KR20150045275A

KR20150045275A - Natural extracts of chrysanthemum extract

Info

Publication number: KR20150045275A
Application number: KR1020130124783A
Authority: KR
Inventors: 배형진
Original assignee: 배형진
Priority date: 2013-10-18
Filing date: 2013-10-18
Publication date: 2015-04-28

Abstract

More particularly, the present invention relates to a composition for a hair dyeing composition comprising a dye, a base and purified water, wherein the composition for hair dyeing composition is selected from the group consisting of extracts of Pseudomonas sp. And 30 to 50% by weight of a natural hair dye composition.
The composition for hair dyestuffs may be selected from the group consisting of extracts of walnut tree chinchilla, extracts of walnut tree chestnut, extracts of lupine bark, extracts of green tea, extracts of Leaf leaf, pine leaf extract, Seomoktae extract, Henna) or camellia oil to produce a hair dye. When dyed with this hair dye agent, it does not stimulate the scalp or mucous membrane, not only promotes hair growth, but also quickly restores damaged hair, and gives elasticity and nutrition for a long period of time.

Description

Natural extract of chrysanthemum rhizome extract (natural extract)

More particularly, the present invention relates to a composition for natural hair dye extract of Phellinus linteus, and more particularly, it relates to a composition for natural hair dye, which is free from scalp or mucous membrane irritation during hair dyeing, promotes hair growth, quickly restores damaged hair, And to provide a natural hair dye composition for extracting chrysanthemum chrysanthemum (Qingdao) extract which is capable of nourishing and maintaining the gloss for a long period of time.

The hair dye is usually prepared by dissolving a first component which can swell the hair to easily diffuse and penetrate the hair into the hair, and a second component which helps the generation of oxygen necessary for oxidizing the dye, And a mixture thereof is used at a certain ratio.

Hair dyeing using these hair dyeing agents is based on the use of melanin pigments present in hair between keratin fibers in the hair, which changes the nature and structure of the hair by using a chemical dye and hydrogen peroxide, so hair damage can not be avoided.

The use of a hair dye makes it easy to cause skin allergy, not only damages the hair but also causes the hair to be damaged due to oxidation due to oxidation in the inside of the hair, resulting in loss of gloss and gloss, There is a drawback that the feel is deteriorated. Dyestuffs that produce color can give irritation to the mucous membranes and eyes, which can cause irritation and rashes in dermatitis.

In recent years, the number of consumers who dye hair has greatly increased, and the incidence of dermatitis and facial edema is rising as the age at which hair starts is lowered.

The use of hair dye causes slight allergies such as itching and inconvenience in the scalp area, and sudden symptom appears in some severe cases, and cases showing such allergic symptoms are increasing.

To solve these problems, various types of hair dye have been developed and studied.

Korean Patent Publication No. 2000-61526 discloses that a stain containing loess is used for hair dyeing by processing harmless and non-toxic clay soil to utilize the properties of the loess rich in minerals.

Korean Patent Publication No. 2002-46100 discloses a permanent hair dye that does not cause a skin allergic reaction. It is also possible to use a dye selected from a direct dye (tar pigment), a nitro dye and a natural dye in a hair dye, It has been suggested that a hair-dyeing agent which is easy to penetrate dye into hair and has excellent durability.

Korean Patent No. 10-0453679 discloses a composition for a hair dye containing henna, indigo, centaurane, rhubarb powder, lichen or lettuce.

It says that the use of natural dyes and natural materials instead of chemical dyes can help protect hair from violent action of alkalis and oxidants, helping color, condition and hair.

In addition, Korean Patent Laid-Open Publication No. 2005-26759 discloses a natural vegetable hair dye, and it is possible to dye the hair by mixing the henna leaf powder with the indigenous side leaf powder as a natural plant and varying the dyeing color according to the mixing ratio .

In recent years, not only hair dyes using natural dyes but also artificial hair dyes containing organic or herbal ingredients have been studied.

Korean Patent Laid-Open No. 2005-115530 contains 0.01 to 5.00% by weight of red ginseng extract, 0.01 to 5.00% by weight of the extract of the present invention, 0.01 to 5.00% by weight of the extract of Chenopodium ambrosioides, 0.001 to 5.00% by weight of dye and 17.00 to 30.00% , Dye fastness, hair conditioning, and hair protecting effect.

