물은 포스포세린(phosphoserine) 6,060㎍/g, γ-아미노부티르산(γ-aminobutyric acid) 1,140㎍/g, 페룰산(ferulic acid) 107.60㎍/g, p-쿠마르산(p-coumaric acid) 252.40㎍/g 등을 포함할 수 있다. The Lac dye hot water extract contained 6,060 μg/g of phosphoserine, 1,140 μg/g of γ-aminobutyric acid, 107.60 μg/g of ferulic acid, and 107.60 μg/g of p-coumaric acid. acid) 252.40 μg/g and the like.
또한 상기 Lac 색소 메탄올 추출물은 포스포세린(phosphoserine) 4,290㎍/g, γ-아미노부티르산(γ-aminobutyric acid) 60㎍/g, 타우린(taurine) 210㎍/g, 페룰산(ferulic acid) 1,042.13㎍/g, p-쿠마르산(p-coumaric acid) 60.43㎍/g, 4-하이드록시벤조산(4-hydroxybenzoic acid) 87.90㎍/g, 로즈마린산(rosmarinic acid) 7.92㎍/g, t-시나믹산(t-cinnamic acid) 191.38㎍/g, 루틴(rutin) 155.21㎍/g, 탁시폴린(taxifolin) 69.00㎍/g 등을 포함할 수 있다. In addition, the Lac pigment methanol extract contained phosphoserine 4,290 μg/g, γ-aminobutyric acid 60 μg/g, taurine 210 μg/g, and ferulic acid 1,042.13 μg/g. g, p-coumaric acid 60.43μg/g, 4-hydroxybenzoic acid 87.90μg/g, rosmarinic acid 7.92μg/g, t-cinnamic acid (t- cinnamic acid) 191.38 μg/g, rutin 155.21 μg/g, taxifolin 69.00 μg/g, and the like.
(실시예 2) Lac 색소 추출물의 DPPH 소거특성 (Example 2) DPPH scavenging characteristics of Lac pigment extract
Lac 색소 추출물 100 ㎕(100 ㎍/㎖)에 100 mM Tris-HCl(pH 7.4) 400 ㎕를 혼합한 후, 500 μM DPPH (1,1-diphenyl-2-picrylhydrazyl in MeOH, Sigma-Aldrich, St. Louis, MO, USA) 용액 500 ㎕을 넣고 혼합한 다음, DPPH 라디칼 소거특성을 측정하였다. After mixing 400 μl of 100 mM Tris-HCl (pH 7.4) with 100 μl (100 μg/ml) of Lac pigment extract, 500 μM DPPH (1,1-diphenyl-2-picrylhydrazyl in MeOH, Sigma-Aldrich, St. Louis, MO, USA) solution was added and mixed, and DPPH radical scavenging properties were measured.
(%)DPPH radical scavenging activity
(%)
(30:70)Lac pigment hot water extract + Lac pigment methanol extract
(30:70)
(50:50)Lac pigment hot water extract + Lac pigment methanol extract
(50:50)
(10:90)Lac pigment hot water extract + Lac pigment methanol extract
(10:90)
(100:30:20)Lac pigment methanol extract + Lac pigment hot water extract + Lac pigment water soluble extract
(100:30:20)
(100:30:5)Lac pigment methanol extract + Lac pigment hot water extract + Lac pigment water soluble extract
(100:30:5)
(100:30:40)Lac pigment methanol extract + Lac pigment hot water extract + Lac pigment water soluble extract
(100:30:40)
상기 표에서 알 수 있듯이, Lac 색소 열수 추출물 또는 Lac 색소 메탄올 추출물을 사용하는 경우 DPPH 라디칼 소거활성이 증가되어 항산화 특성이 향상됨을 확인할 수 있다. As can be seen from the above table, it can be confirmed that the antioxidant properties are improved by increasing the DPPH radical scavenging activity when the Lac pigment hot water extract or the Lac pigment methanol extract is used.
