KR20190096088A - Production method for natural toothpaste using lettuce - Google Patents

Abstract

The present invention relates to a method for preparing a natural lettuce toothpaste composition which is harmless to a human body and has an improved tooth whitening function. The method comprises: a first step of preparing a toothpaste mixture; a second step of washing a lettuce; a third step of mixing lettuce powder with the toothpaste mixture; a fourth step of mixing propolis as a natural preservative, a grapefruit seed extract, an apple wash, dental abrasion silica, and kaolin clay white with the toothpaste mixture; and a fifth step of preparing a natural lettuce toothpaste composition.

Description

 TECHNICAL METHOD FOR NATURAL TOOTHPASTE USING LETTUCE

The present invention relates to a method for preparing lettuce natural toothpaste composition using lettuce.

Generally, discoloration of teeth occurs due to various factors such as food waste, nicotine, coffee, etc. are deposited on the tooth surface, tartar or deposit on the tooth surface, periodontal disease or long-term medication.

Recently, various whitening toothpastes have been commercialized in order to prevent and prevent tooth discoloration, and a whitening effect is obtained by physically polishing the tooth surface by containing a strong abrasive, or chemical action by using peroxide as an active ingredient. The method of obtaining a whitening effect is known.

By repeated use of this whitening toothpaste for a long time, there is a problem that the teeth are excessively worn to become irritable teeth or cause abrasion, and the peroxide is decomposed to generate gas or cause strong irritation to the gums and due to chemical action with other ingredients. It causes several problems.

In addition, as a drug for periodontal disease, triclosan, aminocaproic acid, tocopherol, catechin, and bamboo salt were used, but the effect was insignificant.

Therefore, the necessity of a natural toothpaste manufacturing method that can improve the whitening function while harmless to the human body by using natural materials rather than artificial chemical composites.

1. Korean Patent Publication No. 10-2012-0011351 (2012.12.05)

The purpose of the present invention to solve this problem is to produce a natural lettuce toothpaste using natural materials other than artificial chemical compounds, to improve the teeth whitening function and improve the feeling of use, and to keep the mouth clean, harmless to the human body In addition to improving the bactericidal power for preventing periodontal disease or inflammation.

In addition, the present invention, the purpose of maximizing the safety of the toothpaste by removing the harmful substances such as foreign substances or pesticides on the lettuce when washing the lettuce to the maximum.

In addition, an object of the present invention is to improve the feeling of use of toothpaste by inhibiting the loss of flavor of lettuce by preparing and mixing lettuce powder through lyophilization to minimize the loss of functional substances contained in lettuce.

In addition, an object of the present invention is to produce a natural toothpaste at a relatively low cost by using lettuce can be obtained easily and inexpensively, so that the mass production is easy to improve the economics.

The object of the present invention is not limited to those mentioned above, and other objects, which are not mentioned above, will be clearly understood by those skilled in the art from the following descriptions.

According to an embodiment of the present invention for achieving the above object, in the lettuce natural toothpaste composition manufacturing method, after heating 35 to 45 parts by weight of organic glycerin with respect to 100 parts by weight of the total composition, 2 to 8 xylitol (xylitol) 1 part by weight of Xanthan Gum is added to dissolve and 1 to 5 parts by weight of Xanthan Gum to prepare a mixed toothpaste mixture, and the sterilization of lettuce, 3 minutes ~ at a temperature of minus 20 degrees ~ 30 degrees After rapid freezing for 5 minutes, the foreign matters adhered to the surface of the lettuce are separated by vaporization using steam which is heated at a temperature of 50 ° C. to 70 ° C. or below, and the separated particulate matter is adsorbed through the zeolite disposed around the lettuce. The second step of performing the washing of the lettuce, and dried the lettuce washed from the second step, the dried lettuce is ground by grinding 0.5 ~ 1.5 parts by weight of powdered lettuce powder A third step of mixing the mixture, from the third step to the toothpaste mixture from 1 to 3 parts by weight of propolis as a natural preservative, 0.5 to 1.5 parts by weight of grapefruit seed extract, apple wash as a natural surfactant ( Protel APL) 6 to 10 parts by weight, a fourth step of mixing 1-3 parts by weight of dental abrasion silica as a natural tooth polishing agent, and 1 to 3 parts by weight of kaolin clay white, and the agent The toothpaste mixture is added to the prepared stirring tank from step 4, and gradually added by alternating 2 to 8 parts by weight of dental thickener silica and purified water as a natural caking agent, and selected from the dental viscosity silica and purified water. Fabric comprising a fifth step of preparing a natural toothpaste composition of lettuce by mixing any one and the toothpaste mixture in a high vacuum of 10-3 Torr for 1 minute to 3 minutes It provides a process for the production of lettuce dentifrice composition method.

