KR20130053799A - The liquefied dentifrice making method besides - Google Patents

Abstract

PURPOSE: Liquid toothpaste and a method for manufacturing the same are provided to treat periodontal diseases and gingival inflammation by anti-inflammatory and antibacterial functions. CONSTITUTION: A method for manufacturing liquid toothpaste comprises: a material preparation step(S1) of cutting Sambucus sieboldiana, Ulmus pumila, and Albizzia julibrissin and preparing ingredients; an extraction step(S2) of mixing the ingredients and water and boiling at 90-100 deg. C, removing the ingredients, and collecting an extract; and a purification step(S3) of mixing the extract with 30-100% ethyl alcohol and distilling at 90-100 deg. C. The extract and ethyl alcohol are mixed in a volume ratio of 1:0.2-0.4. [Reference numerals] (S1) Material preparation step; (S2) Extraction step; (S3) Purification step; (S4) Additive mixing step

Description

Liquid toothpaste and its manufacturing method {The liquefied dentifrice making method besides}

The present invention relates to a liquid toothpaste and a method for manufacturing the same, and more particularly, by preparing a liquid toothpaste, including extracts of the grafting (유 木), Yu-Geun-pi (피 根 皮) and silk tree, Anti-inflammatory and antibacterial and anti-pain-relieving effect of root skin can be expected to treat periodontal disease and gum inflammation, and can also prevent disease by eradicating bacteria that cause periodontal disease and gum inflammation in advance. It relates to a liquid toothpaste and a method for producing the same.

In general, toothpaste compositions typically used for cleaning mouths and teeth are in the form of pastes, powders, gels, mucus, and liquids, and have certain advantages and disadvantages in their use and handling.

For example, the pasty toothpaste has a high viscosity, is likely to cause damage to the tooth enamel layer due to the abrasive component, is not easy to squeeze in use, and the residual amount of toothpaste remains in a container that is discarded because the product in the container cannot be used completely. There is a problem that causes environmental pollution, the powdered toothpaste is inconvenient in use because the particles are sprayed or scattered during use, the gelated toothpaste is a thing containing an abrasive and not containing, but the spreadability is high due to high viscosity There are inconveniences in use that do not readily disperse in the oral cavity.

In addition, the liquid toothpaste is widely used as an oral goggle agent to perform the function of suppressing oral bacteria and removing bad breath, but due to the problem of lacking cleaning components, it can be expected to have sufficient gargling effect such as removing oral plaque and removing oral bacteria. There was no.

Moreover, liquid toothpaste cannot expect the functionality to prevent or treat diseases such as periodontal disease and inflammation of the gums, so the general purpose of use is low. Therefore, there is an urgent need for the development of functional liquid toothpaste that can be expected to prevent and treat diseases. to be.

The present invention has been proposed to solve the above-mentioned problems, the purpose of the liquid toothpaste including the extract of the grafting geungeok (유 木), Yu-Geun-pi (楡 根 皮) and silk tree, Anti-inflammatory action, anti-inflammatory action and antibacterial action of root skin and antibacterial and pain-relieving action of silkworm tree can be expected to treat periodontal disease and gum inflammation as well as eradicate the disease that causes periodontal disease and gum inflammation in advance. The present invention provides a preventable liquid toothpaste and a method of manufacturing the same.

Liquid toothpaste manufacturing method according to an embodiment of the present invention for achieving the above object is to prepare the extraction material by slicing the graft alley, Yukeunpi (피 根 皮), and silk tree (細 切) A material preparation step (S1) consisting of 25 to 50% by weight of the grafted tree, 25 to 50% by weight of the root skin, and 8 to 26% by weight of the silk tree; and, the material preparation step After mixing the extract material prepared in (S1) with water and heated to 90 to 100 ℃, to remove the extract material from the water to collect the extract, the extract material and water to be mixed in a 1: 2 to 4 weight ratio Extraction step (S2); And, the extract extracted in the extraction step (S3) is mixed with 30 to 100% ethyl alcohol (Ethyl-Alchol) and heat distilled to 90 to 100 ℃ to collect the liquid composition from which impurities are removed However, the extract and ethyl alcohol is 1: 0.2 to 0.4 It comprises a; purification step (S3) to be mixed in a volume ratio.

In addition, in place of the roots of the roots used in the material preparation step (S1) is characterized in that any one selected from the roots and violet flowers.

In addition, an additive mixture is added to the liquid composition collected in the purification step (S3) to further improve the quality of the product by adding an additive used as a preservative, a sweetener and a flavoring agent. Step (S4); further comprising, wherein the additive is added to the liquid composition is characterized in that the weight corresponding to 20 to 30% by weight relative to the total weight of the liquid composition.

