KR20130085891A - The method manufacture sap of the lacquer tree resin & sap of the lacquer tree a composition in used antibiotic animal feed - Google Patents

Abstract

PURPOSE: Feeds antibiotic manufacture using lacquer resin composition and sterilization biocide formulation method using the same are provided to the nature feed antibiotic is manufactured and the lacquer extraction material is manufactured with water-soluble and it is usable to the nature killing insects sterilization deodorizing agent. CONSTITUTION: Feeds antibiotic tub using lacquer resin composition and nature sterilization killing insects deodorizing agent manufacturing method comprises the following steps. First process: the process of making urushiol which is the lacquer toxic material which 1 hour gad is stirred in gradually and the tannic acid is completely dissolved in lacquer and is contained in lacquer while it puts the tannic acid 50g into the reaction bath in the lacquer resin 1000g rate and it maintains the heat to about 80°C neutralized. Second process: the process of putting the honeysuckle 1000g Coptidis Rhizoma 1000g into the Houttuynia cordata 1000g rate which becomes in the high-pressure caldron with drying and adding the water 2000ml and manufacturing with the medicinal plant extraction material heating on 4 times about superheat and is concentrated. Third process: the process of putting the medicinal plant extraction material 2000ml of the second process in the caldron and 70% gad blowing moisture and sending and manufacturing the medicinal plant extraction material of about 600ml. Fourth process: the process of putting the corn oil 300g selected into the reaction bath in the lacquer resin composition 1000g rate of the first process among the cooking oil and mixing the gradually and being completely the lacquer resin composition and corn oil eminent. Fifth process: the process of being the mix and manufacturing the lacquer composite solution the herbal composition 30g of the third process with the lacquer resin composition 1000g rate of the fourth process. Sixth process: the process of being the sodium hydroxide 50g and emulsifying the lacquer resin composition while it adds the water 200ml while it is stirred in the gradually while it puts the herbal composition 30g of the third process into the reaction bath in the composition 1000g rate of the fourth process and it maintains heat to 80°C is included.

Description

The method manufacture sap of the lacquer tree resin & sap of the lacquer tree a composition in used antibiotic animal feed}

.

Lacquer has been used wisely by our ancestors for thousands of years. Lacquer is a unique plant that has both weakness and toxicity

In recent years, the value of lacquer has been highly valued. The lacquer has been proven to be antibacterial, deodorant, antibacterial, insect repellent, antiseptic, and anticancer. Lacquer, a sap collected from bark on lacquer trees, is a physiological secretion of plants. Seven-lacquered lacquer is an off-white oily liquid that tastes sweet and astringent and turns brown when in contact with air.

The main component of the lacquer is lacquer acid, or urushiol, which is hardened by enzymatic reaction when it comes into contact with oxygen in the air, and has been used as an old brush painting to form an excellent coating film of three-dimensional polymer, unlike other paints.

The main component of lacquer is urushiol, a polyphenol derivative. It is colorless transparent at first, or turns black when it comes into contact with air, and forms a coating film. Chemical formula C ₂₁ H ₃₄ O ₂ , viscous colorless liquid, boiling point 210∼ 222 ℃ (0.4 ~ 0.6mmHg). In air, it turns black and solidifies

It is not a single compound but a mixture of dihydrophenols. The structural formula of urushiol, the main component, is as follows

In the structural formula of urushiol, the side chain R is a group of four kinds represented by (CH 2) 14 CH 3 (CH 2) 7 CH (CH 2) CH CH CH CH CH CH CH CH CH CH CH CH CH CH CH CH CH CH Mixture.

Urushiol, a lipid component of lucidum, is firstly oxidized by lacase, a carbohydrate enzyme in lacquer tree sap. Subsequently, the unsaturated chain in urushiol is converted into a quinone compound in humid air, This auto-oxidation occurs and forms a complex network structure

Urushiol exhibits antioxidant properties with two hydroxyl groups (-OH) as in the above structural formula. Lacquer decreases the antioxidant level due to the decrease of hydroxyl group by enzymatic polymerization. Therefore, automatic oxidation occurs in two stages as the lacquer polymerizes. This can be confirmed by measuring antioxidant activity and fisheries device.

Urushiol (Phenolic Compounds) + O2 (Air)-Laccase (Oxidase)-> Quinone compound + H2O2 ....... (1)

Quinone commpound + Protein, Amino acid, other organic acids, etc .---> Network structure + H2O2 .... (2)

When lacquer breaks down the skin, urushiol and laccase, which are the components of lacquer, get on the skin, causing uricol to be allergic dermatitis caused by reaction with skin protein as oxidized by the oxidation catalyst of laccase in air. Silver lacquer phenomenon will appear

To date, it has been reported that chilled liquid is very difficult to dry, so it is not easily dried by heat or artificially, and is dried only in moderate moisture and temperature conditions

Once upon a time, when our lacquer was lacquered with lacquer liquor, lacquer liquor was mixed with lacquer liquor in a certain proportion, and lacquer liquor was dissolved.