However, these patents are not mentioned at all on the extracts of the chinese cabbage fruit.

In order to solve the above problems, the inventors of the present invention have developed a composition for hair dyeing using chrysanthemum morifolium extract as a natural material which is not harmful to the human body. In addition to extracts of chrysanthemum chinensis, To prevent scalp trouble during dyeing, not only to accelerate hair generation but also to restore damaged hair quickly, and to maintain elasticity and nutrition for a long period of time.

It is an object of the present invention to provide a natural hair dye composition for extracting the extract of Pseudomonas sp.

It is another object of the present invention to provide a natural hair dye composition comprising the extract of Pseudomonas sp.

In order to achieve the above object,

In a composition for a hair dye containing a dye, a base and purified water,

Wherein the composition for hair dyeing comprises 30 to 50% by weight of a spruce outer skin extract.

At this time, the composition for hair dyeing agent contains 5.0% by weight in the dye 0.001, 10 to 50% by weight of the base, and the balance of purified water.

In addition, the composition for hair dyeing composition includes Seomotai (snow bean bean) and camellia seed herbal medicine extract, and more specifically, a walnut fruit chinchilla extract, a lupine bark extract, a green tea extract, a Leaf leaf extract, a pine needle extract, Henna) and a mixture thereof in an amount of 10 to 20% by weight in the total composition.

At this time, the extract of Phellinus lintia extract and herbal medicine extract

a) extracting the first extraction solution with water, a lower alcohol, or a mixed solvent thereof at a weight ratio of 5 to 30 times the weight of each component;

b) The primary extraction solution is filtered and concentrated,

c) Extracting the obtained concentrated solution with water, alkylene glycol, or a mixed solvent thereof in a weight ratio of 5 to 30 times,

d) The secondary extraction solution is obtained by filtration and concentration.

Also,

The purified water, the base and the dye are mixed at 80 to 85 캜,

The present invention also provides a composition for a hair dyeing composition, which is prepared by adding an extract of Phellinus linteus to a skin.

The present invention also provides a hair dye composition comprising a first agent comprising the composition for a hair dye and a second agent comprising an oxidizing agent.

Hereinafter, the present invention will be described in more detail.

The composition for hair dyeing composition according to the present invention contains extract of chrysanthemum berry extract to prevent scalp trouble during dyeing. It not only accelerates hair generation but also restores damaged hair quickly, Continue for a long time.

The spruce tree used in the present invention is a dicotyledonous plant, a deciduous broad-leaved arboreous tree of the spore tree, and the scientific name is Juglans mandshurica Maxim. there is. mandshurica for. It is called mandshurica, and it is called 楸子, also known as 楸子木, which inhabits in Korea (central, northern, Siberia, etc.). It is called "楸子" The fruit is an egg-shaped circle, egg-shaped, 4 ~ 8cm long, ripened in September, and the fruit is in the shape of a wing And the fruit endothelium is dark brown, very hard, pointed at both ends, and the phloem, leaves, fruit, and endothelium have an alkaloid reaction, which is 5-hydroxytryptamine, Tannic acid and essential oil, and the content of alcaloids in the endothelium is 0.03%. Fresh leaves contain 1720 mg of arconvic acid, root roots of yulleron and its derivatives, and 5.1% of tannin There are 14% tannic acid seeds in every coat and 50% in oil. Distillation of leaves gives 0.06% essential oil, leaves are quercetin, isoquercetin, and flesh endothelium It has a strong anti-inflammatory action and has an anthelmintic and anthelmintic effect against staphylococcus aureus, E. coli, E. coli, , Due to the yulonite component in the root shell.

In the treatment of acupuncture, the inner skin of the fruit skin is used when it is used for acupuncture, hair wound, pore drainage, acute bacterial suffrage, and in the case of the private, diarrhea and inflammation in the mouth. And the seeds of insect repellent, leprosy, cough medicine, and seed oil are used for skin diseases. The inner skin of the fruit skin is also hyrogenol, which is used for skin diseases such as marine diseases and scar tissue. It is used for rheumatism, psoriasis, and eczema.

There are sugar, dextrin, starch, cellulose, and pectin as carbohydrates. Chlorophyceae, carotenoids, carotenoids, carotenoids, carotenoids, Flavonoid derivatives, anthocyanins, essential oils, waxes, resins (resins), organic acids, enzymes, vitamins, and inorganic components.

