KR20150094851A - Soap composition comprising pine pollen salt - Google Patents

Soap composition comprising pine pollen salt Download PDF

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Publication number
KR20150094851A
KR20150094851A KR1020140015237A KR20140015237A KR20150094851A KR 20150094851 A KR20150094851 A KR 20150094851A KR 1020140015237 A KR1020140015237 A KR 1020140015237A KR 20140015237 A KR20140015237 A KR 20140015237A KR 20150094851 A KR20150094851 A KR 20150094851A
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salt
soap
weight
soap composition
black garlic
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KR1020140015237A
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Korean (ko)
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KR101599123B1 (en
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김동청
인만진
김재광
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태안군소금명품화사업단
청운대학교산학협력단
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Priority to KR1020140015237A priority Critical patent/KR101599123B1/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/02Inorganic compounds
    • C11D7/04Water-soluble compounds
    • C11D7/10Salts

Abstract

The present invention relates to a soap composition containing pine pollen salt and, more specifically, to a soap composition containing pine pollen salt, which can contribute to an increase of the income of a pine pollen salt farm and to stimulation of a local economy because the soap composition is not soft and does not split, and has excellent whitening effects, moisturizing abilities and antibacterial activities.

Description

송화소금을 포함하는 비누조성물{SOAP COMPOSITION COMPRISING PINE POLLEN SALT}SOAP COMPOSITION COMPRISING PINE POLLEN SALT [0002]

본 발명은 송화소금을 포함하는 비누조성물에 관한 것으로, 보다 상세하게는 무르거나 쪼개짐이 발생하지 않으면서 미백효과와 보습력 및 항균활성이 우수하여 송화소금 농가의 소득증대 및 지역경제 활성에 기여할 수 있는 송화소금을 포함하는 비누조성물에 관한 것이다.
More particularly, the present invention relates to a soap composition comprising a salt of sesame, and more particularly, to a soap composition which is excellent in whitening effect, moisturizing power and antimicrobial activity without causing ripening or cleavage, The present invention relates to a soap composition comprising sesame salt.

태안반도의 천일염은 염도가 낮고 미네랄이 풍부해 김치 등 전통 발효식품을 만드는 데 훨씬 우수한 효과를 보이며, 특히 태안반도는 소나무가 산림의 90% 이상을 차지해 송화소금 생산의 최적지로써, 송화소금은 5월 송화가 염전에 내려앉는 시점에 맞춰 생산하는 것으로 칼슘과 비타민이 풍부해 노화방지와 지방간 해소, 피부미용 등에 효능이 있는 것으로 알려져 있다.In Taean Peninsula, Taean Peninsula is the best place for the production of pineapple salt, because the pine tree occupies more than 90% of the forest. It is produced according to the time when the pine mushroom falls down before the salt, and is rich in calcium and vitamins, and it is known to be effective for preventing aging, eliminating fatty liver, and skin beauty.

하지만, 현재까지의 소금산업은 소금 자체의 판매에 집중되어 있어, 소금 생산자의 자생력과 경쟁력 확보를 위해 후속 연계사업 추진이 요구되는 상황이므로 그 방안으로서 송화소금을 활용한 식품 및 제품 개발이 필요한 상황이다.
However, to date, the salt industry is concentrated on the sales of salt itself, and it is necessary to pursue a follow-up business in order to secure the self-sufficiency and competitiveness of the salt producers. Therefore, to be.

본 발명은 상기한 바와 같은 종래기술이 가지는 문제를 해결하기 위해 안출된 것으로, 그 목적은 무르거나 쪼개짐이 발생하지 않으면서 미백효과와 보습력 및 항균활성이 우수하여 송화소금 농가의 소득증대 및 지역경제 활성에 기여할 수 있는 송화소금을 포함하는 비누조성물을 제공함에 있다.
The object of the present invention is to solve the problems of the prior art as described above. The object of the present invention is to provide a method for improving the whitening effect, moisturizing power and antimicrobial activity without causing ripening or cleavage, Which is capable of contributing to the activity of the soap composition.