또한 Lac 색소 열수 추출물 및 Lac 색소 메탄올 추출물을 동시에 사용하는 경우 DPPH 라디칼 소거활성이 현저히 증가함을 확인할 수 있다. 이때 Lac 색소 열수 추출물 및 Lac 색소 메탄올 추출물의 중량비가 20~40:60~80 인 경우, DPPH 라디칼 소거활성이 극대화될 수 있다. In addition, it can be confirmed that the DPPH radical scavenging activity significantly increased when the Lac pigment hot water extract and the Lac pigment methanol extract were simultaneously used. At this time, when the weight ratio of the Lac pigment hot water extract and the Lac pigment methanol extract is 20 to 40:60 to 80, DPPH radical scavenging activity can be maximized.
아울러 Lac 색소 메탄올 추출물, Lac 색소 열수 추출물 및 Lac 색소 수용성 추출물을 동시에 사용하는 경우 DPPH 라디칼 소거활성이 현저히 증가함을 확인할 수 있다. 이때 Lac 색소 메탄올 추출물, Lac 색소 열수 추출물 및 Lac 색소 수용성 추출물의 중량비가 100:20~40:10~30 인 경우, DPPH 라디칼 소거활성이 극대화될 수 있다. In addition, when the Lac pigment methanol extract, the Lac pigment hot water extract, and the Lac pigment water-soluble extract were simultaneously used, it was confirmed that the DPPH radical scavenging activity significantly increased. At this time, when the weight ratio of the Lac pigment methanol extract, the Lac pigment hot water extract, and the Lac pigment water-soluble extract is 100:20 to 40:10 to 30, the DPPH radical scavenging activity can be maximized.
(실시예 3) (Example 3)
Lac 색소 메탄올 추출물 1중량%, 디프로필렌글리콜 3중량%, 카보머 0.2중량%, 폴리글리세릴-10 라우레이트 0.2중량% 및 잔량의 정제수를 혼합하여 화장료 조성물을 제조하였다. A cosmetic composition was prepared by mixing 1% by weight of Lac pigment methanol extract, 3% by weight of dipropylene glycol, 0.2% by weight of carbomer, 0.2% by weight of polyglyceryl-10 laurate, and the remaining amount of purified water.
(실시예 4) (Example 4)
Lac 색소 메탄올 추출물 0.05중량%를 사용한 것을 제외하고는 실시예 3과 동일한 방법으로 화장료 조성물을 제조하였다. A cosmetic composition was prepared in the same manner as in Example 3, except that 0.05% by weight of the Lac pigment methanol extract was used.
(실시예 5) (Example 5)
Lac 색소 메탄올 추출물 3중량%를 사용한 것을 제외하고는 실시예 3과 동일한 방법으로 화장료 조성물을 제조하였다. A cosmetic composition was prepared in the same manner as in Example 3, except that 3% by weight of the Lac pigment methanol extract was used.
(실시예 6) (Example 6)
Lac 색소 메탄올 추출물 1중량% 대신에, Lac 색소 메탄올 추출물 0.7중량% 및 Lac 색소 열수 추출물 0.3중량%를 사용한 것을 제외하고는 실시예 3과 동일한 방법으로 화장료 조성물을 제조하였다. A cosmetic composition was prepared in the same manner as in Example 3, except that 0.7% by weight of the Lac pigment methanol extract and 0.3% by weight of the Lac pigment hot water extract were used instead of 1% by weight of the Lac pigment methanol extract.
(실시예 7) (Example 7)
측백엽 열수 추출물 0.5중량%, 물봉선 열수 추출물 0.5중량% 및 참당귀 열수 추출물 0.5중량%를 추가로 사용한 것을 제외하고는 실시예 3과 동일한 방법으로 화장료 조성물을 제조하였다. A cosmetic composition was prepared in the same manner as in Example 3, except that 0.5% by weight of the hot-water extract of Arborvitae japonica, 0.5% by weight of the hot-water extract of Mulbongseon, and 0.5% by weight of the hot-water extract of Angelica gigas were additionally used.