In addition, in the third step, the lettuce is dried for 2 hours in an electric oven having an internal temperature of 45 degrees, and the second step is freeze-dried for 1 hour at a temperature of minus 20 degrees to 40 degrees using a freeze dryer. It can provide a natural lettuce toothpaste composition manufacturing method comprising a.

According to the present invention, by manufacturing a natural lettuce toothpaste using natural materials other than artificial chemical compounds, it is harmless to the human body, improves the whitening function of teeth, improves the feeling of use, and keeps the mouth clean, periodontal It has the effect of improving the bactericidal power for preventing disease or inflammation.

In addition, the present invention has the effect of maximizing the safety of the toothpaste by removing harmful components such as foreign substances or pesticides on the lettuce when the lettuce is washed.

In addition, the present invention has the effect of suppressing the loss of the flavor of the lettuce to improve the feel of the toothpaste by preparing and mixing the lettuce powder through lyophilization to minimize the loss of the functional material contained in the lettuce.

In addition, the present invention can produce a natural toothpaste at a relatively low cost by using lettuce can be obtained easily and inexpensively, so that the mass production is easy to improve the economics.

The effects of the present invention are not limited to those mentioned above, and other effects that are not mentioned will be clearly understood by those skilled in the art from the following description.

1 is a flow chart of a method for manufacturing a natural lettuce toothpaste composition according to an embodiment of the present invention.

Hereinafter, exemplary embodiments of the present invention will be described in detail with reference to the accompanying drawings. Advantages and features of the present invention and methods for achieving them will be apparent with reference to the embodiments described below in detail with the accompanying drawings. However, the present invention is not limited to the embodiments disclosed below, but may be implemented in various forms, and only the embodiments are intended to complete the disclosure of the present invention, and the general knowledge in the art to which the present invention pertains. It is provided to fully inform the person having the scope of the invention, which is defined only by the scope of the claims. Like reference numerals refer to like elements throughout.

Unless otherwise defined, all terms (including technical and scientific terms) used in the present specification may be used in a sense that can be commonly understood by those skilled in the art. In addition, the terms defined in the commonly used dictionaries are not ideally or excessively interpreted unless they are specifically defined clearly.

The terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. In this specification, the singular also includes the plural unless specifically stated otherwise in the phrase. As used herein, "comprises" and / or "comprising" does not exclude the presence or addition of one or more other components in addition to the mentioned components.

Hereinafter, a method for preparing lettuce natural toothpaste composition according to an embodiment of the present invention will be described with reference to the accompanying drawings.

Lettuce natural toothpaste composition manufacturing method according to an embodiment of the present invention by producing a natural lettuce toothpaste using natural materials other than the artificial chemical compound, the tooth whitening function is improved while improving the feeling of use and clean mouth, Not only to maintain, but also to improve the bactericidal power for preventing periodontal disease or inflammation, and natural toothpaste can be manufactured at a relatively low cost by using easily and inexpensive lettuce, so that mass production is easy and economic efficiency is improved. In order to prepare a natural toothpaste composition for lettuce, it is to proceed to the first step (S10) to the fifth step (S50).

Specifically, the first step (S10) is a step of preparing a toothpaste mixture, after heating 35 to 45 parts by weight of organic glycerin with respect to 100 parts by weight of the total composition, xylitol is dissolved by adding 2 to 8 parts by weight of xylitol , 1 to 5 parts by weight of xanthan gum is added to prepare the toothpaste mixture.

The second step (S20) is a step of washing the lettuce, sterilizing the lettuce, and after freezing for 3 minutes to 5 minutes at a temperature below minus 20 degrees ~ 30 degrees, at a temperature below 50 degrees ~ 70 degrees The washing step is performed by separating particulate foreign matters on the surface of the lettuce using steam which is heated and evaporated. The separated particulate foreign matters may be adsorbed through the zeolite disposed around the lettuce.