상기한 바와 같은 본 발명의 기술적 과제는 다음과 같은 수단에 의해 달성되어진다.The technical problem of the present invention as described above is achieved by the following means.

(1) 송화소금을 활성성분으로 포함하는 비누조성물.
(1) A soap composition comprising sesame salt as an active ingredient.

(2) 상기 (1)에 있어서,(2) In the above (1)

송화소금은 0.1 중량% 이상 0.2 중량% 미만으로 첨가되는 것을 특징으로 하는 비누조성물.
Wherein the salt is added in an amount of not less than 0.1% by weight and less than 0.2% by weight.

(3) 상기 (1)에 있어서,(3) In the above (1)

송화소금은 흑마늘 농축액을 송화소금에 혼합하고 건조한 흑마늘 송화염인 것을 특징으로 하는 비누조성물.
Wherein the salt of sesame is a mixture of black garlic concentrate and sesame salt and dried black sesame seed flour.

상기와 같이 본 발명에 의하면, 무르거나 쪼개짐이 발생하지 않으면서 미백효과와 보습력 및 항균활성이 우수하여 송화소금 농가의 소득증대 및 지역경제 활성에 기여할 수 있는 송화소금을 포함하는 비누조성물을 생산할 수 있다.
As described above, according to the present invention, it is possible to produce a soap composition containing Pineapple Salt, which is excellent in whitening effect, moisturizing power and antibacterial activity without causing ripening or cleavage, have.

도 1은 본 발명의 실시예 1에 따라 제조한 송화소금을 포함하는 비누의 제품사진.
도 2는 본 발명의 실시예 2에 따라 제조한 송화소금을 포함하는 비누의 제품사진.
Fig. 1 is a photograph of a product of soap comprising the salt of pine prepared according to Example 1 of the present invention. Fig.
FIG. 2 is a photograph of a product of soap containing the salt of Pineapple prepared according to Example 2 of the present invention. FIG.

이하 본 발명의 내용을 보다 상세하게 설명하면 다음과 같다.
Hereinafter, the contents of the present invention will be described in more detail.

본 발명에 사용되는 송화소금은 특별한 종류의 것으로 한정되는 것은 아니나, 바람직하게는 태안반도에서 생산되어지는 송화소금으로 하는 것이 좋다. 보다 바람직하게는 흑마늘 농축액과 상기 송화소금을 혼합하여 건조한 흑마늘 송화소금을 사용하는 것으로, 흑마늘 송화소금의 제조과정을 아래와 같다.
Although the salt to be used in the present invention is not limited to a particular kind, it is preferable that the salt is produced from Tainan. More preferably, the dried garlic sauce prepared by mixing the black garlic concentrate and the safflower salt is used. The process for producing safflower safflower is as follows.

(1) 준비단계(1) preparation step

재료가 되는 흑마늘을 파쇄하여 자루에 넣고 재료가 밖으로 빠져 나오지 못하도록 한다. 재료가 되는 흑마늘은 건조시킨 흑마늘 뿐만 아니라 생 흑마늘도 사용할 수 있다. 이때, 흑마늘의 파쇄의 정도는 파쇄된 흑마늘이 필터기능을 수행하는 자루의 천 구멍을 빠져 나오지 않을 정도일 것이 요구된다.
Crush the black garlic as a material and place it in a bag so that the material does not come out. Black garlic as a material can be used not only as dried black garlic but also raw black garlic. At this time, the degree of crushing of the black garlic is required to be such that the crushed black garbage does not come out of the hole of the bag performing the filter function.

(2) 추출단계(2) Extraction step

상기 흑마늘이 담긴 필터용 자루를 통상적인 추출기에 넣고, 물을 부은 후 밀봉한 다음 추출기 내의 물을 순환시키면서 일정 시간 끓여서 흑마늘 성분을 추출한다.The filter bag containing the black garlic is placed in a conventional extractor, the water is poured and then sealed. The water in the extractor is circulated and boiled for a predetermined time to extract the black garnet component.

