KR20130108010A - Cosmetic composition with the effect of calming skins - Google Patents

Abstract

PURPOSE: A cosmetic composition containing a fermented extract containing Sophora Flavescens roots, Chrysanthemum Boreale flowers, Cnidium Officinale roots, Saponaria Officinalis leaves, and Houttuynia cordata is provided to protect scalp and to relive skin irritation. CONSTITUTION: A cosmetic composition which protects scalp and relieves skin irritation contains 0.001-30 wt% (preferably 2 wt%) of a fermented extract containing Sophora Flavescens roots, Chrysanthemum Boreale flowers, Cnidium Officinale roots, Saponaria Officinalis leaves, and Houttuynia cordata. A method for preparing the cosmetic composition comprises the steps of: boiling a mixture containing Sophora Flavescens roots, Chrysanthemum Boreale flowers, Cnidium Officinale roots, Saponaria Officinalis leaves, and Houttuynia cordata at 80-100°C for 30 minutes to one hour to reduce contamination by microorganisms; dry-fermenting the mixture under an anaerobic fermentation condition at 20-50°C and a pH concentration of 5.0-7.0 for 1-7 days; performing solid fermentation of the fermented mixture using Bacillus sp. microorganisms and producing polymeric materials; sterilizing the polymeric materials; adding purified water or low carbon number alcohol (ethanol) to the polymeric materials in a volume ratio of 1:1-1:5; extracting the secondary mixture by hot water extraction or ultrasonic extraction and collecting the extract; and concentrating the extract.

Description

Cosmetic composition with the scalp protection and skin calming effect {Cosmetic composition with the effect of calming skins}

The present invention relates to a cosmetic composition having a scalp protection and skin soothing effect, and more particularly, as main ingredients, red ginseng (Sophora Flavescens Root), wild chrysanthemum (Chrysanthemum Boreale Flower), Cnidium Officinale Root, Soap (Saponaria Officinalis) It relates to a cosmetic composition capable of providing scalp protection and skin soothing effect by containing a fermented extract of Leaf, Houttuynia Cordata.

In general, the skin may be sensitive to external stimuli such as a dry environment. In this case, a simple case of temporary erythema may occur, but it may also cause complex problems such as severe itching and stinging, which causes an inflammatory response in appearance.

The mechanism of skin irritation is not known, but it is known that the most important defense function of the skin is abnormal and irritants penetrate into the skin and cause inflammation. Skin irritants also abnormally induce the function of intracellular metabolism and the pain associated with stimulation further increases the inflammatory response.

As an effort to prevent such skin irritation, research has been conducted on anti-irritant cosmetics, and in recent years, research and development on cosmetics using natural vegetable raw materials have been actively conducted in response to consumer demand.

Patent Document: Korean Application No. 10-2002-0013675

The present invention is to solve the above problems, to provide a cosmetic composition having a scalp protection and skin soothing effect using a fermented extract consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, eoseongcho as a component for skin protection.

Hereinafter, the present invention will be described in more detail.

In order to achieve the above object, the present invention provides a cosmetic composition containing a fermented extract obtained by fermenting a mixture consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, and eosungcho and then extracting and filtering.

Preferably the fermentation is a cosmetic composition, characterized in that obtained by fermenting 1 to 7 days while maintaining the pH 5 to 7 under the temperature conditions of 20 to 50 degrees C. to provide.

In addition, the Bacillus bacteria is preferably provided with a cosmetic composition, characterized in that Bacillus subtilis (Bacillus subtilis).

In addition, the extraction process is preferably 1 to 24 hours at a temperature of 40 to 90 degrees Celsius

It provides a cosmetic composition, characterized in that obtained during the treatment.

Further, preferably, the extract is a solvent selected from the group consisting of purified water, methanol, ethanol, glycerin, ethyl acetate, butylene glycol, propylene glycol, dichloromethane, chloroform, ethyl ether, butylene glycol, hexane and mixtures thereof. It provides a cosmetic composition, characterized in that the extraction using.

In addition, preferably the fermented extract consisting of red ginseng, wild chrysanthemum, cheongung, soap paste, eoseongcho is characterized in that it is contained in an amount of 0.0001 to 30.0% by weight based on the total weight of the cosmetic composition.

In addition, the cosmetic composition preferably provides a cosmetic composition having a scalp protection and skin soothing effect.