This second step (S20) may be provided to perform the washing in a manner to separate the particulate foreign matter on the lettuce surface through the water vapor generated by the heating of the zeolite.

That is, there is a problem that the lettuce is physically damaged by the hydraulic pressure when the water is usually fired on the lettuce surface to wash the lettuce.

Therefore, in order to prevent this, while minimizing the physical damage caused by water pressure when washing the lettuce to remove harmful substances such as foreign substances or pesticides on the lettuce as possible, as a result to maximize the safety of the use of natural lettuce toothpaste.

In this case, in the second step (S20), when the lettuce is frozen in a condition outside the temperature range of minus 20 degrees to 30 degrees during the process, the tissue forming the lettuce may be greatly damaged.

In addition, when the lettuce is frozen from the second step (S20), if the lettuce is frozen under a time condition exceeding the time range of 3 minutes to 5 minutes, tissue damage of the lettuce may gradually increase. have.

For example If the lettuce is frozen for more than 5 minutes at temperatures below minus 30 degrees, damage to the lettuce tissue may increase, and if the lettuce is frozen within 3 minutes at minus 20 degrees or more, the fragrance loss of lettuce will increase. Cleaning can be very difficult.

In other words, it is difficult to wash the lettuce, since the loss of natural fragrance of lettuce, it is most preferable to perform the rapid freezing of lettuce by maintaining the temperature range of the minus 20 degrees to 30 degrees or the time range of 3 minutes to 5 minutes Do.

In addition, when heating the rapidly frozen lettuce from the second step (S20), when the heating is performed at a temperature condition outside the temperature range of 50 degrees to 70 degrees, rapid steam generation may occur or water vapor generation may be reduced. There is a number.

Therefore, due to the pressure of the steam applied to the lettuce, the fibrous tissues forming the lettuce may be destroyed, or it may take a long time to wash, and the fragrance of the whole lettuce may be greatly lost. Preference is given to performing heating under temperature conditions.

The third step (S30) is a step of drying the lettuce washed from the second step (S20), crushing the dried lettuce and mixing 0.5 ~ 1.5 parts by weight of powdered lettuce powder in the toothpaste mixture.

In this case, the third step (S30) may include the step of lyophilizing using a freeze dryer when the lettuce is dried.

For example, in the third step S30, when the lettuce is dried after washing the lettuce, the lettuce is dried for two hours in an electric oven at a temperature condition in which the internal temperature is set to 45 degrees.

If the temperature condition set in the electric oven is out of the range of the image 45 degrees, it may cause a problem of large loss of nutrients or functional substances of lettuce, it is preferable to maintain the temperature conditions of the image 45 degrees.

Next, the second lyophilizer is dried for 1 hour at a temperature of minus 20 degrees to 40 degrees, and the lettuce is frozen to freeze the lettuce through a drying program of a predetermined freeze dryer, that is, a sublimation of water using sublimation. The drying process is performed.

Thereafter, the dried lettuce may be prepared by pulverizing and mixing the lettuce powder prepared by pulverizing in the toothpaste mixture.

Accordingly, the lettuce is dried on the first and second stages by maintaining the appropriate temperature and time conditions to minimize the loss of the functional substance contained in the lettuce, and the lettuce powder prepared through the dried lettuce By mixing in the toothpaste mixture, the loss of the flavor of the lettuce can be suppressed, thereby greatly improving the feel of the toothpaste.

The fourth step (S40) is 1 to 3 parts by weight of propolis as a natural preservative in the toothpaste mixture from the third step (S30), 0.5 to 1.5 parts by weight of grapefruit seed extract, apple as a natural surfactant 6 to 10 parts by weight of Wash (Protel APL), 1 to 3 parts by weight of dental abrasion silica (natural abrasion silica), and 1 to 3 parts by weight of kaolin clay white (kaolin clay white) is mixed.

That is, the fourth step (S40) is to minimize the artificial chemicals in the toothpaste mixture and to mix the natural substances in the toothpaste mixture, as a result, when using the lettuce natural toothpaste composition, it is possible to ensure excellent safety harmless to the human body do.

In addition, the fourth step (S40) is a flavoring agent in the toothpaste mixture, any one selected from lemon essential oil (lemon essential oil), peppermint essential oil (peppermint essential oil), spearmint essential oil (spearmint essential oil) As it comprises the step of adding, the flavoring agent added to the toothpaste mixture can greatly improve the feel of the toothpaste, it is possible to significantly reduce the rejection even when the infant or child use.