이때 추출과정에 사용되는 물의 양은 사용되는 재료가 건조한 흑마늘일 경우 중량비로 5~20배수가 적당하며, 생 흑마늘일 경우에는 중량비로 1~5배수가 바람직하다.In this case, the amount of water used in the extraction process is preferably 5 to 20 times as much as the weight of dried black garlic, and 1 to 5 times as large as the weight of raw black garlic.

추출기는 식물체나 동물체 등의 성분을 추출하는 데 흔히 사용되는 압력추출기이면 충분하고, 추출 온도는 80℃~120℃, 추출시간은 60분~480분, 바람직하게는 120분으로 조정하고 추출기 내의 물이 순환되도록 조정한 후 추출기의 일반적인 추출방법에 따라 추출되도록 하면 된다.It is sufficient that the extractor is a pressure extractor commonly used for extracting components such as plants and animals, and the extraction temperature is 80 to 120 DEG C, the extraction time is 60 to 480 minutes, preferably 120 minutes, And then extracted according to a general extraction method of the extractor.

파쇄한 재료를 필터용 자루에 넣은 후 추출기 내의 물을 순환시키면서 고온 및 고압으로 추출함으로써 흑마늘에서 성분을 효과적으로 추출하고, 이 후 분리단계에서 추출액과 재료찌꺼기를 쉽고 완전하게 분리할 수 있다는 장점을 제공한다.
It provides the advantage of extracting the ingredients effectively from black garlic by extracting the crushed materials into the filter bag and circulating the water in the extractor and extracting them at high temperature and high pressure, and then separating the extract and the material debris easily and completely in the separation step do.

(3) 분리단계(3) Separation step

흑마늘 추출액을 흑마늘 고형물로부터 분리하여 수거하는 단계이다. 추출단계 완료 후 사용된 추출기의 배출 콕크를 개방하면 압력추출기 내부 압력과 대기압 간의 압력차에 의해 추출기 내의 흑마늘 추출액이 필터용 자루의 고형물과 분리되어 추출기 밖으로 완전히 배출된다.The black garlic extract is separated from the black garlic solid and collected. When the discharge cock of the extractor is opened after the completion of the extraction step, the black garlic extract in the extractor is separated from the solids of the filter bag by the pressure difference between the pressure inside the pressure extractor and the atmospheric pressure, and is completely discharged from the extractor.

이때 자루에 남은 고형물 찌꺼기는 거의 탈수된 상태로 회수되므로 폐기처리하기가 용이하다.
At this time, the solid residue remaining in the bag is recovered in a dehydrated state, so that it is easy to dispose of it.

(4) 농축단계(4) Concentration step

흑마늘 추출액을 농축하는 과정으로, 본 발명에서는 바람직하게는 가용성 고형분이 30~40 Brix 가 되도록 농축한다.
In the present invention, the concentrate is preferably concentrated so that the soluble solid content is 30 to 40 Brix.

(5) 흑마늘 농축액과 송화염의 혼합물의 제조 (5) Preparation of a mixture of black garlic concentrate and callus flame

상기 단계 (4)에서 얻은 흑마늘 농축액을 송화염의 중량 대비 1~9 중량%, 바람직하게는 2~4 중량%, 보다 바람직하게는 3 중량%로 하여 송화염에 첨가하고 혼합기인 V 믹서(V-Mixer)에 넣어 혼합한다. 1 중량% 미만으로 첨가시 첨가에 따른 효과가 극히 미미할 뿐 아니라 10 중량%를 초과하여 흑마늘 농축액을 첨가할 경우에는 케이킹이 발생하여 상품가치를 현저히 떨어뜨릴 우려가 있다.
The concentration of the black garlic concentrate obtained in the step (4) is adjusted to 1 to 9% by weight, preferably 2 to 4% by weight, and more preferably 3% by weight based on the weight of the flame. -Mixer) and mix. When the content is less than 1% by weight, the effect of addition is very small. In addition, when the concentrated black gum is added in an amount exceeding 10% by weight, caking may occur and the product value may be considerably lowered.