The cosmetics of the present invention through the above examples and experimental examples are to provide a cosmetic composition excellent in scalp protection and skin soothing effect by containing a fermented extract consisting of red ginseng, wild chrysanthemum, cheonggung, soap paste, eoseongcho.

The present invention relates to a cosmetic composition having a scalp protection and scalp protection and skin soothing effect, and more specifically, the main ingredient contains fermented extract consisting of red ginseng, wild chrysanthemum, cheongung, soap grass, eoseongcho, skin protection and soothing effect It has a large non-absorbance, good solubility, affinity, and stability in various bases and additives for cosmetics, organic solvents, etc., and provides a synergistic effect of significantly increasing the UV protection index, especially when used in combination with existing sunscreens. .

In the composition according to the present invention, the main ingredient is used in an amount of 0.0001 to 30% by weight, based on the dry weight of the fermented extract consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, and eosungcho.

The present invention wet-heat the mixture consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, Eochocho for 30 minutes to 1 hour at a temperature of 80 to 100 degrees Celsius to reduce microbial contamination and eluting the nutrients of the raw materials constituting each mixture After the step of forming the conditions to be easy to use the dry heat conditions of the mixture heat-treated mixture consisting of red ginseng, wild chrysanthemum, Cheongung, soap paste, eoseongcho at 20 to 50 degrees Celsius temperature, pH 5-7 and anaerobic fermentation conditions After fermentation using Bacillus microorganisms for 1 to 7 days under a solid material to produce a high molecular material, and then through the sterilization step, mixed with lower alcohol, especially ethanol, in a volume ratio of 1: 1 to 1: 5 Alternatively, the extract is stirred by using an ultrasonic extraction method, and the extract is concentrated and purified first. For further purification, low-molecular-weight substances can be removed by dialysis using a membrane filter with a molecular weight of 10 kD at 4 ° C. Distilled water in the same volume as the separated solution was added to lower the viscosity of the extract and then lyophilized to determine dry weight to determine productivity.

The extract thus prepared is added during cosmetic preparation.

The characteristics of the genus Bacillus strains are gram-positive bacteria, endogenous spore forming ability, characterized in that it has the form of enterococci. In addition, it is possible to grow under aerobic or anaerobic conditions, but not under anaerobic conditions, and has the characteristics of catalase production, casein, gelatin, and starch resolution. As the growth conditions, it is possible to grow at 7% saline, and to grow at about 45 ° C, which is a fermentation condition, and to grow at about pH 5.0 to 7.0. In addition, glucose, arabinose, xylose, and mannitol has the characteristic of generating an acid.

The cosmetic composition according to the present invention is characterized in that the fermented extract consisting of the prepared ginseng, wild chrysanthemum, cheonggung, soap paste, eoseongcho to 0.0001 to 30% by weight to preferably 2% by weight.

Cosmetic composition having scalp protection and scalp protection and skin soothing effect according to the present invention may have a conventional formulation, for example, supple cosmetics, astringent cosmetics, nourishing cosmetics, nutrition cream, body lotion, body oil, body essence, etc. It can be formulated as. The composition of each of these formulations may contain various kinds of bases and additives necessary for formulation of the formulation, and the kinds and amounts of these ingredients can be easily selected by those skilled in the art. Representative skin and lotion compositions of cosmetic compositions having scalp protection and scalp protection and skin soothing effects are described below by way of example.

In addition, the cosmetic composition having a scalp protection and scalp protection and skin soothing effect according to the present invention may be used according to a conventional method of use, and the number of times of use may vary depending on the user's skin condition or taste.

Hereinafter, the cosmetic composition having the scalp protection and scalp protection and skin calming effect of the present invention will be described in more detail with reference to the present invention, but the present invention is not limited to these examples.

Example 1 Preparation of Fermented Extract Composed of Red Ginseng, Wild Chrysanthemum, Cheongung, Soap Paste, Eoseongcho

The mixture consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, and eosungcho was wet-treated at 90 ° C for 1 hour to reduce microbial contamination and to form conditions to make the nutrients of the raw materials constituting each mixture easy to elute. After the fermentation process, the solid fermentation is carried out using Bacillus microorganism under dry fermentation conditions of 45 ° C temperature and pH 6.0, followed by the sterilization step to lower alcohol, especially ethanol as purified water or organic solvent. The mixture was added and mixed at a volume ratio, followed by stirring using a hot water extraction method to recover the extract, and concentrated and firstly purified. Productivity was determined by adding distilled water in the same volume as the separated solution to lower the viscosity of the extract and freeze-drying to measure the dry weight.

