KR20120070990A - Manufacturing method of pills comprising opuntia humifusa - Google Patents

Abstract

PURPOSE: A preparation method of opuntia humifusa pills is provided to enable users to easily intake all kinds of nutrients from opuntia humifusa without the loss of the nutrients. CONSTITUTION: A preparation method of opuntia humifusa pills comprises the following steps: extracting an opuntia humifusa mixture using an alcohol water solution, and concentrating the same to obtain opuntia humifusa mucilage; drying and crushing extraction residue obtained after extracting stems, fruits, and roots of opuntia humifusa; mixing 100 parts by weight of residue powder, 3-15 parts by weight of opuntia humifusa flower powder, and 5-30 parts by weight of opuntia humifusa mucilage; and adding 5-20 parts by weight of fermented wheat dough to the mixture before molding the mixture into pills. The wheat dough is obtained by mixing flour and water, and fermenting the mixture at 25-40 deg. C. for 2-4 days.

Description

Manufacturing method of pills comprising Opuntia humifusa

The present invention relates to a method for producing millennial vinegar which can be used as a dietary supplement or feed.

Cheonnyeoncho (Opuntia humifusa) is a native Korean cactus that grows in Jeonnam, etc. The Opuntia ficus-indica var saboten, commonly known as palm cactus, grows to 1-2 m long and has many long and thick thorns, while cheonnyeoncho has fluffy thorns. And grow to about 30 cm in size. Baeknyeoncho, which is grown on Jeju Island, is native to the tropics and is difficult to cultivate in the open field, while Korean native cactus, Chunnyeoncho, survives in the open field even in the dormant winter season, and is resistant to pests.

Although much research has not been conducted on the activity of cheonnyeoncho compared to naturalized baeknyeoncho, Park MK, Lee YJ, Kang ES (2005) Hepatoprotective effect of Cheonnyuncho (Opuntia humifusa) extract in rats treated carbon tetrachloride. J Korean Food Sic Technol 37: 822-826) reported the antioxidative activity of cheonnyeoncho stem extracts from hot water and the prevention of liver damage from carbon tetrachloride, including Lee KS, Kim MG, Lee KY (2004) Antimicrobial effect of the Extracts of cactus Chounnyouncho (Oputia humifusa) against food borne pathogens.J Korean Soc Food Sci Nutr 33: 1268-1272.) has shown that ethyl acetate fraction of cheonnyeoncho exhibits antioxidant activity similar to α-tocopherol in the study of the antioxidant effects of Cactus extract. It was reported that the antimicrobial effect of Cactus extract was excellent against pathogenic food poisoning microorganisms. Kwon DK, Song YJ (2005) Effect of opuntia humifusa supplementation on endurance exercise performance in rats fed a high-fat diet.The Korean Journal of Exercise Nutrition 9: 183-188. It has been reported to have anti-arteriosclerosis effect by reducing hyperlipidemia and increasing HDL-cholesterol concentration, and suggested the possibility of improving aerobic exercise capacity.

The solid content of cheonnyeoncho varies from 8 to 15% depending on the season, because the water content is high and grows well in summer and the water content is lowered and growth stops in winter to prevent freezing.

Cheonnyeoncho has a high protein content, tastes good, is nutritionally valuable, and most carbohydrates are made up of dietary fiber, which is essential for diet and health. The dietary fiber content is about 5%, higher than that of 칡, and the vitamin C content is about 1%, higher than other cactus or aloe. Analyzing cheonnyeoncho leaves is very low in fat and salt and high in fiber, vitamin C and calcium. So cheonnyeoncho is available to people with diabetes and is characterized by a high content of essential amino acids.

However, mucus has viscosity due to pectin or polysaccharides, which are the main constituents of stems, fruits, and roots of cheonnyeoncho, and due to such problems, it is difficult to extract active ingredients or process them into various forms of food or feed. Until now, cheonnyeoncho is used as a dietary supplement or feed that allows you to take the nutritional ingredients of millennial as it is, there is almost no situation.

