KR20140124221A - Preparation method of gel for deodorant by using natural mineral - Google Patents

Preparation method of gel for deodorant by using natural mineral Download PDF

Info

Publication number
KR20140124221A
KR20140124221A KR1020130041696A KR20130041696A KR20140124221A KR 20140124221 A KR20140124221 A KR 20140124221A KR 1020130041696 A KR1020130041696 A KR 1020130041696A KR 20130041696 A KR20130041696 A KR 20130041696A KR 20140124221 A KR20140124221 A KR 20140124221A
Authority
KR
South Korea
Prior art keywords
weight
natural mineral
parts
deodorant
agent
Prior art date
Application number
KR1020130041696A
Other languages
Korean (ko)
Inventor
이상진
김인미
최인숙
이정순
Original Assignee
(주)세영씨앤티
이상진
이정순
김인미
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by (주)세영씨앤티, 이상진, 이정순, 김인미 filed Critical (주)세영씨앤티
Priority to KR1020130041696A priority Critical patent/KR20140124221A/en
Publication of KR20140124221A publication Critical patent/KR20140124221A/en

Links

Images

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/01—Deodorant compositions
    • A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/01—Deodorant compositions
    • A61L9/014—Deodorant compositions containing sorbent material, e.g. activated carbon
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20—Method-related aspects
    • A61L2209/21—Use of chemical compounds for treating air or the like

Landscapes

  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

Provided is a manufacturing method of deodorant gel with natural mineral, which comprises: a step of mixing purified water with a buffering agent, a gelation agent, inorganic salts, an antifoaming agent, a deodorizing ingredient, and natural mineral, controlling the pH of a mixture of the purified water, the buffering agent, the gelation agent, the inorganic salts, the antifoaming agent, the deodorizing ingredient, and the natural mineral to be in a range of 4 - 9, and then preparing a natural mineral-mixed solution by heating the mixture at a temperature range of 50 - 90°C; a step of preparing a dispersant-mixed solution by mixing a solubilizing agent, a dispersion stabilizer, an air freshener, and a food coloring; a step of preparing a deodorant gel solution by stirring the dispersant-mixed solution into the natural mineral-mixed solution at a temperature range of 65 - 85°C for 10 - 60 minutes; and a step of manufacturing the deodorant gel cooling the deodorant gel solution after injecting the deodorant gel solution into a mold.

Description

[0001] The present invention relates to a method for preparing a deodorant gel containing a natural mineral,

The present invention relates to a method for producing a deodorant gel having improved antibacterial activity by adding a functional natural mineral to an existing deodorant.

Conventional deodorizers for deodorization mostly utilize the deodorizing function of nitrogen compounds, sulfur compounds and aldehyde components, and in the case of deodorizers for toilets, a detergent using a cleaning effect using a surfactant is used. However, such a deodorant has a limitation in removing various complicated contaminants in recent years, and can be another environmental pollutant source by using a large amount of a synthetic surfactant.

Korean Patent Laid-Open Publication No. 10-1989-0008477 discloses a malodor removing agent

Conventional deodorizing agents are produced by adding yeast to rice bran or molasses, adding zeolite to the mixture, stirring the resulting mixture, fermenting the mixture, adding a small amount of iron sulfate thereto and drying at a temperature of about 15 to 20 ° C and a humidity of about 80 to 90 ° C.

However, the conventional deodorant has a problem that the effect of removing the odorous substance occurs in a short time, but there is no persistence in use for a long period of time. When the odorous substance is saturated with the adsorbent, the odorous substance is released again.

The present invention aims to provide a method for manufacturing a deodorant gel having antibacterial function while minimizing the cause of secondary environmental pollution by minimizing the amount of surfactant.

The present invention relates to a method for preparing a natural mineral mixture solution, which comprises adding buffering agent, gelling agent, inorganic salt, antifoaming agent, deodorizing component and natural mineral to purified water, mixing the purified water with water, adjusting pH to 4 to 9, ; Preparing a dispersing agent mixture solution by mixing a solubilizing agent, a dispersion stabilizer, a fragrance, and a food coloring matter; Adding the dispersant mixture solution to the natural mineral mixture solution and stirring the mixture for 10 to 60 minutes while maintaining the temperature in the range of 65 to 85 ° C to prepare a deodorant sol solution; And a step of putting the deodorant sol solution into a mold and cooling the deodorant gel to prepare a deodorant gel.