Example 2 Preparation of hair color having scalp protection and scalp protection and skin soothing effect according to the present invention

To prepare a hair color in the composition ratio as shown in Table 1. The alcohol part was produced by dissolving in the order of MP, tween 20, NP-12 in alcohol distilled at 78 ° C in the order of grain, and the purified water part was glycerin, 1,3-BG, DC-193, hyaluronic acid in sterilized purified water. , Allantoin, citric acid, prepared by dissolving in the order of soda citric acid and then mixed with the fermented extract consisting of red ginseng, wild chrysanthemum, cheongung, soap grass, Eochocho prepared in Example 1 to prepare a hair color.

Classification Raw material name Weight (% by weight) Award part Purified water 61.8 Etidronic acid 0.1 Ammonium thioglycolate 1.0 Polyquaternium-10 0.2 Resorcin 1.0 m-Aminophenol 0.6 p-amino-o-cresol 0.7 2-amino-5-nitrophenol 0.2 Sulfuric acid-p-phenylenediamine 2.4 Toluene Sulfate-2,5-diamine 0.3 Oil portion Cetyl alcohol 8.0 Cetearyl alcohol 3.5 Polyoxyethylene stearyl ether 2.0 Glyceryl Stearate SE 1.5 Sorbitan sesquioleate 1.5 Polysorbate 80 1.2 White Vaseline 4.0 Mineral oil 6.0 Isopropyl myristate 2.0 Natural ingredients Fermented extract of the present invention 2 Sum 100

Example 3: Preparation of hair tonic with scalp protection and scalp protection and skin soothing effect according to the present invention

Hair tonic was prepared in the same manner as in Example 2.

Raw material name Weight (% by weight) ethanol 25.0 Butylene glycol 3.0 glycerin 3.0 Dexpanthenol 0.1 Allantoin 0.1 Ginkgo Leaf Extract 0.1 L-menthol 0.3 Fiji-40-hydrogenated castor oil 0.5 Salicylic acid 0.2 Triclosan 0.1 Phenoxyethanol 0.2 Purified water 65.2 Methylparaben 0.1 Disodium iodide 0.1 Fermented extract of the present invention 2.0 Sum 100

Experimental Example 1: Check the skin irritation and calming effect of the hair color according to the present invention

Apply the hair color prepared in Example 2 (10m / 5cm2) to the forearm of 20 healthy men and women (10 males and 10 females) by a predetermined amount (10m / 5cm2) and shield the rest with aluminum foil for 30 minutes. Subsequently, long wavelength ultraviolet rays were irradiated at a dose of 10.2 J / cm 2 using an ultraviolet irradiator, and skin conditions (erythema, edema, papules, etc.) were observed after 24 hours. As a result, it was confirmed that the side effects such as erythema did not occur on the skin, and thus the hair color had no phototoxicity and had scalp protection, scalp protection, and skin calming effect.

Experimental Example 2: Confirm the skin irritation and calming effect of the hair tonic according to the present invention

Apply the hair tonic prepared in Example 3 (10m / 5cm2) to the forearm of 20 healthy males and females (10 males, 10 females) and cover the rest with aluminum foil for 30 minutes. Subsequently, long wavelength ultraviolet rays were irradiated at a dose of 10.2 J / cm 2 using an ultraviolet irradiator, and skin conditions (erythema, edema, papules, etc.) were observed after 24 hours. As a result, it was confirmed that the side effects such as erythema do not occur on the skin, and thus the hair tonic has no phototoxicity and has scalp protection and skin calming effect.

Experimental Example 3 Skin Stability Test of Hair Color and Hair Tonic According to the Present Invention

Human hair patch test was performed on the hair color and hair tonic prepared in Examples 2 and 3 in the forearm of 20 healthy adults (10 males and 10 females). Wipe the forearm of the subject well with 70% ethanol, and then place a pin chamber containing 20 μl of the hair color and hair tonic prepared in Examples 2 and 3 on a conventional cosmetic base using an adhesive tape for 24 hours. Closed attachment. After 24 hours, the adhesive tape and the pin chamber were removed, and the sample remaining on the skin with a gauze was lightly removed, and then the skin condition was observed, and again after 24 hours. As shown in Table 3, it was confirmed that there was no irritation on the human skin because no positive reaction was observed in the human patch test for confirming the skin irritation of the hair color and hair tonic according to the present invention.

sample After 24 hours (n = 20) After 48 hours (n = 20) Remarks Skin lotion 0/20 0/20 Number of reaction proton / Total number of subjects Hair tonic 0/20 0/20

To prepare a shampoo composition with reference to the components and contents shown in Table 4. In the case of the embodiment by combining a certain amount of fermented extract consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, eoseongcho to have an excellent scalp protection effect in addition to the cleaning effect, thereby having the effect of delaying hair loss caused by acne.