In addition, the additive is characterized by consisting of any one or two or more selected from the group consisting of vegetable glycerin, lavender essential oil, menthol, pine salt, xylitol.

Liquid toothpaste according to another embodiment of the present invention for achieving the above object is characterized in that it is prepared through the manufacturing method described above.

According to the liquid toothpaste according to the present invention and the manufacturing method as described above, by preparing a liquid toothpaste, including the extract of the graft alley (接骨木), Yu Geun-pi (楡 根 皮) and silk tree, Anti-inflammatory and antibacterial and anti-pain-relieving effect of root skin can be expected to treat periodontal disease and gum inflammation, and can also prevent disease by eradicating bacteria that cause periodontal disease and gum inflammation in advance. It works.

1 is a block diagram of a liquid toothpaste manufacturing method according to an embodiment of the present invention

The method for preparing a liquid toothpaste according to a preferred embodiment of the present invention will be described in detail with reference to the accompanying drawings.

1 illustrates a method for preparing a liquid toothpaste according to an embodiment of the present invention.

As shown in the figure, the liquid toothpaste manufacturing method 100 according to an embodiment of the present invention comprises a material preparation step (S1), an extraction step (S2), and a purification step (S3).

The material preparation step (S1) is prepared by extracting the graft alley (接骨木), yugeunpi (楡 根 皮), and the silk tree (추출) to prepare the extraction material, the graft alley with respect to the total weight% of the extract material It consists of 25 to 50% by weight, 25 to 50% by weight of the root skin, 8 to 26% by weight of the silk tree.

[ Grafting ]

In general, the grafting tree belongs to Indong and Elderberry, and it is a larch tree that grows in mountain marshes and valleys.

It grows up to 3 ~ 5m in height, leaves are pinnate leafs, 5 ~ 7 small leaves, long oval (long oval), long pointed, sharp edges, not bent inside. Conical at the end of branch with small bumps, hairless, small yellow-green flowers. The flower is deeply divided into 5 pieces, without hairs, and the anther is yellow. Fruits are round, dark red, and ripe.

The roots and roots of the graft alley are grafted to the root of the graft (접 木 根), the leaves to the graft on the leaves (接骨木 葉) and blossoms are called medicinal graft (接骨木 花).

The names of the grafting alleys are grafting alleys (接骨木, woodcutting, Dangboncho), golgolcho [Yumamamboncho], Sokgol Alley [續 骨 木: Bonchogangmok] Cheoncheon bow [Bonggyeongbong garden], Chil yeophwang hyung [七葉 黃 荊, Banggon line: 放 棍 行, Coral boat: 珊瑚 配, Cheoncheon bow: Wangyeonsa (汪 連 仕), Chaeseoseo (採藥 書) ], Cheolgolsan [鐵骨 散: Botanical Name Room Dogo], Golgoldan [Goldan: Herbal Herbs], Chilgeumum [七葉 金: Tugolcho: 透骨 草: Fujian Folk herb (福建 民間 草藥)], golgol wind [接骨 風: Sichuan medicinal land], undertaking [highway road number: 公道 老 樹, large leaf alley: 大 葉 接骨木, large leaf cutting, Seo Geun Soo: 舒筋 樹, Jangmoksoo: 樟木 樹: Chinese medicinal dictionary (中藥 大 辭典)], Goryeo alley (高 목 木), earthworm tree, cedar, elder tree and so on.

[Pharmacological action]

These, graft alleys are usually effective to drive out the wind sand (을), discharge moisture, promote blood circulation and relieve pain, pain, back pain, species, wind yang, Eunjin (damage), postpartum anemia It is used to treat swelling and pain from bruises, fractures, wound bleeding, and inflammation in the throat and mouth.

On the grafting alley, An Deok-gyun's CD-ROM Herbal Medicine of Korea records as follows.

Origin of the branch of Sambucus williamsii var. Coreana Nakai.

[Taste] Taste is sweet and bitter, weakness is mediocre.

[Efficacy doctors] Dungpoong 祛 (濕 風 利濕), blood circulation pain (活血 止痛) is.

[Clinical application]

1. It is effective for customary arthritis, back pain, fractures and traumatic bleeding.

2. There is an act of blood (活血), after the postpartum (産後) to remove the blood (瘀血), write on the bruise.

3. Hives, itchy skin, used as a bath.

4. It shows remarkable response to fracture fusion promotion.

[Clinical study] Promotes bony union on fractures. Pregnant women should not take it.

[Pharmacological] Water decoction is used to treat pain and inflammation in the throat and mouth. Diuretic effect was also shown.