The present invention is to provide a method for producing a millennial ring used as a health functional food or feed that can be easily ingested as it is without any loss of nutrients.

As an example for achieving the above object, the manufacturing method of the cheonnyeoncho ring of the present invention, the extract of a mixture of 10 to 30 parts by weight of cheonnyeoncho fruit, 1 to 10 parts by weight of the cheonnyeoncho root in 100 parts by weight of cheonnyeoncho stem and concentrated by ethanol mucilage Preparing a; Drying and pulverizing the residue remaining after alcohol extraction from the stem, fruit and root of the cheonnyeoncho; And mixing 3 to 15 parts by weight of millennial flower powder and 5 to 30 parts by weight of cheonnyeoncho mucus to 100 parts by weight of the cheonnyeoncho stem, fruit and root residue powder.

Hereinafter, the present invention will be described in detail.

First, 10 to 30 parts by weight of Cheonnyeoncho fruits and 1 to 10 parts by weight of the root of Cheonnyeoncho extract to 100 parts by weight of the stem of the Cheonnyeoncho extract and concentrated with alcohol to prepare a cheonnyeoncho mucus.

Stems, fruits and roots, except for cheonnyeoncho flowers, contain mucus and are difficult to dry by themselves. The cheonnyeoncho stem, berries and roots mix 10 ~ 30 parts by weight of cheonnyeoncho berries, 1 ~ 10 parts by weight of cheonnyeoncho stem to 100 parts by weight of cheonnyeoncho stem. It is preferable to increase the weight gain and growth rate as the antioxidant function and feed of the millennial plant in the composition range.

The stems and roots of cheonnyeoncho are cut into 5-15 cm size, and the cheonnyeoncho fruit is cut by itself or in 2-4 parts and used for extraction. The cheonnyeoncho stem, root, and fruit may be extracted with an aqueous alcohol solution, and the residue may be used. However, since the number of manufacturing processes increases with little difference in effect, it is preferable to first mix the respective composition ratios and then extract the alcohol. The aqueous alcohol solution used for extraction is preferably an aqueous alcohol solution of 1 to 4 carbon atoms containing 5 to 80% by weight of alcohol, an aqueous methanol solution, an ethanol solution, an aqueous solution of propanol, an aqueous butanol solution or an aqueous solution of isopropyl alcohol may be used. Preferably an aqueous ethanol solution.

By extracting the aqueous solution of alcohol, pectin and polysaccharide components of stems, roots and berries of cheonnyeoncho are mainly extracted, and fibers including dietary fibers are not extracted but remain as residues. Cheonnyeoncho stem, root and fruit extracts and residues can be separated by conventional filtration and compression methods, preferably using a filter press.

After mixing 0.8 ~ 5 times, preferably 1 ~ 2 times the aqueous solution of alcohol with the weight of the stem, root and fruit mixture of cheonnyeoncho, 8 to 62 hours at a low temperature of 10 to 50 ℃, preferably 10 to 25 to 45 ℃ Extract for 36 hours. If the extraction temperature is below the lower limit, the extraction time is too long. If the extraction temperature is exceeded, the polysaccharide component is browned, and a large amount of residues which are not aggregated and dissolved are produced, resulting in a decrease in the production yield or when included in the preparation of millennial rings. Cause.

After extracting cheonnyeoncho mucus with an aqueous solution of alcohol, it is concentrated under reduced pressure to remove the water contained in the aqueous solution of alcohol and mucus. Concentration under reduced pressure is maintained at 40 ~ 50 ℃ extraction temperature. If the temperature is lower than the lower limit, the concentration does not proceed well and takes a long time, and if the upper limit is exceeded, many residues due to browning and aggregation of polysaccharides are generated. Concentration of the cheonnyeoncho mucus is carried out until 30 to 60%, preferably 40 to 55% by weight relative to the weight of the first added cheonnyeoncho stem, root and fruit mixture. If it is concentrated to less than 30%, it takes too much time and money for concentration, and if it is more than 60%, sufficient binding strength cannot be exerted with the millennial ring binder, which leads to a high incidence of failure of the ring during or after the manufacturing process. .