In the case of using the above-mentioned extract of the spruce fruit, the tannic acid which tightens the pores and the plano-void ingredient which has strong cleansing power act to generate less dandruff, and the sterilizing action of the catechin ingredient and the toxicity of the shampoo and rinse Keeps your scalp healthy by removing it. It is also effective in regenerating skin. It is rich in vitamins and minerals, and it also helps to prevent dandruff on the scalp.

In addition, testosterone is converted to dihydrotestosterone (DHT) by a 5-alpha reduction factor, and this DHT affects the hair follicle, resulting in hair loss. At this time, the extract of chrysanthemum fruits prevents the formation of DHT, .

In this invention, the natural hair dye composition of extract of chrysanthemum chrysanthemum which has such an effect is used in a composition for natural hair dye of extract of chrysanthemum chinensis (Qingdao) extract.

The composition for a hair dyeing composition according to the present invention usually comprises a dye, a base and purified water, wherein 30 to 50% by weight, preferably 35 to 40% by weight, of a natural hair dye composition, .

The natural hair dye composition of the extract of Phellodendron chinensis can be used in any known extraction method and is not particularly limited in the present invention.

For example, the extract of Pseudomonas sp.

b) The primary eluting solution is filtered and concentrated,

Specifically, in step (a), a natural hair dye composition is extracted from the surface of the extract of the extract of the extract of the extract of the extract of the extract of the extract of the extract of the extract of the extract of the extract of the extract of the seeds , Is added to the extraction solvent, and the first extraction solution is obtained by first extracting the hot water extraction method or the ultrasonic extraction method.

At this time, water, a lower alcohol or a mixed solvent thereof and a dried nodule fruit (dried noodle) of 5 to 30 times, preferably 10 to 15 times (weight ratio), based on the weight of the dried natural noodle composition, The blueberry skin extract composition is mixed.

The lower alcohol may be one selected from the group consisting of ethanol, propanol, butanol, and mixtures thereof. Preferably, water / ethanol is mixed in a weight ratio of 1:10 to 10: 1.

The resulting mixture is then subjected to hydrothermal extraction at an extraction temperature of 40 to 120 DEG C, preferably 60 to 90 DEG C, for 1 to 48 hours, preferably 10 to 20 hours. Or the mixture is subjected to microwave irradiation at 500 to 1500 W for about 5 to 20 minutes.

In step b), the primary extraction solution obtained by the first extraction is filtered or centrifuged to separate the supernatant, preferably filtered, then concentrated or dried to a volume of 1/10 to 1/3, A primary extract in liquid or dry state is obtained.

In step c), the primary extract obtained from the extraction step is filtered, and then water or an alkylene glycol or a mixed solvent thereof is further added thereto, and repeatedly produced under the same conditions as above to obtain a secondary extraction solution.

The alkylene glycol may be selected from the group consisting of ethylene glycol, propylene glycol, butylene glycol, and mixtures thereof. Preferably, the alkylene glycol is mixed with water / butylene glycol in a weight ratio of 1:10 to 10: 1 do.

In step d), the second extraction solution obtained by the second extraction is filtered or centrifuged to separate the supernatant, to obtain a natural hair dye composition of the extract of Aspergillus oryzae as a secondary extract.

The mixture of 30% to 50% by weight, preferably 35% to 40% by weight of the composition of the natural hair dye composition obtained by the step of extracting the extract of the spiny mackerel is used to prevent scalp trouble during dyeing, Not only does it accelerate, it quickly restores damaged hair, but also gives elasticity and nutrition for a long period of time. It is difficult to obtain the above-mentioned effects when the content of the natural hair dye composition of the extract of Phellodendron sunflower extract is less than or more than the above range.

Wherein the composition for the hair dyeing agent comprises 0.001 to 5.0% by weight of the dye, 10 to 50% by weight of the base, and the balance of purified water, and the dyes and the bases are of known compositions.

