KR20200109745A - a manufacture method of natural hair fixative hair-spray - Google Patents

Abstract

The present invention relates to a method for producing a natural hair fixative hairspray. The method for producing a natural hair fixative hairspray comprises: a lysate production step of mixing water soluble chitosan with purified water (H2O) purified through an ion exchange resin, and dissolving the same until a transparent body is completely dissolved in an agitator; an extract production step of producing an extract including vegetable ethanol and herbal medicinal extracts; a mixed extract production step; and a completed extract production step. According to the present invention, the light fragrances and the safety of hair are ensured, and thus damage to the scalp can be prevented.

Description

Manufacturing method of natural hair fixative hairspray {a manufacture method of natural hair fixative hair-spray}

The present invention relates to a method for producing a natural hair fixative hair spray,

More specifically, after completely dissolving by mixing water solubility chitosan in purified water, 16 kinds of oriental medicine herbs (16 kinds of oriental medicine herbs) are mixed with the extract base for primary aging, followed by primary aging. The purpose of the invention is a mixed extract obtained by mixing the extract with a water solubility chitosan dissolved product and then fermenting the second mixture, and by mixing additional extracts added to the second mixed aging at a certain ratio, It relates to a method for producing a natural hair fixative hair-spray synthesized from a pure natural extract that does not contain any chemical components prepared by adding natural essence oils.

Hair fixatives are ingredients used to fix hair or preserve style, and hair fixatives for the purpose of physically adhering and fixing hair are added with moisture, oil, gloss, and fragrance. It protects the hair and prepares the hairstyle, so it is called a hairdressing agent. Representative hairdressing agents include oily hair oil and pomade, emulsion-type hair cream and set lotion (for maintaining haircut power and hairstyle), and hair spray. Maintains the hairstyle while forming a film on the hair. It is a finishing cosmetic for hair that is used to easily comb and dry hair, and to finish hair setting, hair drying and other hairstyles in an attractive and beautiful style.

In particular, hairspray is a time when the market growth rate is progressing very rapidly due to changes in the social concept of men's image and appearance. In general, standard hair fixation hairspray is mainly octylacrylamide, acrylates, and butylamino. Ethyl methacrylate copolymer, VEA, polyvinyl pyrrolidone, or a super-vinyl copolymer or acrylic resin or vinyl methyl ethyl thereof /Butyl maleate copolymer is used, and silicone alcohol, modified alcohol, phenoxyethanol, sebum, fragrance, etc. are often used as additives that impart flexibility and fragrance. These chemicals have problems that cause nausea, dizziness, and skin problems. In addition, chemical components can cause severe irritation when they come into contact with the skin and eyes, and some compounds have reported toxicity to the respiratory tract and liver. Some products require ventilation due to severe gas odor, and there are many problems that may cause hair loss such as hair damage and various troubles.

In order to solve the above problems, in order to solve the above problems, in preparing a pure natural hair fixative hair spray with no chemical components added, first, after completely dissolving water-soluble chitosan in purified water, 16 kinds of herbal herbs are added to the extract base. Mix and let the first ripening. The purpose of the invention is a mixed extract obtained by mixing water solubility chitosan dissolved in the first ripening extract and secondary ripening, and the second mixed ripening is mixed with additional extracts in a certain ratio to complete. The purpose is to prepare a natural fixative hair spray by synthesizing a quantitative amount of essential oil in the extracted extract. In particular, the present invention has the advantage of being composed of pure natural ingredients and that the extract prepared by dissolving and aging water-soluble chitosan in 16 kinds of herbal extracts absorbs and discharges heavy metals and toxicity, so that it is used as a natural extract that does not irritate the human body at all. It is an object of the present invention to help with scalp damage and hair loss by ensuring a gentle scent and hair safety by using natural essential oils.