(6) 건조단계(6) Drying step

상기 흑마늘 농축액과 송화염의 혼합물을 건조하여 흑마늘 송화염을 얻는 단계로써, 건조는 자연풍을 이용하거나, 열풍 건조기를 이용할 수 있다(70~80℃에서 2~6시간).
The mixture of the black garlic concentrate and the flame is dried to obtain a black garlic flame. The drying can be performed using a natural air or a hot air dryer (2 to 6 hours at 70 to 80 ° C).

(7) 사별(7) Bereavement

상기 과정 (6)을 통해 건조된 흑마늘 송화염을 크기별로 사별하고, 바람직하게는 일정 크기의 흑마늘 송화염을 사별한다.
In step (6), dried black gourd shoots are sieved by size, preferably black gourd shoots of a certain size are shed.

본 발명에서는 상기 송화소금(혹은 흑마늘 송화소금)이 활성성분으로 함유되며, 바람직하게는 비누 조성물의 중량을 기준으로 0.05 중량% 이상 0.2 중량% 미만으로 첨가되어진다. 송화소금의 첨가로 인하여 미백효과와 보습력 및 항균활성이 개선되어지며, 만일 0.05 중량% 미만으로 첨가될 경우에는 송화소금의 첨가로 인한 상기 미백, 보습 내지 항균활성에 대한 개선효과를 기대하기 어렵고, 0.2 중량% 이상으로 첨가할 경우 무르거나 쪼개짐이 발생하여 상품적 가치가 현저히 떨어질 우려가 있다. 보다 바람직하게는 0.1 중량%이다.
In the present invention, the salted salted fish (or black sesame salted salted fish) is contained as an active ingredient, preferably 0.05% by weight or more and less than 0.2% by weight based on the weight of the soap composition. The addition of sesame salt improves the whitening effect, the moisturizing power and the antibacterial activity. If it is added in an amount of less than 0.05% by weight, it is difficult to expect an improvement effect on the whitening, moisturizing or antimicrobial activity due to the addition of the salt, If it is added in an amount of 0.2% by weight or more, the product may be broken or cracked and the product value may be significantly lowered. More preferably 0.1% by weight.

상기와 같이 송화소금은 비누조성물에 첨가하여 사용할 경우 미백, 보습 내지 항균활성에 대한 개선효과를 제공하지만, 이와 더불어 송화소금이 갖고 있는 특유의 생리활성을 피부를 포함한 인체내에 제공하게 되어 국민건강의 증진을 함께 도모할 수 있는 장점을 제공하게 된다.
As described above, when the salt is added to a soap composition, it provides an improvement effect on the whitening, moisturizing and antibacterial activity. In addition, the unique physiological activity of the salt is provided in the human body including skin. It is possible to provide the advantage of being able to simultaneously promote the promotion.

본 발명에서 비누조성물은 특별한 한정을 요구하지는 않으며, 다음과 같은 과정에 의해 얻을 수 있다. The soap composition in the present invention does not require any particular limitation and can be obtained by the following procedure.

송화소금 0.05 중량% 이상 0.2 중량% 미만을 통상적으로 사용되는 비누베이스 (예를 들어, 우지와 야자유에 가성소다를 첨가), 향료, 보습제, 기포제 등과 함께 혼합한 것을 분쇄기를 이용하여 미분쇄한다.A mixture of 0.05% by weight or more and less than 0.2% by weight of sesame salt with a commonly used soap base (for example, adding caustic soda to woji and palm oil), flavor, moisturizing agent, foaming agent and the like is finely pulverized using a pulverizer.

상기 비누베이스는 지방산을 65∼68℃로 가열 용해한 후 820∼87℃에서 알칼리염을 첨가하여 비누화 반응을 실시하고, 상층부분만을 취하여 진한 소금물로 수회 세척한 후 이를 진공 건조하여 수분함량이 15%정도가 되도록 하면 용이하게 얻을 수 있다.The soap base was prepared by heating and dissolving the fatty acid at 65 to 68 ° C, adding an alkali salt at 820 to 87 ° C to saponify, collecting the upper layer of the soap base, washing it with brine several times and vacuum drying it to obtain a water content of 15% Of the total amount of water.