The dye to be used in the present invention may be a conventionally used oxidation dye and is not particularly limited in its kind. Examples of the dye include p-phenylenediamine, o-phenylenediamine, resorcin, 2-methyl Aminophenol, p-aminophenol, toluenediamines, aminonitrophenols, diphenylamines, N-phenyldiamines, diaminopyridines and the like, and at least one selected from the group consisting of m-phenylenediamine, m- And one or more of these salts are used in combination. The content of the dye is generally within the range of, for example, 0.001 to 5.0% by weight based on the total amount of the hair dye composition. Oleic acid. One selected from oleic alcohol, dimethicone, sodium ascorbate, sodium myristoyl glutamate, behenyl alcohol, sodium cocoyl isethionate, cocamidopolofibutamine, polyquaternium-10 and glyceryl stearate, or It may be a mixture of two or more. At this time, the content of the base is used in an amount of 10 to 50% by weight, preferably 10 to 30% by weight, in the composition for the total hair dyeing agent.

In addition, the present invention uses various herbal medicine extracts in addition to a natural hair dye composition for extracting chrysanthemum morifolium extract from a composition for hair dye.

Examples of the herbal medicine extracts include a group consisting of a mixture of a walnut extract, a bark extract, a green tea extract, a bark extract, a pine needle extract, a henna bean, Henna and camellia oil One selected paper is available and is used in an amount of 10 to 20% by weight, preferably 10 to 15% by weight, in the total composition.

These herbal extracts are described in more detail as follows.

Walnut trees (Juglan regia L. Var. Sinensis C.D. Candolle) have been planting walnut trees for the purpose of barking around the temple for years, and they have been used as a medium for praying for the good health of a year by eating walnuts in the New Year's Eve. Walnut husk outer skin and walnut alum, leaves are useful medicinal materials for human body, various amino acids, batamin is used as a good source of medicine. There are α hydroxydrones and β hydroxydrons in the walnut fruit juice and walnut fruit juice. The α-hydrourogloss is oxidized in the air to become uylon. β-Hydroxyglucone is not oxidized, but when it is subjected to the action of Alcoholic Hydrochloric Acid, it becomes α Hydroxyuron. The walnut leaves also contain naphthoquinone-uroglutarin, αβ hydrouroglutane, flavonoid, heparocide, quercetin, 3 arabanoside, chemerol 3 arabinoside, vitamins Brns, ascorbic acid 4-5% It contains 3 to 4% of tannin, ellagic acid, gallic acid, 0.1% of caffeic acid, 30 mg or more of β-carotene, violaxshantin, flavocaxanthin, crinkaxanthin and 0.03% of essential oil.

The wool nut and the yulon component contained in the leaves have a bactericidal action, increase the permeability of the capillaries, and prevent arteriosclerosis. It is also excellent in insecticidal action and antiparasitic activity. In the private sector, walnut oil is used for various skin diseases, and walnut green tea is used to make the hair come out and to color black. Walnut fruit Cheongpije (皮皮) The moon dignity is effective in prevention of green fox, eczema and hair loss.

The root of the elm tree is called the root bark of elm, and the shell of the elm stem is distinguished as milky white bloom. The scientific name is Ulmus davidiana. It is commonly found in mountain valleys and waterfronts in the central and northern parts of the Republic of Korea, and has been used as a medicine in the early spring and autumn, with its roots removed. In Donguibogam, elm trees are well-balanced, tasteful, and have no poison, so it is easy to make soft feces. It is effective for various swelling and nausea, but it is also noted that it is not toxic.

Green tea (Thea sinensis) contains caffeine, purine base, caffeine, purine base, tannic acid, protein, amino acid and amide. Carbohydrates include sugar, dextrin, starch, cellulose and pectin. , Carotenoids, flavonoid derivatives, anthocyanins, essential oils, waxes, resins (resins), organic acids, enzymes, vitamins, and inorganic components.

When used in the green tea extract hair dye, it has tannic acid that tightens the pores and a strong cleansing planovoid component that acts to reduce the dandruff and protects the scalp health by eliminating the sterilizing action of the catechin ingredient and the toxicity of the shampoo and rinse . Or green tea extract Excellent in skin soothing and regenerating effect, vitamin D component of green tea extracts make hair shiny and soft and inhibits dandruff on scalp.

By containing these ingredients, it has an effect of delaying or preventing skin aging with excellent constant effect, and enhancing skin blood circulation. It can maintain healthy skin, promotes blood circulation of the scalp, and helps hair loss prevention and hair growth.

The dwarf tree is the old tree and the evergreen tree. The leaves are blue. Leaves of Cervus spp. Promote hair.