In order to achieve the above object, the present invention is one step of preparing various raw materials quantitatively, a clear transparent body that is completely dissolved by mixing water-soluble chitosan in purified water and stirring for 30 minutes, two steps of a finished product, 16 kinds of herbal herbs, purified water, Base extract (butylene glycol) and vegetable ethanol are quantitatively mixed in a certain ratio and put in a sealed aging tank for first aging for 30 days at 20C~30C° (stirring every 10 days) Step 3, Step 3 Extracts are precisely purified Extract 4th step, 2nd step lysate and 4th step extract are quantitatively measured and mixed and put into a sealed aging tank, and the mixed extract is aged for 20 days at an average of 20C~30C°. Process, process 6 It consists of 8 processes in which a natural hair fixative hairspray product is completed by quantitatively synthesizing essential oils in the finished extract in the 7th and 7th processes of the final extract, which quantitatively mixes the added extracts in the mixed extract.

A feature of the present invention is that it does not use any chemical raw materials and uses only pure natural raw materials to realize the fixing power, cleaning power, and safety of hair. In particular, chitosan's strong hair fixation effect, soothing and moisturizing effect of the scalp, washing effect without residual residue, hair that does not spoil, softens hair, soft setting power that does not seem to be brittle, and realizes natural hairstyle with a clean feeling without cloudiness There is an effect.

1 is a manufacturing process diagram of a natural hair fixative hairspray according to an embodiment of the present invention
2 is a photograph of the manufactured product of Example 1, Example 2, and Example 3 of the present invention

Water solubility chitosan, which is the main material according to the present invention, is a natural high molecular material and is the only soluble dietary fiber on the planet having a structure very similar to cellulose. Chitin is a material that is widely distributed in the cell walls of fungi such as shells of crustaceans and insects, fungi, and mushrooms. It is mainly extracted from the shells of crustaceans. Chitosan is used to desorb chi-tin under high temperature, strong alkali conditions. It is obtained by acetylation (D/A), and is a natural polymer material in which more than 5000 glucosamines are bound. Chitosan is obtained by chemically removing more than 70% of the acetyl group (acetyl+基: CH3CO<SUP>) from chitin. It is called this. Since ancient times, it has high human affinity, and especially has the properties of adsorbing heavy metals such as surgical threads, contact lenses, artificial blood vessels, immunity strengthening, aging suppression, disease prevention, and biological rhythm control for wound healing and medical use. In addition, it is ideal for moisturizing the skin, regenerating the skin and fixing the hair. The water-soluble chitosan (water solubility chitosan) is mixed with purified water (H2O) through an ion exchange resin, dissolved in a completely transparent mixture in a stirrer, and prepared for use.

Another additional additive of the present invention is

Acours gramineus extract, Acacia concinna fruit extract,

Elesthep (hexamidine diisethionate), silk amino acids, panthenol, arginin, citric acid, and vegetable ethanol are added to the scalp. By supplying health and nutrition to hair, it has good moisture-proof properties and air permeability, and has a special luster and function of blocking UV rays. In addition, by using a natural extract, Citrus lemon peel oil, you can use it comfortably with a gentle scent.

As described above, the combination of chitosan and natural extracts has excellent healing activity of the scalp and stabilizes cracked hair and hair loss by forming a film on the hair, and it coats the hair to soften it to improve scalp dead skin cells and hair damage. Powerful hair fixation effect, soothing and moisturizing effect of the scalp, washing effect without residual residue, hair that does not spoil and softens, soft setting power that is not brittle, and has the effect of realizing a natural hairstyle with a clean feeling without cloudiness It relates to a method for producing a natural hair fixative hairspray.

The method of manufacturing the natural hair fixative hairspray of the present invention will be described as follows.

(Manufacturing process of natural hair fixative hair spray)

1. First step; Preparation of raw materials

Various raw materials are prepared by quantification.

2. Second process: Preparation of aqueous chitosan solution

Prepare for use by mixing water solubility chitosan with purified water (H2O) purified through an ion exchange resin and completely transparently dissolving in a stirrer.

3. 3rd process: Manufacture of 16 kinds of herbal extracts

In a mixture of purified water (H2O), base extract (butylene glycol), and vegetable ethanol (ethyl alcohol) in a fixed ratio, 16 kinds of herbal herbs are prepared and put in a sealed aging tank 20C°~30C Prepare an extract that was first aged for 30 days (stirred every 10 days) at °. At this time, the contents (16 types of herbal herbs) are stirred at intervals of the 10th day so that the ingredients are sufficiently extracted. In particular, it is not a physical extraction method such as heat extraction or increased pressure extraction, but a pure natural aging extraction method, so that a method that respects the principle of nature is selected.