Today, in order to lacquer the lacquer solution (liquor) on the column, lacquer solution is mixed with a certain ratio of terfenafine to maintain the humidity at 70 to 75%, and the lacquer is dried at a temperature of 20 ° C to 25 ° C

So far, there is a manufacturing method of lacquered chicken using lacquer. For example, the polyolefin polymer material is raised to the polymer application temperature (130 ° C.-200 ° C.). To form a polymer agglomerate and mix the lacquer sap in an amount within 20% by weight based on the weight of the polymer, and then stir to produce a mixed melt of the polymer and lacquer, and then extrude and manufacture the salt-resistant heat-resistant waterproof antiseptic insect repellent And a polyolefin composite resin and a method of preparing the same, which are mixed with a lacquer component having excellent insulating properties, but the prior art is a polyolefin resin and a polypropylene resin because the polymer structure does not mix the polyolefin resin and the polyethylene resin. There is a problem that the composition-containing polyolefin composite resin can not be produced, and Publication No. 1020020 090040 (20021130) describes an engineering synthetic resin such as polysulfone polycarbonate (PC) dissolved in an organic solvent in a concentration of 1-50% by weight, and purified lacquer liquor is 20% by weight based on the weight of the polymeric material. Engineering composite resin mixed with flameproof heat-resistant waterproof antiseptic antiseptic property and insulation prepared by molding the mixed solution of the polymer and the lacquer sap and drying it, and its manufacturing method are described. Patent No. 103342930000 (20020413) discloses that a <1> polymer material used as a synthetic resin is dissolved in an organic solvent at a concentration of 10% by weight, and then the purified lacquer sap is mixed within 20% by weight based on the weight of the polymer material. And melt the polymer solution of the polymer lacquer sap and then dry the polymer material that is stored or used as a synthetic resin. After melted, it is melted and extruded through a slit die, and then rapidly cooled in a roller, and then taken into consideration. A functional synthetic resin blended in the same and a method of manufacturing the same are disclosed, and U.S. Publication No. 1008420320000 (20080623) contains a urushiol prepared by pulverizing a raw vegetable mixture prepared by mixing a reaction of urushiol and isocyanate (ISOCYANATE). It is understood that a lacquer-containing sealant and a method for producing the lacquer, characterized in that the lacquer powder or lacquer is mixed with a silon sealant or an acrylic sealant and then cured.

In addition, the medicinal herbs used in the present invention, Indongcho, Eochocho and Pyeonchang are widely used in Korean medicine. Echoseongcho has been used for many years in dysentery diarrhea because it has been proved to have excellent sterilization ability since ancient times. It has been widely used for various treatments and has been reported to be effective for colds and respiratory diseases, and especially for killing E. coli, Staphylococcus aureus.

In addition, Hwangyeon is a perennial herb attached to Apiaceae, which has the effect of killing various bacteria. Especially, it has been recorded that antibacterial has detoxification effect on diarrhea and killing allergic pneumococci.

In the present invention, when the medicinal herbs are mixed with lacquer extracts, the extracted medicinal water is mixed with lacquer extract to produce a feed, and when fed to leather or animals, it has a natural antibiotic effect and is especially developed for lacquer juice. The technical core of the present invention is to prepare a passive natural insecticide disinfectant by mixing with the Indongcho liquor composition and use it as a deodorant for agricultural crops or livestock manure.

In general, lacquer liquor is highly toxic and thus is a problem in use, and it is a problem in use because it is not mixed well with other substances.

In the present invention, when tannin acid is mixed and stirred in the lacquer solution, urushiol contained in the lacquer causes toxicity, and tannin acid reacts with urushiol to neutralize the lacquer toxicity, using tannic acid as a lacquer poisoning remover, and also removing lacquer toxicity. In order to find out that lacquer toxic solution is boiled at high temperature for a long time, lacquer poisoning is removed.Because the lacquer is boiled at high temperature to remove poison, the lacquer juice is mixed well with soybean oil, corn and vegetable varieties, which is cooking oil. A lacquer composition was prepared by mixing at a ratio, and then concentrated by weighing the medicinal herbaceous japonica with sterilizing effect from herbs, and mixing the lacquer composition with a predetermined amount and then mixing the lacquer composition with a predetermined amount of feed material in a feed manufacturing process. Natural feed antibiotics were prepared by adding lacquer feed, especially lacquer It was mixed with the liquid composition and the Houttuynia cordata indongcho chrome expelled water to prepare a water-soluble essence lacquer composition that is dissolved in water to prepare a sterile natural pesticide is an object of the object of the present invention

.