Pine needles serve as terpene α-pinene, β-pinene sources, and linoleic acid, palmitic acid and 5-oleic acid inhibit the formation of lipid peroxides produced by active oxygen to prevent aging. In addition, it contains a large amount of essential amino acids that can not be produced by the human body, thereby allowing hair to be regenerated with elasticity.

Seomok-tae is a perennial herbaceous plant of soybean and has brown stem and leaves. Seomok-tae has been used as a sight-enhancing, detoxifying and soothing treatment since ancient times and is called "Yak-ko" and it has become a traditional food culture of Korea. Seomok-tae (bean curd) is not only high-quality protein, but also nutrients such as vitamin B1, vitamin B2 and vitamin E, which serves as lipid, plant estrogen and saponin supply. It also contains cysteine, an essential ingredient for hair growth, and is effective in preventing hair loss. Isoflavone contained in Seomok-tae (winter bean) is an indispensable substance for hair growth. It regulates the metabolism of sugar, which is the energy source of hair, inhibits aging and activates. Anthocyanin pigment contained in the shell of Seomuntae (bean bean) It has antioxidant effect that eliminates free radicals, and has the effect of soothing the scalp when staining.

Henna is a plant known as Lawsonia inermis that grows up to 1.5 to 3 meters after sowing seeds with a unique herbal smell similar to mugwort. After seeding, leave about 10cm from the surface of the tree, pick branches and leaves, and use most of the leaves for dyeing. The leaf of this plant was dried and then ground to make henna powder with natural dyeing properties called tannic acid. This henna is divided into products for skin dyes and hair, and the natural henna is brown in color and usually lasts for one to four weeks.

Henna is a natural plant material harmless to the human body and having a dyeing effect.

The above-mentioned barn wax extract is used in a composition for a hair dyeing composition in the form of henna extract, henna extract, henna leaf, pine needles, green tea leaves, pine needles, and henna seeds. The extract is obtained in the same manner as the natural hair dye composition.

The composition for a hair dyeing composition according to the present invention having such a composition can be optionally added with ingredients that can be blended with common external preparations for hair. For example, hair protecting agents, chelating agents, surfactants, pH adjusters, alkalis, moisturizers, thickeners, preservatives, antioxidants, bactericides, anti-inflammatory agents, antimicrobial agents, solvents, flavoring agents and pigments can be used. These additives are suitably used within the normal range by those skilled in the art.

The hair protecting agent helps to fix the dye on the hair surface and forms a water repellent thin film on the hair to slow down the discoloration of the dye due to washing with water and sunlight to give an excellent conditioning effect to the surface of the hair, It also helps to stabilize. Usable hair-protecting agents include, but are not limited to, sodium methylstearoyltaurate hydrolyzed keratin, tocopheryl acetate, settimuronium chloride, glyceryl stearate, phage-11 methyl ether dimethicone, cyclomethicone, ammonium glycyrrhizate, Glyceryl linoleate, linoleic acid, ceramide, mineral oil, polyquaternium-10, camellia oil, and the like.

Chelating agents include disodium EDTA, tetrasodium EDTA, and the like, and act as metal sequestrants.

Specific examples of the pH adjusting agent include organic acids such as citric acid, succinic acid, tartaric acid, lactic acid, malic acid, fumaric acid, maleic acid and glycolic acid, and inorganic acids such as hydrochloric acid, sulfuric acid, phosphoric acid, nitric acid, Potassium salt, ammonium salt, or the like may be used in combination. Sodium hydroxide and potassium hydroxide may also be used.

Alkaline agents use monoethanolamine or strong aqueous ammonia to swell the hair to facilitate penetration of dye molecules into the hair.

Specifically, the dissolution aid may be isopropyl myristate, polyethylene glycol, triglycerides of medium chain fatty acids, hydrocarbons, glycols and the like.

Specific examples of the anionic surfactant in the surfactant include ammonium lauryl sulfosuccinate, ammonium lauryl sulfate, sodium cocoyl isocyanate, sodium lauryl isethionate, triethanol amine lauryl sulfate, sodium lauryl ether sulfate Ethylene oxide 1-3), and the like.

The moisturizing agent may specifically be glycerin, propylene glycol, 1,3-butylene glycol, dipropylene glycol, sorbitol, and the like.

Examples of the thickener include methylcellulose, hydroxymethylcellulose, hydroxyethylcellulose, carrageenan, carboxymethylcellulose, carboxymethylhydroxyguanine, cetearyl alcohol, stearic acid, polyquaternium-7, polyquaternium-10 , And the amount to be used may be variously used.