(비교예 1) (Comparative Example 1)
Lac 색소 메탄올 추출물을 사용하지 않은 것을 제외하고는 실시예 3과 동일한 방법으로 화장료 조성물을 제조하였다. A cosmetic composition was prepared in the same manner as in Example 3, except that the Lac pigment methanol extract was not used.
(관능검사)(sensory test)
20명의 패널을 대상으로 하루에 한번 씩 10일 동안 화장료 조성물을 얼굴에 사용한 후의 보습력, 피부탄력, 주름, 지속성 및 종합적 기호도 평가를 실시하였다. After using the cosmetic composition on the face once a day for 10 days, 20 panelists were evaluated for moisturizing power, skin elasticity, wrinkles, durability, and overall preference.
관능검사는 5점 척도법(5: 매우 우수하다, 4: 우수하다, 3: 보통이다, 2: 나쁘다, 1: 매우 나쁘다)에 따라 실시되었으며, 상기 특성을 조사한 후 이를 산술평균하였다. The sensory test was conducted according to a 5-point scale (5: very good, 4: excellent, 3: average, 2: bad, 1: very bad), and after examining the characteristics, they were arithmetic averaged.
표 2에서 알 수 있듯이, 실시예 3 내지 7은 보습력, 피부탄력, 주름, 지속성 및 종합적 기호도 평가가 우수하다. 특히 실시예 3, 6 및 7은 상기 특성이 가장 우수하다. As can be seen in Table 2, Examples 3 to 7 are excellent in moisturizing power, skin elasticity, wrinkles, durability and overall preference evaluation. In particular, Examples 3, 6 and 7 have the most excellent properties.
반면 비교예 1은 상기 특성이 실시예에 비해 열등함을 확인할 수 있다. On the other hand, Comparative Example 1 can confirm that the properties are inferior to those of Examples.
Claims (6)
A cosmetic composition comprising water, a Lac pigment extract, a moisturizer, a thickener and a surfactant.
상기 화장료 조성물은 Lac 색소 추출물 0.1~2중량%, 보습제 1~10중량%, 점증제 0.1~1중량%, 계면활성제 0.1~1중량 및 잔량의 물을 포함하는 것을 특징으로 하는 화장료 조성물.
According to claim 1,
The cosmetic composition is a cosmetic composition comprising 0.1 to 2% by weight of Lac pigment extract, 1 to 10% by weight moisturizer, 0.1 to 1% by weight thickener, 0.1 to 1% by weight of surfactant and the remaining amount of water.
상기 Lac 색소 추출물은 Lac 색소 열수 추출물 및 Lac 색소 알코올 추출물을 포함하고,
상기 Lac 색소 열수 추출물 및 Lac 색소 알코올 추출물의 중량비는 20~40:60~80 인 것을 특징으로 하는 화장료 조성물.
According to claim 2,
The Lac pigment extract includes a Lac pigment hot water extract and a Lac pigment alcohol extract,
The cosmetic composition, characterized in that the weight ratio of the Lac pigment hot water extract and Lac pigment alcohol extract is 20 ~ 40: 60 ~ 80.
상기 화장료 조성물은 측백엽 추출물 0.1~1중량%를 추가로 포함하는 것을 특징으로 하는 화장료 조성물.
According to claim 3,
The cosmetic composition is a cosmetic composition, characterized in that it further comprises 0.1 to 1% by weight of the extract of cypress japonica.
상기 화장료 조성물은 물봉선 추출물 0.1~1중량%를 추가로 포함하는 것을 특징으로 하는 화장료 조성물.
According to claim 4,
The cosmetic composition further comprises 0.1 to 1% by weight of water bongseon extract.
A cosmetic comprising the cosmetic composition of claim 1.
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