Contains chemicals Sanbicyanin, cyanidol glucoside, amino acid, canogenic glucoside, iridoid glucoside, morronniside.

[ Yugunpi ]

In general, the name of elm is called dermis, dermis root, stem bark dermis, root bark is called dermis.

This elm tree is about 10m tall, and its shape is similar to zelkova. It grows near the watersides and valleys in the mountains of central and northern Korea. There are many kinds, the ripening time and the type of peel is different, but the pharmacological effect is the same. Fruits of elm round elm ripen in September-October, and sugar elm trees ripen in April-May.

On the nutritional side, the bark contains flavonoid saponin tannin slime, the leaves contain flavonoids, and the fruit contains tannin slime.

In <Dictionary of Synonym>, “Yu Geun-pi's acts on parenteral menopause and colonoscopy. Pee well, remove the heat of the stomach and calm the swollen. Write medicine as a cough, edema, gastritis, etc. 12 to 30 grams a day or moon is made into powder. When used as an external medicine, wash or powder with decoction. ”

In particular, myodermis extract is good for the treatment of inflammation that can appear anywhere, such as body organs and skin.

[Wood tree]

A silk tree is a symbol of the couple's golden thread, and it is also called a sum-of-water, sum-of-the-law, wild water, or oil. For this reason, many trees were planted in the yard as garden trees. Since it was a tree used to make the handle of the silk, there is a place called a silk tree, and the cow eats well.

The trunk of the tree is bent or slightly laid down. It is 3 ~ 5m high, and large branches are sparse. Small branches have ridges. The leaves are alternated and the two-folded double leaves. The leaf is curved like a sickle, long oval with the same right and left side, and the edge is flat. Small leaves are 6 ~ 15mm long, and butterfly is 2.5 ~ 4.0mm long. There are no hairs on both sides or hairs on the back vein.

The flower is light pink and blooms in June-July, and hangs 15-20 at the end of a small branch. Calyx and corolla are shallowly divided into 5 and turn green. Surgery is about 25, long out and the upper part is red. The flower appears red because of the color of the stamens. Fruits ripen in September-October, flat pods, about 15cm long, with 5-6 seeds. The peculiarity is that the nerve sheath or mimosa are attached to the external stimulus, but the algae are folded after the sun goes down.

[Pharmacological effect]

1. Excellent for alleviating pain.

2. The antibacterial effect of removing harmful bacteria in the body is excellent.

3. It has the effect of stabilizing the mind and body to clear the mind.

4. Good osteopathy effect on bone.

In addition, in place of the roots of the roots used in the material preparation step (S1), any one selected from the roots and violets having a similar effect to roots of roots can be used.

[Mallow root]

The official name of the mango tree is Cheongmirae vine, a deciduous broad-leaved vine that grows wild in the sun below 1,600m above the alpine area.

The growing environment inhabits half shade or sunny places. The height is 2 ~ 3m, the leaves are 3 ~ 12㎝ long, 2 ~ 10㎝ wide, radiant and chewy. The petiole is 0.7 ~ 2㎝ long, and the chin leaves are tendrils. The flower is yellowish green and hangs on the axilla. The stem is 1.5 ~ 3㎝ long and the stem is 1cm long. Fruits ripen in red in September-October and are round and about 1cm in diameter.

Young leaves and fruits are used as edible and root medicinal, and the roots are widely used as antidote because they are excellent in detoxifying heavy metals such as syphilis, playing window, inflammation, swelling, swelling and mercury.

[violet]

It is also commonly called longevity flower, chick flower, orange flower, wrestling flower and sitting flower. Commonly growing in the field, about 10cm high. Leaves grow with long stems, without stems, and spread obliquely to the side. Leaves are long oval lancets, with dull and marginal sawtooths. After flowering, the leaves are broad triangular lancets, with wings on top of petioles. Grow up

Normally, flowers bloom from April to May, with stalks growing between the leaves, one at the end, running sideways. Flower color is deep reddish purple, and calyx leaves are basso shaped, pointed at the end, and appendages are semi-circular with flat edges. The petals are hairs on the side fork and have a large honey bag. The fruit is ripe and ripens in June.

These, violets are widely used as medicinal herbs because of their excellent detoxification, antibacterial action and anti-inflammatory action against various inflammations.

As described above, the material having the effects of anti-inflammatory and analgesic action of the grafting graft, anti-inflammatory and antimicrobial action of the roots and antimicrobial and analgesic action of the rootwood extract as an extract in the extraction step (S2) to be removed By using it in the liquid toothpaste, through the antibacterial action can be expected to remove harmful caries and treatment of periodontal disease and gum inflammation caused by caries.