Shampoo Cosmetic Composition (Unit: wt%) Raw material name Comparative Example 1 Example 4 Lauryl diethanolamide 6.0 6.0 Sodium polyoxyethylene lauryl ether sulfate 30.0 30.0 Sodium Lauryl Sulfate Solution 15.0 15.0 Propylene glycol 1.0 1.0 Methyl Parahydroxybenzoate 0.2 0.2 Fermented extract of the present invention - 4.0 Pigment 0.5 0.5 Spices 0.5 0.5 Citric acid 0.1 0.1 Purified water Balance Balance Sum 100 100

Experimental Example 4: Determination of cleaning power

After 30 days, 1 day, 3 days, and 7 days after each dandruff and itching test, the degree of cleansing power was observed by the following method.

Criteria for Satisfaction Judgment Degree of skin irritation -2 The comparative example is very good -One The comparative example is slightly better 0 There is no difference. One The embodiment is slightly better 2 The embodiment is very good

The satisfaction of each subject was measured, and the average satisfaction was calculated by dividing by the number of subjects and is shown in Table 6 below.

Cleaning force measurement result sample Cleaning power After 1 day 3 days later After 7 days satisfaction 1.1 1.3 1.7

In the comparison between Example 4 and Comparative Example 1, the product according to Example 4 of the present invention was found to have a significant difference in satisfaction.

Experimental Example 5 Measurement of the Itching Effect of the Scalp

After 7 days, the degree of the itching effect of the scalp was observed according to the following judgment method for each 20 male and female subjects who had itching caused by the usual acne.

Measures for removing the itchiness of the scalp (based on a maximum of 10 points and a minimum of 1 point) score evaluation 10-8 points Very good (****) 7.9-6 points good(***) 5.9-4 points A little (**) 3.9-2 points is average(*) 1.9-1 points none

The satisfaction of each subject was measured, and the results are shown in Table 8.

Satisfactory effect of scalp removal division Comparative Example 1 Example 4 The itching effect of scalp * ****

As shown in Table 5, it can be confirmed that the cleaning composition prepared by containing fermented extract consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, and eochocho about the itch removal effect of the scalp is superior to the above items compared to the existing products. there was. In other words, the above effect is a natural physiologically active substance of fermented extract consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, and eochocho can be obtained by supplying an appropriate amount of the maximum functional active ingredient, due to the abundant essential nutritional ingredients It has an excellent scalp protection effect, which can delay hair loss due to acne, which can be expected to ultimately prevent hair loss by improving the itching of the scalp.

Claims (3)

Natural ingredients with scalp protection and skin soothing effect, contains 0.0001 to 30% by weight, preferably 2% by weight of fermented extracts consisting of red ginseng, wild chrysanthemum, cheonggung, soap grass, and eoseongcho Cosmetic composition having a soothing effect The method of claim 1,
The mixture consisting of red ginseng, wild chrysanthemum, cheonggung, soap paste, and eosungcho was wet-treated at 80 to 100 degrees Celsius for 30 minutes to 1 hour to reduce microbial contamination and to easily elute the nutrients of the ingredients constituting each mixture. After the step of forming a condition to ferment the mixture consisting of red ginseng, wild chrysanthemum, Cheongung, Soap, Eochocho in fermentation conditions at 20 to 50 degrees Celsius, pH 5.0 to 7.0, and anaerobic fermentation conditions for 1 to 7 days under dry culture conditions After fermentation, Bacillus microorganisms are used to produce high-molecular materials by solid fermentation, followed by the sterilization step, followed by addition and mixing of lower alcohols, particularly ethanol, in a volume ratio of 1: 1 to 1: 5 as purified water or organic solvent. A fermentation extract comprising a step of recovering the extract by stirring using the method, and concentrating and firstly purifying the extract. Cosmetic composition having a scalp protection and skin soothing effect, characterized in that The method of claim 2,
Scalp protection, characterized in that the step of removing the low molecular weight material through a dialysis using a membrane filter having a molecular weight of 10kD at 4 degrees C. And cosmetic composition having a soothing effect