.

As described above, the lacquer extract and herbal composition of the present invention are added to the feed as a natural antibiotic to prepare a lacquer feed, and the lacquer extract and the herbal composition are mixed to remove the water-soluble lacquer composition to remove natural fungicides and insecticides. The manufacturing method is explained in more detail as follows.

▶ Step 1

Process of neutralizing urushiol, a lacquer toxic substance contained in lacquer, by adding 50 g of tannic acid to the reaction tank at a rate of 1000g of lacquer solution and stirring it slowly for about 1 hour while maintaining the heat at about 80 ° C.

▶ Step 2

Process of preparing concentrated herbal extracts by adding 1000g of Indongcho to 1000g ratio of well-dried fish vinegar in high pressure cauldron and adding 2000ml of water to boil at high heat for about 4 hours.

▶ Third Process

Put 2000ml of herbal extracts of the second process into the cauldron and blow about 70% of moisture and produce about 600ml of herbal extracts

▶ Fourth Process

Edible oil (soybean oil, corn oil, vegetable varieties, etc.) at a ratio of 1000 g of lacquer essence composition of the first step

Put 300g of selected corn oil into the reaction tank and slowly stir to make the lacquer liquid composition and corn oil completely dissolve

▶ Fifth Process

A process of preparing a lacquer composition solution by mixing and mixing 30 g of the herbal composition of the third process at a rate of 1000 g of the lacquer liquid composition of the fourth process

▶ Sixth Process

Process of adding 30 g of the herbal composition of the third step to the reaction tank at the rate of 1000 g of the composition of the fourth step into the reaction tank and adding 50 ml of caustic soda while adding 200 ml of water while slowly stirring while maintaining the heat at 80 ° C. and emulsifying the lacquer juice composition.

▶ Step 1

Lacquer feed preparation process by mixing and mixing 1000 g of feedstock at a rate of 30g lacquer liquid composition prepared in the fifth step of [Example 1] in the feed manufacturing process

▶ Step 2

A process of mixing and mixing 10000ml-20000ml of water at a ratio of 100g of lacquer composition prepared in the fifth step of [Example 1] and using it as a natural disinfectant or insecticide and deodorant

<Experiment result>

30 g of the lacquer feed prepared above was mixed with 1000 g of filtered water and 30 g of lacquer extract developed as a bactericidal insecticide in 1000 ml of water, and the bactericidal efficiency of Escherichia coli and Staphylococcus aureus were tested. % Could be confirmed by the test results

Claims (2)

In the manufacture of animal feed antibiotics using natural lacquer composition and the method of manufacturing natural sterilization insecticide deodorant
▶ Step 1
Process of neutralizing urushiol, a lacquer toxic substance contained in lacquer, by adding 50 g of tannic acid to the reaction tank at a rate of 1000g of lacquer solution and stirring it slowly for about 1 hour while maintaining the heat at about 80 ° C.
▶ Second Process
Process of preparing concentrated herbal extracts by adding 1000g of Indongcho to 1000g ratio of well-dried fish vinegar in high pressure cauldron and adding 2000ml of water to boil at high heat for about 4 hours.
▶ Third Process
Put 2000ml of herbal extracts of the second process into the cauldron and blow about 70% of moisture and produce about 600ml of herbal extracts
▶ Fourth Process
Edible oil (soybean oil, corn oil, vegetable varieties, etc.) at a ratio of 1000 g of lacquer essence composition of the first step
Put 300g of selected corn oil into the reaction tank and slowly stir to make the lacquer liquid composition and corn oil completely dissolve
▶ Fifth Process
A process of preparing a lacquer composition solution by mixing and mixing 30 g of the herbal composition of the third process at a rate of 1000 g of the lacquer liquid composition of the fourth process
▶ Sixth Process
Process of adding 30 g of the herbal composition of the third step to the reaction tank at the rate of 1000 g of the composition of the fourth step into the reaction tank and adding 50 ml of caustic soda while adding 200 ml of water while slowly stirring while maintaining the heat at 80 ° C. and emulsifying the lacquer juice composition. Process to use as lacquer natural disinfectant or insecticide and deodorant
▶ Step 1
Lacquer feed preparation process by mixing and mixing 1000g feedstock at 30g ratio of lacquer liquid composition prepared in the fifth step of [Claim 1] in the feed manufacturing process
▶ Second Process
Process of mixing and mixing 10000ml-20000ml of water in 100g ratio of lacquer composition prepared in the fifth step of [Claim 1] to use as natural disinfectant or insecticide and deodorant