4. The 4th process: Manufacture of extracts precisely purified 16 kinds of herbal extracts

After purifying the extracts of 16 kinds of herbal herbs in the first manure (sambei mang), the extract is prepared by precisely second-purifying the extract in a second filter unit (paper net). At this time, there are fine particles according to the 16 kinds of herbal herbs, so if it is not carefully refined, it can cause corruption and rancidity over time.

5.Step 5: Manufacture of secondary aging mixed extract of chitosan solution (step 2) and extracts of 16 kinds of herbal herbs (step 4)

The chitosan solution (step 2) and 16 kinds of herbal extracts (step 4) are quantitatively measured and mixed and put in a sealed aging tank to prepare a mixed extract that is aged for a second time at an average of 20C° to 30C° for 20 days. At this time, if chitosan solution and 16 kinds of herbal extracts are mixed and aged for 20 days, due to the characteristics of chitosan, some parts of chitosan appear as sticky white floating matters by adsorbing heavy metals, toxic and waste materials. It is newly born as a pure natural blended extract without degeneration. This mixed extract is an important object of the present invention.

6. The 6th process: Manufacturing of mixed extract by precisely purifying the mixed extract in the 5th process

Step 5 The mixed extract is first refined in a strainer (fine hemp mesh) and then refined in a second sieve (paper screen) to prepare a mixed extract.

7. The 7th process: Manufacture of extract by mixing quantitative amount of additionally added extract in 6th process mixed extract

Step 6 Prepare the final extract by adding iris extract, Cicacai fruit extract, Elesthep (hexamidine dicethionate), silk amino acid, panthenol, arginine, citric acid, and vegetable ethanol to the extract in step 6 and stirred for 20 minutes in a stirrer. do. At this time, add an appropriate amount of citric acid to make the pH 5.5~6.0.

8. Process 8: Manufacture finished products by quantitatively synthesizing essence oil in the 7 process finished extract

Process 7 A natural hair fixative hairspray finished product is manufactured by quantitatively synthesizing essence oil in the finished extract.

Hereinafter, the method of manufacturing the natural hair fixative hairspray of the present invention will be described in more detail through examples and experimental examples.

[Example]

The present invention natural hair fixative hairspray manufacturing method Example 1, Example 2, Example 3

1. Material preparation

Prepare quantitatively the materials required for this manufacture.

2. Preparation of aqueous chitosan solution

Prepare for use by mixing 90 to 95 g% by weight of purified water (H2O) and 5 to 10 g% by weight of water solubility chitosan purified through an ion exchange resin, and dissolving it in a stirrer until it becomes completely transparent. In particular, chitosan is used as the main raw material of the present invention by forming a film on the hair, coating the cracked hair, making it soft, and acting as a fixing agent (setting).

3. Manufacture of 16 kinds of herbal extracts

16 kinds of herbal herbs: Chrysanthemum Idicum Flower, Licorice (Glycyrrhiza Uralensis Root Extract), Sesamum Indicum Seed Extract, Sophora Flavescens Root Extract, Lycium Chinense Extract, Green Tea (Camellia Sinensis Leaf) ), Angelica Gigas Root Extract, Rosemary (Rosmarinus Officinalis), Mulberry Root (Morus Alba Root Extract), Mulberry Branch (Morus Alba Twig Extract), Acorus Gramineus Extract, Plum Tree Leaf (Prunus Mume Leaf Extract), Polygonum Multiflorum Root Extract, Forsythia Koreana Branch/Leaf Extract, Elm Root (Ulmus davidiana var), Cnidium Officinale Root Extract, respectively Prepare 5~6g quantitative %.