The method of manufacturing a deodorant gel to which a natural mineral is added according to the present invention has an effect of minimizing the amount of a surfactant and improving the function of a deodorant without changing the existing manufacturing process.

1 is a schematic view showing a method for producing a deodorant gel to which natural minerals are added according to the present invention.

The present invention relates to a method for preparing a natural mineral mixture solution, which comprises adding buffering agent, gelling agent, inorganic salt, antifoaming agent, deodorizing component and natural mineral to purified water, mixing the purified water with water, adjusting pH to 4 to 9, ; Preparing a dispersing agent mixture solution by mixing a solubilizing agent, a dispersion stabilizer, a fragrance, and a food coloring matter; Adding the dispersant mixture solution to the natural mineral mixture solution and stirring the mixture for 10 to 60 minutes while maintaining the temperature in the range of 65 to 85 ° C to prepare a deodorant sol solution; And a step of putting the deodorant sol solution into a mold and cooling the deodorant gel to prepare a deodorant gel.

Examples of the buffer that can be used in the present invention include hydroxycarboxylic acids such as citric acid; Natural amino acids such as glutamine and lysine; Inorganic anions such as borate ions, phosphate ions and carbonate ions; And chelating agents such as ethylenediaminetetraacetic acid (EDTA), nitrilotriacetic acid (NTA), and the like.

The antifoaming agents that can be used in the present invention may be one or more selected from non-silicone antifoaming agents such as silicone-based or polyalkylene glycol-based antifoaming agents.

The inorganic salts that can be used in the present invention include sodium salts such as NaCl, NaNO 3, and the like; Or a potassium salt such as KCl, KNO 3, and the like.

The gelling agent that can be used in the present invention may be one or more selected from the group consisting of carrageenan, agar, konjac and xanthan gum.

The deodorant that can be used in the present invention may be one or more porous supports selected from the group consisting of zeolite, silicate, metal phosphate, metal carbonate and metal oxide compounds.

The natural minerals that can be used in the present invention may be one or more selected from the group consisting of ilite, kaolinite, tourmaline and sericite.

Examples of the solubilizer that can be used in the present invention include nonionic solubilizing agents such as ethoxylated propoxylated alcohol (C = 12 to 14) and poly (ethyleneglycol); Anionic solubilizing agents such as sodium lauryl ether sulfate and lauric acid; And an amphoteric solubilizing agent such as cocoamidopropylbetaine, laurylbetaine, and the like.

Examples of the dispersion stabilizer that can be used in the present invention include 3-methyl-3-methoxybutanol (3MMB), 2- (2-butoxyethoxy) ) ethanol (BDG), and ethanol.

The perfume which can be used in the present invention includes natural and synthetic fragrances commonly used in the art, and nitro- and polycyclic fragrance is an artificial musk, and studies on human and environmental pollution due to toxicity and persistence And it is preferable to not use nitric and polycyclic aromatic solvents because they are currently warning of harmfulness.

The food coloring matter which can be used in the present invention may be any food coloring matter commonly used in the art.

BEST MODE FOR CARRYING OUT THE INVENTION Hereinafter, the present invention will be described in detail with reference to the following examples. However, the following examples are intended to illustrate the contents of the present invention, but the scope of the present invention is not limited to the following examples. Embodiments of the present invention are provided to more fully describe the present invention to those skilled in the art.