이때, 상기 비누베이스로는 지방산계 비누베이스, 합성 계면활성제 비누베이스 또는 상기 지방산계 비누베이스와 합성계면활성제 비누베이스가 혼합된 것을 사용할 수 있다.At this time, as the soap base, a fatty acid soap base, a synthetic surfactant soap base, or a mixture of the fatty acid soap base and a synthetic surfactant soap base may be used.

지방산계 비누베이스는 야자유, 팜유, 대두유, 피마자유, 올리브유, 팜핵유 등에서 선택되는 식물유와 우지, 돈지, 어유 등에서 선택되는 동물 유지를 단독 또는 혼합하여 이를 알칼리염과 비누화반응을 통해 용이하게 얻을 수 있다. 합성 계면활성제 비누베이스로는 소듐라우릴설포네이트, 알킬벤젠설포네이트의 소듐염, 소듐코코일이세티오네이트, 아실글루타메이트의 알칼리금속염 등에서 선택되는 통상의 것을 사용할 수 있다. 또한 상기 지방산계 비누베이스와 합성계면활성제 비누베이스를 각각 혼합하여 사용할 수도 있다.The fatty acid-based soap base is easily obtained by saponifying the vegetable oil selected from palm oil, palm oil, soybean oil, castor oil, olive oil, palm kernel oil, and animal fats selected from tallow, lard and fish oil, have. As the synthetic surfactant soap base, conventional ones selected from sodium lauryl sulfonate, sodium salt of alkylbenzene sulfonate, sodium cocoyl isethionate, and alkali metal salts of acyl glutamate can be used. The fatty acid-based soap base and the synthetic surfactant-based soap base may be mixed with each other.

본 발명에 따른 비누 조성물은 이외에도 향료, 색소, 살균제, 소염제, 산화방지제, 방부제에서 선택된 것을 적어도 1종 이상 첨가할 수 있음은 물론이다.
It is needless to say that the soap composition according to the present invention may further contain at least one selected from fragrance, pigment, fungicide, anti-inflammatory agent, antioxidant and preservative.

이와 같은 조성을 갖는 비누조성물을 이용하여 통상의 방법으로 압축성형하게 되면 용이하게 비누를 제조할 수 있으며, 특히 본 발명에 따라 제조된 비누의 경우 미백효과와 항균특성이 우수할 뿐만 아니라 보습효과도 우수한 특성을 얻을 수 있다.
When a soap composition having such a composition is used, it can be easily produced by compression molding by a conventional method. Particularly, the soap produced according to the present invention is excellent in whitening effect and antibacterial property, Characteristics can be obtained.

이하 본 발명의 내용을 실시예를 참조하여 보다 상세하게 설명하고자 하나 이들 실시예는 본 발명의 내용을 이해하기 위한 것일 뿐 이에 의해 본 발명의 권리범위가 한정되는 것으로 해석되어져서는 아니된다.
Hereinafter, the present invention will be described in more detail with reference to examples. However, these embodiments are for the purpose of understanding the present invention and should not be construed as limiting the scope of the present invention.

[실시예 1] 비누의 제조[Example 1] Production of soap

유지를 하기 표 1의 배합비로 배합하여 60∼70℃로 가열 용해한 후 수산화나트륨(NaOH)을 첨가하여 비누화 반응을 실시하고, 상층에 뜬 비누로부터 하층에 가라앉는 비누화 반응의 부산물인 물, 미반응 수산화나트륨, 글리세린 층 등을 분리 제거한 다음, 진한 소금물을 1~2회 가하여 비누 속에 있는 잔류 글리세린과 수산화나트륨 등을 제거하여 통상의 비누층을 얻고, 이를 진공 건조하여 수분 함량 13% 내외의 비누 베이스를 제조하였다.The oil was mixed at a compounding ratio shown in Table 1 and dissolved by heating at 60 to 70 DEG C. Then, sodium hydroxide (NaOH) was added to conduct a saponification reaction. Water, which is a byproduct of the saponification reaction, Sodium hydroxide and a glycerin layer are separated and removed and then concentrated salt water is added 1-2 times to remove residual glycerin and sodium hydroxide in the soap to obtain a conventional soap layer and vacuum dried to obtain a soap base having a moisture content of about 13% .