Preservatives may specifically be benzoic acid, paraoxybenzoic acid esters, mixtures of methylglurooisothiazolinone, phenoxyethanol, dimethyl demethanone, and the like.

The antioxidant may specifically be ammonium thioglycolate, dibutylhydroxytoluene, ascorbic acid, and the like.

The bactericide may specifically be chlorhexidine gluconate, quaternary ammonium salt, pyrrothonol amine, zinc pyrithione suspension, urethropropyl butylcarbamate, salicylic acid and the like.

The anti-inflammatory agent may specifically be monoammonium glycyrrhizinate, dipotassium glycyrrhizinate, stearyl glycyrrhizinate, chamomile, alpha bisabolol, allantoin, and mixtures thereof.

Antimicrobial agents specifically include antioxidants such as phenoxyethanol, chlorhexidine, chlorhexidine gluconate, pylontonol amine, ketoconazole, arnica extract, urethropropyl butylcarbamate, benzalkonium chloride, benzenethonium chloride, benzoic acid and its salts, benzyl alcohol, lavender, Salicylic acid, trichlorocarban, zinc pyrithione suspensions, and mixtures thereof.

The solvent may specifically be ethanol, purified water, tween 20, cyclomethicone, mineral oil, dimethicone, and the like.

Flavoring agents and dyes may be used with the ingredients used in common scalp and hair formulations.

The composition for hair dyes according to the present invention is not specifically limited in the present invention, and is well known in the art.

For example, the purified water, the base and the dye are mixed at 80 to 85 캜,

Herein, a composition for hair dyeing agent is prepared by adding a natural hair dye composition extracted from the spruce tree fruit.

At this time, in addition to the natural hair dye composition of the chrysanthemum extract, the natural hair dye composition, the extract of the walnut tree chestnut, the extract of the lycopene bark, the extract of the green tea, the extract of the bamboo tree leaf, the extract of the pine needles, Henna) and mixtures thereof.

The present invention also provides a hair dye preparation comprising a first agent comprising the composition for a hair dyeing agent and a second agent comprising an oxidizing agent.

When the composition for hair dyeing of the present invention is a hair dye for oxidation, the hair dye for oxidation may be a second preparation comprising a first agent containing an oxidation dye and a second agent containing an oxidizing agent. Such a composition for a two-component hair dye composition is used by mixing a first agent and a second agent immediately before use.

As the second oxidizer, hydrogen peroxide, peroxide, and the like are generally used. In addition, a known compounding agent such as a stabilizer such as EDTA, phenacetin, and sodium stannate, an oil component such as liquid paraffin, vegetable oil, a pH adjuster, and a flavoring agent may be added to the second agent as needed.

The formulation of such a hair dye composition is preferably a cream type, a liquid type, a powder type, a jelly type, and an aerosol type.

The amount of the hair dye composition to be used may be appropriately adjusted according to the condition of the hair, the age of the user, the length of the hair, etc., and the application time may be appropriately adjusted depending on the individual.

The hair dye composition (first agent) according to the present invention and the oxidizing agent (second agent) mixed with hydrogen peroxide are mixed at a ratio of 1: 1 and applied to the hair, Leave about 50 to 200 ml of water for about 5 minutes to 60 minutes, rinse thoroughly with water, and shake again with shampoo or rinse.

As described above, according to the present invention, a composition for hair dyeing agent containing a natural hair dye composition of extract of Phellodendus japonica and an extract of herbal medicine was prepared. The above-mentioned natural hair dye of chrysanthemum extract prevents the scalp trouble during dyeing, not only promotes hair growth but also quickly restores damaged hair, and provides elasticity and nutrition for a long period of time.

The following examples illustrate the invention. However, the present invention should not be construed as being limited to the following examples.

Hereinafter, preferred embodiments of the present invention will be described in order to facilitate understanding of the present invention. However, the following examples are provided only for the purpose of easier understanding of the present invention, and the present invention is not limited by the examples.

Production Example 1: Preparation of a natural hair dye composition of extract of chrysanthemum chinense

100 g of chrysanthemum extract was added to 1 kg of a purified water / ethanol mixed solvent (1: 1, weight ratio), and extracted with an extractor equipped with a cooling condenser at 60 ° C. for 24 hours to obtain an extract solution 900 g). The extraction solution was concentrated under reduced pressure to a volume of 300 g.