In addition, the above-described effects can be expected even when using the root of the tree or violets instead of the roots of the root.

The extraction step (S2) is to mix the extract material prepared in the material preparation step (S1) with water and heated to 90 to 100 ℃, to remove the extract material from the water to collect the extract, the extract material and water Is 1 to 2 to 4 by weight ratio.

Preferably, the extracting material and water are mixed at a weight ratio of 1: 3.

In the purification step (S3), the extract extracted in the extraction step (S3) is mixed with 30 to 100% ethyl alcohol (Ethyl-Alchol) and heated and distilled to 90 to 100 ℃ to collect the liquid composition from which impurities are removed, The extract and ethyl alcohol is a step to be mixed in a volume ratio of 1: 0.2 to 0.4.

Here, the liquid composition collected by removing impurities while the distillation process of the purification step (S3) can be used as a liquid toothpaste as a finished product.

In addition, in order to improve the quality of the liquid composition collected in the purification step (S3) and to improve the feel of toothpaste, additives used as preservatives, sweeteners and flavoring agents are added. It is preferable to further include an additive mixing step (S4) to be added.

Here, the additive is added to the liquid composition to add a weight corresponding to 20 to 30% by weight relative to the total weight of the liquid composition,

The additive may be made of any one or two or more selected from the group consisting of vegetable glycerin, lavender (Lavender) essential oil, menthol, pine salt, xylitol.

Here, vegetable glycerin, lavender essential oil and pine salt are selectively used as a preservative, xylitol is used as a sweetener, and lavender essential oil and menthol are optionally used as a flavoring agent.

Liquid toothpaste manufacturing method 100 according to an embodiment of the present invention having the configuration as described above will be described in detail through the following examples, of course, it is not limited to these examples.

[Example 1] to [Example 3] is a liquid toothpaste prepared by the liquid toothpaste manufacturing method 100 of the present invention, [Comparative Example 1] is a liquid toothpaste prepared by a general method.

[ Example  One]

First, prepare the extract material by cutting each graft alley: 600g, the root of the roots: 600g, the silk tree: 300g. (S1)

Then, 4.5 g of water (the specific gravity of the water is 1 kg / m 3, 4.5 g of water corresponds to 4500 g by weight) were added to 1500 g of the extract material including the grafted glenoid and the roots of bark and silk tree, and then 3 ml of extract was obtained. Heat to 95 ° C. until possible. (S2)

Then, after mixing 80 ml of ethanol concentration 80ml to 3L extract, and purified by heating to 95 ℃ to remove impurities remaining in the extract by distillation to collect the liquid composition. (S3)

Here, of course, the liquid composition purified through the distillation process can be used as a liquid toothpaste as a finished product.

Then, 400 g of additive vegetable glycerin, 10 g of lavender essential oil, 40 g of menthol, 80 g of pine salt, and 130 g of xylitol are further added to the liquid composition to complete the preparation of the liquid toothpaste as a finished product. (S4)

[ Example  2]

First, crush the graft alley: 600g, the tree roots: 600g, the silk tree: 300g to prepare the extract. (S1)

Then, 4.5 g of water (the specific gravity of the water is 1 kg / m 3, 4.5 g of water corresponds to 4500 g by weight) were added to 1500 g of the extract material combining the grafted tree and the spruce roots and silk tree, followed by 3 l of extract. Heated to 95 ° C. until (S2)

Then, after mixing 80 ml of ethanol concentration 80ml to 3L extract, and purified by heating to 95 ℃ to remove impurities remaining in the extract by distillation to collect the liquid composition. (S3)

Here, of course, the liquid composition purified through the distillation process can be used as a liquid toothpaste as a finished product.

Then, 400 g of additive vegetable glycerin, 10 g of lavender essential oil, 40 g of menthol, 80 g of pine salt, and 130 g of xylitol are further added to the liquid composition to complete the preparation of the liquid toothpaste as a finished product. (S4)

[ Example  3]

First, the extracts are cut into small pieces of 600 g, violet: 600 g, and silk tree: 300 g. (S1)

Then, 4.5 g of water (the specific gravity of the water is 1 kg / m 3, 4.5 g of water corresponds to 4500 g by weight) were added to 1500 g of the extract material combining the grafted gall and violet and silk tree, and then 3 extracts were obtained. Heat to 95 ° C. until possible. (S2)

Then, after mixing 80 ml of ethanol concentration 80ml to 3L extract, and purified by heating to 95 ℃ to remove impurities remaining in the extract by distillation to collect the liquid composition. (S3)

Here, of course, the liquid composition purified through the distillation process can be used as a liquid toothpaste as a finished product.