Purified water (H2O) 70-75gwt%, base extract (butylene glycol) 10-15gwt%, vegetable ethanol (ethyl alcohol) 5-10g quantitatively mixed in a certain ratio into a sealed aging tank , Here, 5-6 g of each of the 16 kinds of herbal herbs prepared above is added to the aging tank and first aged for 30 days at 20C~30C°. During the maturation period, rotate the contents (16 types of herbal herbs) every 10 days so that the ingredients are sufficiently extracted.

4. After purifying the extract in the first strainer (burmb net), the extract is precisely refined in the second strainer (paper net). At this time, it is careful because fine particles exist according to 16 kinds of herbal herbs. This is because if it is not refined, it can cause corruption and rancidity over time. The 16 kinds of herbal herbs help the hair nourishment and antibacterial activity, and the skin astringent action and capillary blood vessels are cleared. In addition, it promotes metabolism, helps to remove skin epithelial bacteria, moisturizes hair and helps a lot in hair loss.

5. Preparation of secondary aged mixed extract by mixing water-soluble chitosan solution and 16 kinds of herbal extracts

Chitosan solution (2nd step) 50-60g quantitative% and herbal 16 kinds of herbal extracts (4th process) 50-60g quantitative% are quantitatively measured and mixed and put into a sealed aging tank. Prepare. At this time, if chitosan solution and 16 kinds of herbal extracts are mixed and aged for 20 days, due to the characteristics of chitosan, some parts of chitosan appear as a sticky white floating material by adsorbing heavy metals, toxicity and waste. ), and then refined in a secondary strainer (paper net) to create a pure natural blended extract with no alteration in ingredients. This mixed extract is the main object of the present invention.

6. Manufacture of the finished extract by mixing the amount of added extract added to the mixed extract of 16 kinds of chitosan and herbal herbs

Mixed extract 45-50g by weight, Iris extract 5-10g by weight, Shikakai fruit extract 5-10g by weight, Elesthep (hexamidine diisethionate) 1 to 2g by weight, Silk amino acid 1 to 3g by weight , Panthenol 0.5-1g quantitative%, arginine 0.25-0.5g quantitative%, citric acid 0.4-0.6g quantitative%, and vegetable ethanol 10-15g quantitative% are added and stirred in a stirrer for 20 minutes to produce the final extract. At this time, add an appropriate amount of citric acid to make it a pH of 5.5 to 6.0. Arginin is one of the essential amino acids that make up our body and is a component of natural moisturizing factors that exist in the stratum corneum of the skin. In addition, the additional extract contains a large amount of antioxidants and vitamins A, D, K, C, etc., which helps the scalp health and cleanliness, and provides sufficient nutrition and moisture to the hair.

7. Manufacture of finished products by quantitatively synthesizing essence oil in the finished extract

By synthesizing 0.1~0.5g by amount of essence oil in the finished extract, a natural hair fixative, Hair Soup A, is produced.

A feature of the present invention is that it does not use any chemical raw materials, but uses only pure natural raw materials, which has the advantage of realizing the fixing power, cleaning power, and stability of the hair.

A comparison of the embodiments of the present invention (Example 1, Example 2, and Example 3) is shown in Table 1 below.

Material name Example 1 Example 2 Example 3 Chitosan herb 16 kinds mixed extract 50 47 45 Vegetable ethanol 30 33 35 Iris extract 9 9 9 Shikakai extract 7 7 7 Panthenol One One One Elesthep 1.5 1.5 1.5 Arginine 0.5 0.5 0.5 Citric acid 0.8 0.8 0.8 Essence oil 0.2 0.2 0.2 system(%) 100% 100% 100%

As shown in Table 1, the representative ingredients in Examples 1, 2, and 3 are chitosan extract and 16 kinds of herbs extract, mixed extract 50gwt%, 47gwt%, 45gwt% and vegetable ethanol 30gwt%, 33g When carried out with weight% and 35g weight, Example 1 was a cloudy color and 35% of precipitation proceeded, whereas Example 2 was a medium turbid color and 25% of precipitation proceeded, and Example 3 was a transparent color and no precipitation at all. It was manufactured as a very well-dissolved product, and the fixing power was good.

The analysis of Examples 1, 2, and 3 is shown in Table 2 below.