< Example > Natural minerals Ilright and Tourmaline  Deodorant added Gel  Produce

2.0 parts by weight of NaHCO 3, 2.0 parts by weight of carrageenan, 0.5 parts by weight of a zeolite type deodorizing component and 0.04 parts by weight of a silicone defoamer were added to purified water, and 2 parts by weight of a 40-nm- And 1 part by weight of tourmaline were respectively added and the pH was adjusted to 7.5 to 8.5 and then heated to 80 DEG C to prepare a natural mineral mixed solution. 6.0 parts by weight of cocamidopropyl betaine, 1.0 part by weight of lemon fragrance, 1.0 part by weight of rosemary flavor and 0.01 part by weight of edible blue No. 1 were prepared to prepare a dispersant mixture solution. 60 wt% of the natural mineral mixed solution and 40 wt% of the dispersant mixed solution were mixed and stirred for 30 minutes while maintaining the temperature at 60 to 80 캜 to prepare a deodorant sol solution. The deodorant sol solution was put into a mold and then cooled at room temperature for 180 minutes to prepare a solid deodorant gel.

< Experimental Example > Natural minerals Ilright and Tourmaline  Deodorant added Gel  Evaluation of sterilization characteristics

Staphylococcus aureus and Escherichia coli were used to measure the bactericidal effect of the solid deodorant gel prepared by the above examples, and the test was conducted in accordance with KS J 4206.

The evaluation results of the deodorant gel containing ilite and tourmaline are shown in Tables 1 and 2, respectively. It was confirmed that the treatment of the deodorant gel containing the natural mineral according to the present invention decreased the number of Staphylococcus aureus and E. coli there was.

Strain 1: Staphylococcus aureus
(Staphylococcus aureus ATCC 6538) Inoculum concentration (CFU / ml) 1.3 x 10 5 Growth rate (F) 54 times Ma 1.3 x 10 5 Mb 7.0 × 10 6 Mc <10 Decrease (%) 99.9

Strain 2: E. coli
(Escherichia coli ATCC 25922) Inoculum concentration (CFU / ml) 1.6 × 10 5 Growth rate (F) 51 times Ma 1.6 × 10 5 Mb 8.2 × 10 6 Mc <10 Decrease (%) 99.9

While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is to be understood that such detail is solved by the person skilled in the art without departing from the scope of the invention. will be. Accordingly, the actual scope of the present invention will be defined by the appended claims and their equivalents.

Claims (10)

After mixing the purified water with a buffer, a gelling agent, an inorganic salt, a defoaming agent, a deodorizing component, and a natural mineral, the pH is adjusted to a range of 4 to 9 and then heated to a temperature range of 50 to 90 ° C to prepare a natural mineral mixture solution step;
Preparing a dispersing agent mixture solution by mixing a solubilizing agent, a dispersion stabilizer, a fragrance, and a food coloring matter;
Adding the dispersant mixture solution to the natural mineral mixture solution and stirring the mixture for 10 to 60 minutes while maintaining the temperature in the range of 65 to 85 ° C to prepare a deodorant sol solution; And
And adding the deodorant sol solution to a mold and cooling the deodorant gel to prepare a deodorant gel. The method according to claim 1,
Wherein the buffer is one or more selected from the group consisting of hydroxy acids, natural amino acids, inorganic anions and chelating agents. The method according to claim 1,
Wherein the gelling agent is one or two or more natural polysaccharides selected from the group consisting of carrageenan, agar, konjac and xanthan gum. The method according to claim 1,
Wherein the deodorizing component is one or more porous supports selected from the group consisting of zeolite, silicate, metal phosphate, metal carbonate and metal oxide compounds. The method according to claim 1,
Wherein the natural mineral is one or more selected from the group consisting of ilite, kaolinite, tourmaline and cericite. The method according to claim 1,
Wherein the solubilizing agent is one or more selected from the group consisting of a nonionic solubilizing agent, an anionic solubilizing agent and an amphoteric solubilizing agent. The method according to claim 1,
The dispersion stabilizer may be at least one selected from the group consisting of 3-methyl-3-methoxybutanol (3MMB), 2- (2-butoxyethoxy) ethanol (BDG) Wherein the natural mineral is added to the deodorant gel. The method according to claim 1,
Wherein the natural mineral mixture solution contains 0.1 to 20.0 parts by weight of citric acid, 0.1 to 3.0 parts by weight of carrageenan, 0.1 to 3.0 parts by weight of konjac, 0.1 to 3.0 parts by weight of inorganic salts, 0.01 to 0.5 parts by weight of defoamer, 0.01 to 20.0 parts by weight of a natural mineral added to the deodorant gel. The method according to claim 1,
0.1 to 10.0 parts by weight of coconut amidopropyl betaine, and 0.1 to 10 parts by weight of 2- (2-butoxyethoxy) ethanol; , 0.1 to 5.0 parts by weight of a perfume, 0.1 to 5.0 parts by weight of a perfume, and 0.001 to 0.05 part by weight of a food coloring agent. 9. A deodorant gel to which natural minerals have been added, which is obtained according to the process of any one of claims 1 to 9.
KR1020130041696A 2013-04-16 2013-04-16 Preparation method of gel for deodorant by using natural mineral KR20140124221A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1020130041696A KR20140124221A (en) 2013-04-16 2013-04-16 Preparation method of gel for deodorant by using natural mineral