700 g of a mixed solvent of purified water and butyleneglycol (7: 3, weight ratio) was added to the obtained extract, and the mixture was allowed to stand for 3 days, and then the supernatant was filtered to obtain 900 g of an extract of spruce.

Production Example 2: Production of natural hair dye of extract of Qingdao chinensis

100 g of the extract of Phellinus linteus was washed with water and then added to 1 kg of a purified water / ethanol mixed solvent (1: 1, weight ratio) in an ultrasonic wave extraction apparatus and irradiated at 1000 W for 10 minutes to obtain 900 g of an extraction solution . The extraction solution was concentrated under reduced pressure to a volume of 300 g.

700 g of a mixed solvent of purified water and butyleneglycol (7: 3, weight ratio) was added to the obtained extract solution, and the mixture was allowed to stand for 3 days, and then the supernatant was filtered to obtain 900 g of a natural hair dye composition.

Production Example 3: Preparation of crude drug extract

Walnut bark extract, green peach bark extract, green tea extract, bamboo leaf extract, pine leaf extract, Seomyeongtaek (black soybean) extract and henna extract were obtained in place of the extract of chrysanthemum chinense.

Examples 1 to 6

A: Preparation of first agent (composition for hair dyeing agent)

Compositions for hair dyeing compositions were prepared by using the natural hair dye composition and extracts of herbal extracts of the extracts of the extract of Aspergillus oryzae prepared in Preparation Example 1 and Preparation Example 3 in the compositions shown in Tables 1 and 2 below.

First, the purified water 18, the sequestering agent 7, the preservative 8, the antioxidant 9 and the base agents 10 to 14 were heated to 85 캜 and mixed with stirring in a mixer.

The main components of (1) to (6) were added thereto and stirred at 85 캜 and then the thickening agent 15 and the alkaline agent 16 were added thereto and uniformly mixed to obtain an extract of chrysanthemum chinensis 17 ). In Example 3-6, a herbal medicine extract (18-22) was added together with an extract of Quercus mongolica (17) to prepare a hair dyeing composition.

Table 1

Table 2

B: Preparation of the second agent (oxidizing agent)

An oxidant having the composition shown in Table 3 below was prepared in the following manner.

After the purification, the compositions of (2) and (4) to (11) were added to the reactor, and the mixture was heated to 80 ° C and mixed with stirring.

The resulting mixture was adjusted to 55 캜 and mixed with phosphoric acid (3), mixed with hydrogen peroxide solution (1) at 40 캜, and finally mixed with glycine (12) at 35 캜 to prepare an oxidizing agent.

Table 3

Comparative Example 1

Extract of Phalaenopsis sp. Cetal Extract A composition for hair dyeing agent was prepared in the same manner as in Example 1, except that the natural hair dye composition was not used.

Experimental Example 1: Skin irritation test of composition (first agent) for hair dyeing agent

The compositions for hair dyes prepared in Examples 1 and 4 were submitted to the Korean Chemical Testing and Research Institute, which is a nationally recognized testing institute, and skin irritation tests were conducted using the test methods of the Korean Food and Drug Administration Notice 2005-60. Table 4 shows the results.

Table 4

Skin irritation test result

Referring to Table 4, it was confirmed that the composition for hair dyeing agent obtained according to the present invention is a non-irritant substance on the skin.

Experimental Example 2: Testing of the mucosal irritant property of the composition for hair dyeing agent (the first agent)

The composition for hair dye preparation prepared in Examples 1 and 4 was subjected to a skin irritation test using the test method of Korean Food and Drug Administration Notification No. 2005-60 by the Korean Chemical Testing and Research Institute, Table 5 shows the results.

Table 5

Referring to Table 5, it was confirmed that the composition for hair dyeing agent obtained according to the present invention was free from salt mucous membrane stimulation.

Experimental Example 3: Heavy metal elusion test of the composition for hair dyeing agent (the first agent)

The raw material compositions for hair dyeing prepared in Examples 1 and 4 were subjected to a heavy metal elution test using the test method of ICP analysis by the Korean Chemical Testing and Research Institute which is a nationally recognized testing institute and as a result, It was not.

Table 6

Heavy metal dissolution test result

Experimental Example 4: Dyeing characteristic test

The hair dyeing properties of the compositions prepared in the above Examples and Comparative Examples were examined.