상기 비누베이스 99.2중량%를 혼합하여 교반하면서 균질화하고, 여기에 하기 표 2에서와 같이 송화소금을 0.1 중량%를 넣고 교반하여 균질화하였다. 그런 다음, 상기와 같이 균질화한 혼합물에 편백나무오일 0.2 중량%, 아쿠아향 0.5 중량%를 첨가하여 10분간 추가교반한 후 원형의 형틀에서 굳히고, 얻어진 비누를 랩핑하고 포장하였다(도 1).99.2% by weight of the soap base were mixed and homogenized with stirring. To this, 0.1% by weight of sesame salt was added as shown in Table 2, followed by stirring to homogenize. Then, 0.2 wt% of white wood oil and 0.5 wt% of an aqua flavor were added to the homogenized mixture as described above, and the mixture was further stirred for 10 minutes, and then solidified in a circular mold, and the obtained soap was wrapped and packaged (FIG.

비누베이스 조성Soap base composition 성분ingredient 배합비(중량%)Compounding ratio (% by weight) 1One 증류수Distilled water 1717 22 팜유, 야자유 지방산의 나트륨염Palm oil, sodium salt of palm oil fatty acid 2525 33 글리세린glycerin 1010 44 프로필렌글리콜Propylene glycol 99 55 소듐라우릴설페이트Sodium lauryl sulfate 66 66 Sodium Laureth(3mol) SulfateSodium Laureth (3 mol) Sulfate 66 77 염화나트륨Sodium chloride 0.030.03 88 E.D.T.A-4NaE.D.T.A-4Na 0.030.03 99 염화칼륨Potassium chloride 0.030.03 1010 스테아린산Stearic acid 2 2 1111 캐스터오일Castor oil 0.3 0.3 1212 솔비톨Sorbitol 14.6114.61 1313 수산화나트륨Sodium hydroxide 1010 합계Sum 100100

비누조성물의 성분Component of the soap composition 원료명Raw material name 함량(중량%)Content (% by weight) 비고Remarks 비누베이스Soap base 99.299.2 투명비누베이스Transparent soap base 송화소금Songhwa salt 0.10.1 편백나무오일Linseed oil 0.20.2 아쿠아향 Aqua incense 0.50.5 합계Sum 100.0100.0

[실시예 2] 비누의 제조[Example 2] Production of soap

비누베이스의 조성에 해바라기씨 오일 및 올리브 오일을 더 첨가하고, 편백나무 오일 및 아쿠아향 대신에 유칼립투스오일0.1 중량% 및 오렌지오일 0.2 중량%를 대체한 것을 제외하고는 실시예 1에서와 동일한 과정에 따라 비누조성물(불투명)을 제조하였다(도 2).
Except that sunflower seed oil and olive oil were further added to the composition of the soap base and 0.1 wt% of eucalyptus oil and 0.2 wt% of orange oil were substituted for the white wood oil and the aqua flavor Followed by preparing a soap composition (opaque) (Fig. 2).

[실시예 3] 비누의 제조[Example 3] Production of soap

송화소금을 하기 방법에 따라 제조한 흑마늘 송화염으로 대체한 것을 제외하고는 실시예 1에서와 동일한 과정에 따라 비누를 제조하였다.The soap was prepared according to the same procedure as in Example 1, except that the sesame salt was replaced with the black sesame seed flour prepared according to the following method.