Then, 400 g of additive vegetable glycerin, 10 g of lavender essential oil, 40 g of menthol, 80 g of pine salt, and 130 g of xylitol are further added to the liquid composition to complete the preparation of the liquid toothpaste as a finished product. (S4)

[ Comparative example  One]

A general liquid toothpaste is prepared by adding 400 g of vegetable glycerin, 10 g of lavender essential oil, 40 g of menthol, 80 g of pine salt, 130 g of xylitol, and 3 l of water.

Therefore, [Example 1] was purified the extracts of Graft Alley, Root Bark and Silkwood, and prepared liquid toothpaste by adding an additive to the purified liquid composition, and [Example 2] Graft Alley, Aspen root and After purifying the extract of the Albizia julibrissin, an additive was added to the purified liquid composition to prepare a liquid toothpaste. To prepare a liquid toothpaste was prepared, whereas [Comparative Example 1] was prepared by adding an additive to water to prepare a general liquid toothpaste.

That is, the composition and the additives of the [Example] and [Comparative Example] are as shown in [Table-1] below.

Table-1

Here, for the liquid toothpaste of [Example 1] to [Example 3] and [Comparative Example 1], the change in the gum inflammation index was evaluated while brushing according to a conventional method. The results are shown in Table 2 below.

Gingivitis Index (GI) is a measure proposed by Loe and Silness as follows:

0: normal gingiva;

1: mild inflammation (slight tint change, mild edema, no tendency to bleeding from periodontal probe);

2: severe inflammation (redness, change in hue of edema gingival, bleeding from periodontal probe);

3: severe inflammation (with significant redness, swelling, ulceration and continuous bleeding)

TABLE 2

That is, as shown in [Table-2], the liquid toothpaste of [Example 1] to [Example 3] manufactured according to the liquid toothpaste manufacturing method 100 of the present invention, the liquid toothpaste of [Comparative Example 1] It was confirmed that the effect of improving gum inflammation is excellent.

Therefore, the liquid toothpaste prepared through the liquid toothpaste manufacturing method 100 of the present invention can prevent the periodontal and gum disease that may be caused by the decay bacteria in advance by removing the decayed bacteria that cause inflammation of the gums, at the same time when the inflammation of the gum It can effectively improve gum inflammation.

While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is clearly understood that the same is by way of illustration and example only and is not to be construed as limiting the scope of the invention as defined by the appended claims. You will understand the point. It goes without saying that variations can be made by those skilled in the art without departing from the spirit of the present invention. Accordingly, the scope of claim of the present invention is not limited within the scope of the detailed description, but will be defined by the following claims and technical ideas thereof.

S1. Material preparation step S2. Extraction step
S3. Purification step S4. Additive Mixing Step
100. Liquid toothpaste manufacturing method

Claims (5)

In the liquid toothpaste manufacturing method,
Prepare the extraction material by slicing the grafting alley, Yugeunpi (楡 根 皮), and silk tree, but 25 to 50% by weight of the grafting allotment with respect to the total weight of the extraction material 25 to 50% by weight, the material preparation step (S1) consisting of 8 to 26% by weight of the silk tree;
After mixing the extract material prepared in the material preparation step (S1) with water and heated to 90 to 100 ℃, to remove the extract material in water to collect the extract, the extract material and water is 1: 2 to 4 weight Extraction step (S2) to be mixed at a ratio; And
The extract extracted in the extraction step (S3) is mixed with 30 to 100% ethyl alcohol (Ethyl-Alchol) and heated and distilled to 90 to 100 ℃ to collect the liquid composition from which impurities are removed, the extract and ethyl alcohol is 1 : Purifying step (S3) to be mixed in a volume ratio of 0.2 to 0.4; Liquid toothpaste manufacturing method comprising a.
The method of claim 1,
Liquid toothpaste manufacturing method, characterized in that any one selected from the roots of the root and violets instead of the root of the roots used in the material preparation step (S1).
The method of claim 1,
Additive mixing step to improve the quality of the product by further adding an additive used as a preservative, sweetener and flavoring agent to the liquid composition collected in the purification step (S3) ( S4); further comprising,
The additive is added to the liquid composition is a liquid toothpaste manufacturing method, characterized in that to add a weight corresponding to 20 to 30% by weight relative to the total weight of the liquid composition.
The method of claim 1,
The additive is a liquid dentifrice manufacturing method comprising any one or two or more selected from the group consisting of vegetable glycerin, lavender (Lavender) essential oil, menthol, pine salt, xylitol.
Liquid toothpaste characterized in that it is prepared through the liquid toothpaste manufacturing method of any one of claims 1 to 4.

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