The first and second compositions of the compositions of Examples 1 to 6 and Comparative Example 1 were mixed in equal proportions and uniformly applied to dark brown and white hair having a length of 8 cm and a weight of 0.7 g. After 20 minutes had elapsed, the mixture was shampooed Next, it was washed 5 times with lukewarm water, the water was wiped off and dried with a hair dryer. Table 7 shows the results obtained by measuring the dyeability and dyeing fastness to hair after drying.

The color difference (ΔE) between the dyed and untreated hairs was measured using a spectrophotometer (Minolta CM-3700d, JAPAN). The larger the color difference, the better the dyeability of the hair dye.

The dye fastness was measured by immersing the above-mentioned dyed hair in an acidic solution similar to a sweat component, after lapse of a certain time.

Table 7

Experimental Example 5: Skin irritation property

The frequency of allergy and the hair damage prevention effect of the compositions for saline prepared in Examples 1 and 4 and Comparative Example 1 were evaluated.

Fifty men aged 25 to 40 years old and 50 women aged 25 to 40 years old were selected and 20 persons (10 sexes) were selected for each of them. Then, the hair was dyed with the compositions of the above Examples and Comparative Examples, Damage occurrence was investigated, and the obtained results are shown in Table 8 below.

Table 8

Referring to Table 8, it can be seen that almost all of the allergy or hair damage does not occur even when dyeing is performed with a composition for a hair dye containing various extracts of Chrysanthemum morifolium extract and herbal medicine according to the present invention. Compared with this, hair damage was found to occur when the composition of Comparative Example 1, which did not contain any natural hair dye composition or herbal medicine extract, was used.

Claims

A natural hair dye composition for extracting chrysanthemum chinense (Qingdao)
Wherein the composition for hair dyeing comprises 30 to 50% by weight of a natural hair dye composition of extracts of Pseudomonas sp. Citrus extract, wherein the hair dye composition comprises 0.001 to 5% by weight of a dye, 10 to 50% by weight of a base, &Lt; / RTI &
The natural hair dye composition of the extract of Pseudomonas sp.
a) extracting the first extraction solution by using 5 to 30 times of water, a lower alcohol, or a mixture thereof in a weight ratio of each component as a solvent,
b) The primary extraction solution is filtered and concentrated,
c) Extracting the obtained concentrated solution with water, alkylene glycol, or a mixture thereof in a weight ratio of 5 to 30 times by weight as a mixed solvent,
d) a natural hair dye composition obtained by extracting the secondary extraction solution and then concentrating it.

The method according to claim 1,
In addition, the composition for hair dyeing composition may be selected from the group consisting of a walnut fruit cunechial extract, a carrot bark extract, a green tea extract, a cinnabar extract, a pine needle extract, a Henna extract, Wherein the composition comprises 10 to 20% by weight of a herbal medicine extract selected from the group consisting of a herbal extract and a herb extract.

The method according to claim 1,
Wherein the primary extraction solution is extracted by hot water extraction at 40 to 120 ° C for 1 to 48 hours or by applying microwave at 500 to 15,000 W for 5 minutes to 20 minutes. Extract natural hair dye composition.

The method according to claim 1,
The dye may be selected from the group consisting of p-phenylenediamine, o-phenylenediamine, resorcin, 2-methylresorcinol, m-phenylenediamine, o-aminophenol, p-aminophenol, toluenediamines, , N-phenyldiamines, diaminopyridines, and salts of any one of them, or a mixture of two or more thereof.

The method according to claim 1,
The composition for hair dyeing composition may further comprise at least one selected from the group consisting of hair protecting agents, chelating agents, surface active agents, pH adjusting agents, alkaline agents, Wherein the natural hair dye composition comprises at least one selected from the group consisting of:

The method of claim 1, wherein
The composition for a hair dyeing composition may further comprise at least one component selected from the group consisting of a hair protecting agent, a chelating agent, a surfactant, a pH adjusting agent, an alkaline agent, a moisturizer, a thickening agent, an antiseptic, a coral inhibitor, a bactericide, an anti- inflammatory agent, an antimicrobial agent, Wherein the natural hair dye composition contains at least one selected ingredient.

The method of claim 1, wherein
Wherein the composition for hair dyeing agent is a cream type, a liquid type, a powder type, a jelly type, or an aerosol type.