흑마늘 송화소금의 제조:Preparation of black garlic safflower:

건조한 흑마늘을 파쇄하여 필터용 자루에 넣고 재료가 밖으로 빠져 나오지 못하도록 한 후, 상기 흑마늘이 담긴 필터용 자루를 통상적인 압력추출기에 넣고, 10배수의 물을 부은 후 밀봉한 다음 추출기 내의 물을 순환시키면서 90℃에서 120분 동안 가열하여 흑마늘 성분을 추출하였다.The dried black garlic was crushed and placed in a filter bag to prevent the material from coming out. The filter bag containing the black garlic was put into a conventional pressure extractor, and 10 times of water was poured thereinto and sealed. Then, water in the extractor was circulated And heated at 90 DEG C for 120 minutes to extract black garnet components.

추출을 완료한 후 사용된 추출기의 배출 콕크를 개방하여 압력추출기 내부 압력과 대기압 간의 압력차에 의해 추출기 내의 흑마늘 추출액을 필터용 자루의 고형물과 분리시켜 추출기 밖으로 완전히 배출하였다. 상기와 같이 분리된 흑마늘 추출액을 감압농축하여 가용성 고형분이 30~40 Brix 가 되도록 농축하고, 이와 같은 흑마늘 농축액을 송화염의 중량 대비 9 중량%로 송화염에 첨가하고 혼합기인 V 믹서(V-Mixer)에 넣어 혼합하였다.After completion of the extraction, the exhaust cock of the used extractor was opened, and the black garlic extract in the extractor was separated from the solids of the filter bag by the pressure difference between the pressure inside the pressure extractor and the atmospheric pressure. The black garlic extract thus separated was concentrated under reduced pressure to obtain a soluble solid fraction of 30 to 40 Brix. The black garlic concentrate was added to the flame salt in an amount of 9% by weight based on the weight of the flame, and the resulting mixture was stirred in a V mixer ).

상기와 같은 과정으로 얻은 흑마늘 농축액과 송화염의 혼합물을 열풍 건조기를 이용하여 70℃에서 4시간 동안 건조하여 20~40 mesh 크기의 흑마늘 송화염을 얻었다.The mixture of the black germ extract and the flame obtained by the above process was dried at 70 ° C for 4 hours using a hot air drier to obtain a black garlic flame having a size of 20 to 40 mesh.

[실험예 1] 성형성[Experimental Example 1] Moldability

실시예 1 내지 3과 대조군으로 비교예 1(송화소금 0.2중량% 첨가군)의 비누를 육안으로 관찰한 결과, 비교예 1의 비누의 경우 물러지고 깨지는 경우가 발생하여 상품적인 가치가 하락하는 것을 확인하여 송화소금은 0.2 중량% 미만으로 첨가하는 것이 좋은 것으로 판단되었다.
As a result of observing the soaps of Comparative Examples 1 and 2 (0.2 wt% of sesame salt added group) as a control and visually observing the soaps of Comparative Example 1, there was a case where the soaps were broken and broken, It was judged that it was better to add less than 0.2% by weight of sesame salt.

[실험예 2] 미백효과[Experimental Example 2] Whitening effect

20, 30 및 40대 여성 각 10인씩 모두 30인을 선정하여 실시예 1 내지 3과 대조군으로 비교예 2(송화소금 무첨가군)의 비누를 배부하고 한달간 사용하도록 한 후 미백효과 여부를 5점 척도법을 이용하여 평가하였다. (미백효과가 매우 우수하다:5점, 미백효과가 우수하다:3점, 미백효과가 나쁘다:1점, 미백효과가 매우 나쁘다 :0점)30, and 40 women were selected for each of the ten women, and the soaps of Comparative Example 2 (no added sesame oil) were distributed to the subjects of Examples 1 to 3 and the control group for a month, and then the whitening effect was evaluated by the 5-point scale method . (The whitening effect is excellent: 5 points, the whitening effect is excellent: 3 points, the whitening effect is bad: 1 point, the whitening effect is very bad: 0 point)