Example Solubility analysis Sedimentation analysis Color analysis Fixation analysis Fixed time analysis Spray degree analysis Example 1 3 3 3 2 3 3 Example 2 2 2 2 One 2 2 Example 3 One One One One 2 One

* Solubility: 1=90% or more, 2=80% or more, 3=70% or more

Sedimentation: 1=95% or more, 2=85% or more, 3=75% or more

Color degree: 1=transparent, 2=cloudy, 3=very cloudy

Fixed force: 1=good, 2=medium, 3=poor

Fixed time: 1=very fast, 2=fast, 3=medium

Spray degree: 1 = very good, 2 = normal, 3 = bad

As shown in Table 2, the analysis result of Example 3 was judged to be the best, and Example 3 was selected as the finished product.

[Experimental example]

Analysis of the experimental results of the finished product in Example 3 of the present invention

As described above, the product manufactured in Example 3 was applied to a total of 25 men (13) and women (12).They were used in Experimental Example 1, Experimental Example 2, Experimental Example 3, Experimental Example 4, Experimental Example 5, and Experimental Example 6. The experiment was conducted with the contents, and the evaluation method was evaluated in 5 stages (1: very good, 2: good, 3: normal, 4: bad, 5: very bad) and set the evaluation value as an average. The contents of the experiment are shown in Table 3 below.

Experiment example Contents male female Average value ranking Experimental Example 1 ingredient One One One One Experiment Example 2 Blowing force One One One One Experiment Example 3 Holding force One 2 1,2 1,2 Experiment Example 4 Fixed time One 2 1,2 1,2 Experiment Example 5 Spray incense 2 One 1,2 1,2 Experimental Example 6 preference One One One One

Since the male and female experiment results in Table 3 above show that the preference is high when viewed as an average value, it is judged that the product of Example 3 is suitable for the blending ratio of 45g% by weight of chitosan and 16 kinds of herbal herbs and 35g% by weight of vegetable ethanol. The finished product of Example 3 tested in Table 3 is shown in the photograph of FIG. 2. As described above, a product prepared by mixing an extract of 16 kinds of herbal herbs with a water-soluble chitosan solution and adding an additionally added extract to the secondary aging mixed extract is born as the natural hair fixative hair spray of the present invention.

Claims (3)

In the method for producing a hairspray, a natural hair fixative according to the present invention, 90-95 g% by weight of purified water (H2O) and 5-10 g% by weight of water solubility chitosan are mixed through an ion exchange resin to be completely transparent in a stirrer. 2 process of manufacturing the melt until it becomes

Purified water (H2O) 70-75g% by weight, base extract (butylene glycol) 10-15g% by weight, vegetable ethanol (ethyl alcohol) 5-10g in a predetermined ratio, put a mixture in a sealed aging tank , Here, 5 to 6 g of each of the 16 kinds of herbal herbs prepared above were added to the aging tank, and the extract was first aged at 20 C to 30 C for 30 days.

Chitosan solution (2nd step) 50-60g quantitative% and herbal 16 kinds of herbal extracts (3rd step) 50-60g quantitative% are quantitatively measured and blended and put into a sealed aging tank and then aged for 20 days at an average of 20C to 30C. Manufacturing 5 process.

Add additional extract to the mixed extract and stir in a stirrer for 20 minutes.
Method for producing a hairspray composed of natural hair fixative
In paragraph 1
Purified water (H2O) 70-75gwt%, base extract (butylene glycol) 10-15gwt%, vegetable ethanol (ethyl alcohol) 5-10g 5-6g quantitative% of each of 16 herbal herbs are sealed and aged A method for producing a natural hair fixative hairspray characterized by primary aging for 30 days at 20C° to 30C°
In paragraph 1
Mix 50-60g quantitative% of chitosan solution (2nd step) and 50-60g quantitative% of 16 herbal herbal extracts (3rd step) and put them in a sealed aging tank and then aging for 20 days at an average of 20C°~30C° for 20 days to prepare the mixed extract. A method of manufacturing a natural hair fixative hairspray characterized by manufacturing

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