In the fifth step (S50), the toothpaste mixture is added to the prepared stirred tank from the fourth step, and 2-8 parts by weight of dental thickener silica and purified water are gradually added alternately as a natural binder. However, the dental viscous silica and any one selected from the purified water and the toothpaste mixture is mixed for 1 minute to 3 minutes at a high vacuum of 10-3 Torr to prepare a natural natural toothpaste composition as a result to obtain a pasty composition It is

Here, the reason for mixing any one selected from the dental viscous silica and the purified water and the toothpaste mixture from the fifth step (S50) in a high vacuum condition of 10-3 Torr for 1 minute to 3 minutes is a smooth mixing of the mixture To make this happen.

In addition, in order to remove bubbles that may be present in the mixture as much as possible, if the mixing is performed outside the above conditions, there may be a problem that the probability of failure is greatly increased due to the deterioration of the mixture and poor mixing. .

Therefore, it is preferable to perform mixing under suitable conditions in which any one selected from the dental viscous silica and the purified water and the toothpaste mixture are mixed under a high vacuum condition of 10-3 Torr for 1 minute to 3 minutes.

As a result, the lettuce natural toothpaste composition according to the embodiment of the present invention configured as described above is manufactured by using natural materials other than artificial chemical composites to manufacture natural lettuce toothpaste, which is harmless to the human body and improves the whitening function and improves the feeling of use, Not only keeps clean, but also improves sterilization for preventing periodontal disease or inflammation, and maximizes safety when using toothpaste by removing harmful substances such as foreign substances or pesticides on lettuce. In order to minimize the loss of functional substances contained in lettuce, the lettuce powder is prepared and mixed through lyophilization, thereby suppressing the loss of the fragrance of lettuce to improve the feel of toothpaste, and can be easily and cheaply available lettuce Can be used to manufacture natural toothpaste at a relatively low cost. It is an invention having the effect of making mass production easy and improving economics.

Although embodiments of the present invention have been described above with reference to the accompanying drawings, those skilled in the art to which the present invention pertains may implement the present invention in other specific forms without changing the technical spirit or essential features thereof. I can understand that. Therefore, it should be understood that the embodiments described above are exemplary in all respects and not restrictive.

Claims (2)

In the lettuce natural toothpaste composition manufacturing method,
Toothpaste mixture mixed with 35 to 45 parts by weight of organic glycerin based on 100 parts by weight of total composition, followed by dissolving by adding 2 to 8 parts by weight of xylitol, and 1 to 5 parts by weight of Xanthan Gum. Preparing a first step;
Sterilize the lettuce, rapidly freeze at minus 20 ~ 30 ℃ for 3 ~ 5 minutes, heat at 50 ℃ ~ 70 ℃, and separate the foreign matters on the surface of the lettuce using evaporated water vapor. A second step of separating and removing the particulate foreign matter by adsorbing through the zeolite disposed around the lettuce to perform the washing of the lettuce;
Drying the lettuce washed from the second step, and crushing the dried lettuce to mix 0.5 to 1.5 parts by weight of the powdered lettuce powder in the toothpaste mixture;
From the third step to the toothpaste mixture 1 to 3 parts by weight of propolis as a natural preservative, 0.5 to 1.5 parts by weight of grapefruit seed extract, 6 to 10 parts by weight of Apple Wash (Protel APL) as a natural surfactant, A fourth step of mixing 1-3 parts by weight of dental abrasion silica and 1 to 3 parts by weight of kaolin clay white as a natural tooth polishing agent; And
The toothpaste mixture is added to the prepared stirring tank from the fourth step, and gradually added by alternating 2-8 parts by weight of dental thickener silica and purified water as natural binders, the dental viscosity silica and the purified water Method of producing a natural lettuce toothpaste composition comprising a; and a fifth step of mixing the selected one of the toothpaste mixture with a high vacuum of 10-3 Torr for 1 minute to 3 minutes; .
The method of claim 1,
The third step includes drying the lettuce, first drying for 2 hours in an electric oven at which the internal temperature is set to 45 degrees, and lyophilizing for 1 hour at a temperature of minus 20 to 40 degrees using a lyophilizer. Natural lettuce toothpaste composition manufacturing method characterized in that.

Images