미백효과 Whitening effect 구분division 미백효과Whitening effect 실시예 1Example 1 4.74.7 실시예 2Example 2 4.74.7 실시예 3Example 3 4.94.9 비교예Comparative Example 3.53.5

[실험예 3] 보습력[Experimental Example 3]

위 미백효과에서 선정된 여성 30명의 시험 대상자의 피부를 본 발명에 따라 얻어진 비누로 세정한 후 2시간 경과 후 피부 표피의 수분을 수분측정기(Corneometer CM820)로 25℃ 상대습도 35℃에서 실시하였다.The skin of 30 testees selected by the stomach effect was washed with the soap obtained in accordance with the present invention, and 2 hours later, the skin surface moisture was measured with a moisture meter (Corneometer CM820) at 25 ° C and a relative humidity of 35 ° C.

보습력Moisture power 구분division 보습력Moisture power 사용전Before use 사용후after use 실시예 1Example 1 6464 8181 실시예 2Example 2 6565 8181 실시예 3Example 3 6565 8383 비교예Comparative Example 6565 7777

[실험예 4] 항균성 [Experimental Example 4]

항균성은 널리 공지된 칼프스킨 테스트 방법에 따라 실시하였으며, 다음 균주에 대하여 배양되는 정도를 0점(성장억제력이 없음)에서 4점(완전히 성장을 억제함)까지 5단계로 등급을 표시하여 시험하였다. 이때, 점수가 높을수록 항균성이 우수한 것으로 판정하였다. 배양과정에서 사용된 균주는 E. coli ATCC 10536와 S.arueus ATCC 9144가 이용되었다.The antimicrobial activity was carried out according to the well-known Karl's skin test method. The degree of cultivation of the following strains was tested in a scale of 5 points from 0 points (no growth inhibition ability) to 4 points (completely inhibiting growth) . The higher the score, the better the antimicrobial activity. E. coli ATCC 10536 and S. aureus ATCC 9144 were used in the cultivation process.

항균성Antimicrobial activity 구분division 항균성Antimicrobial activity E.coliE. coli S.arueusS.arueus 실시예 1Example 1 44 44 실시예 2Example 2 44 44 실시예 3Example 3 44 44 비교예Comparative Example 22 22

상기와 같이, 본 발명의 바람직한 실시 예를 참조하여 설명하였지만 해당 기술 분야의 숙련된 당업자라면 하기의 특허청구범위에 기재된 본 발명의 사상 및 영역으로부터 벗어나지 않는 범위 내에서 본 발명을 다양하게 수정 및 변경시킬 수 있음을 이해할 수 있을 것이다.
While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it will be understood by those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention as defined in the appended claims. It can be understood that

Claims (3)

송화소금을 활성성분으로 포함하는 비누조성물.A soap composition comprising sesame salt as an active ingredient. 제 1항에 있어서,
송화소금은 0.1 중량% 이상 0.2 중량% 미만으로 첨가되는 것을 특징으로 하는 비누조성물.
The method according to claim 1,
Wherein the salt is added in an amount of not less than 0.1% by weight and less than 0.2% by weight.
제 1항에 있어서,
송화소금은 흑마늘 농축액을 송화소금에 혼합하고 건조한 흑마늘 송화염인 것을 특징으로 하는 비누조성물.

The method according to claim 1,
Wherein the salt of sesame is a mixture of black garlic concentrate and sesame salt and dried black sesame seed flour.

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KR101627300B1 (en) 2016-02-01 2016-06-03 강근영 Soap composition comprising eggshells
JP6461410B1 (en) * 2018-07-12 2019-01-30 株式会社金水 Cosmetics containing black garlic extract
CN112029598A (en) * 2020-09-10 2020-12-04 山东钰财农业发展有限公司 Production process of black garlic perfumed soap and functional effects of black garlic extract and enzyme
KR102355540B1 (en) 2021-09-08 2022-02-09 오정미 Soap composition comprising medicinal herbs
KR102355539B1 (en) 2021-09-08 2022-02-09 오정미 Soap composition comprising carrot

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