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1020130041696A KR20140124221A (en) 2013-04-16 2013-04-16 Preparation method of gel for deodorant by using natural mineral

Publications (1)

Publication Number Publication Date
KR20140124221A true KR20140124221A (en) 2014-10-24

Family

ID=51994557

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020130041696A KR20140124221A (en) 2013-04-16 2013-04-16 Preparation method of gel for deodorant by using natural mineral

Country Status (1)

Country Link
KR (1) KR20140124221A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20170003771A (en) * 2015-06-30 2017-01-10 (주)기륭산업 Agent for reducing foul smell and moisture content of sewage or wastewater sludge and manufacturing method thereof
KR101991826B1 (en) * 2018-04-19 2019-06-21 동의대학교 산학협력단 Deodorant for cleaning and antibacterial fiber

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20170003771A (en) * 2015-06-30 2017-01-10 (주)기륭산업 Agent for reducing foul smell and moisture content of sewage or wastewater sludge and manufacturing method thereof
KR101991826B1 (en) * 2018-04-19 2019-06-21 동의대학교 산학협력단 Deodorant for cleaning and antibacterial fiber

Similar Documents

Publication Publication Date Title
KR101433937B1 (en) Composition and methods for disinfectant and deodrant
KR101955683B1 (en) Eco-friendly hand-disinfectant composition containing extracts of natural material
US20100221207A1 (en) Fragrance coated salt crystals
JPH0211501A (en) Antimicrobial composition
JP2013508472A (en) Green sterilizing / disinfecting composition and method for producing the same
CN110813012A (en) Air purifying agent and preparation method and application thereof
CN109481713A (en) A kind of liquid deodorant and preparation method thereof
JP6896856B2 (en) Gel deodorant
JP2008081739A (en) Aromatic detergent for toilet
CN113349201A (en) Ethanol-gel-free no-wash disinfectant and preparation method thereof
CN104368026A (en) Environmental-friendly indoor environment purifying agent and preparation method thereof
KR20140124221A (en) Preparation method of gel for deodorant by using natural mineral
CN107828564A (en) A kind of soap for being capable of mosquito-expelling bactericidal and preparation method thereof
KR20130128512A (en) Preparation method of gel composition for deodorant and gel composition for deodorant obtained thereby
CN110947289B (en) Nano sterilizing smell-removing agent
CN109287626A (en) A kind of slow-release long acting antibiotic spray and its preparation and application
KR101772091B1 (en) Antibacterial fragrances composition and method for manufacturing antibacterial fragrances using the same
CN107603752B (en) Air conditioner cleaning agent with degerming effect
CN109463380A (en) A kind of high activity composite antibacterial spray and preparation method thereof
WO2008116768A1 (en) Anti-mite product
CN112877150A (en) Antibacterial and deodorant laundry detergent and preparation method thereof
CN101006788A (en) A nano-load slow release type antiseptic and preparation method thereof
KR20070080317A (en) Detergent composition
JPH06256792A (en) Antimicrobial cleansing agent for medicinal use
KR20060006709A (en) Nano silver or perfume raw materials contain papering walls adhesives

Legal Events

Date Code Title Description
A201 Request for examination
E902 Notification of reason for refusal
E601 Decision to refuse application