Next, after extracting the stem, root and fruit of millennial plants with an aqueous alcohol solution, the remaining residue is dried and pulverized. Ordinary cheonnyeoncho stem, root or fruit is very difficult to dry by the conventional method due to the mucus, and in some uses a freeze-drying method of rapid freezing the stem and then drying under reduced pressure. However, such lyophilization was rarely used for mass production because of the high equipment cost and high processing cost. However, in the present invention, since the mucous part of the stem, root and fruit of the cheonnyeoncho, which is difficult to dry, is mostly removed through extraction, it is less than 5% of moisture content only by drying with normal hot air drying, for example, 3 to 12 hours at 40 to 60 ° C. Drying is possible. After alcohol extraction of dried cheonnyeon stem, root and fruit, the residue may be ground to an average particle size of 10 ~ 500 ㎛ using a conventional mill, for example hammer mill.

Next, 3 to 15 parts by weight of millennial flower powder and 5 to 30 parts by weight of cheonnyeoncho mucilage to 100 parts by weight of the residue of the cheonnyeoncho stem, fruit and root to prepare a ring.

All cheonnyeoncho flower powder can be dried up to less than 5% moisture content only by drying for 3 to 12 hours at 40 ~ 60 ℃, it is pulverized to an average particle size 10 ~ 500 ㎛ after drying.

If the millennial slime is less than the lower limit, it is difficult to prepare the ring, the manufactured ring is easily brittle, and if it exceeds the upper limit, it takes a long time to dry after the manufacture of the ring, and viscosity may remain on the surface of the ring.

The cheonnyeoncho prepared as described above is a ring manufactured so that it is easy to use and consume only with the ingredients of cheonnyeoncho without any other additives or excipients that have not been previously, and has a loosening property and easy to chew when compared to a conventional pill. have.

However, when the binding is only cheonnyeoncho mucilage strength may be weak compared to the normal ring, the following wheat dough can be used to supplement the strength.

Wheat dough, which may be additionally added for the production of pill, is kneaded by mixing 30 to 80 parts by weight of water, preferably 40 to 50 parts by weight of water, and fermentation at 25 to 40 ° C for 2 to 4 days using 100 parts of wheat flour. do. The wheat dough prepared through the fermentation process gives a binding force during the millennium ring production and provides the strength of the finished product ring.

The wheat dough is added 5 to 20 parts by weight together with 5 to 30 parts by weight of millennial slime to 100 parts by weight of the total of the residue powder of the cheonnyeoncho stem, fruit and root in the manufacture of millennial rings.

The wheat dough may further include 1 to 5 parts by weight of lactic acid bacteria (based on 1 × 10 ⁷ CFU / g) based on 100 parts by weight of wheat flour. Wheat dough containing lactic acid bacteria becomes acidic during fermentation, softens dough, and blends with cheonnyeoncho stem, fruit, root, and flower components to enhance functionality when used as a dietary supplement and feed.

According to the present invention provides a method for producing a pill that can be easily ingested as it is without any loss of nutrients of millennia, and the cheonnyeoncho prepared in this way as a livestock feed such as health functional foods or broilers, ducks, pigs It can also be used for fish farming.

Hereinafter, the present invention will be described in detail with reference to Examples. The present invention is not limited by the following examples.

Example 1

1) cheonnyeoncho mucus manufacturing

1 kg washed cheonnyeoncho stem, 50 g of root cut to 10 cm size, 200 g of fruit was further mixed, 1 kg of alcohol diluted with purified water to 10% by weight of ethanol was mixed and 1 every 12 hours at 30 ℃ The alcohol was extracted for 36 hours with stirring. The extracts of stems, roots and berries of cheonnyeoncho were pressed with a filter press to store 400 g of the residue separately, and the alcohol extracts were concentrated under reduced pressure at 45 ° C. to concentrate until the weight of the concentrate reached 300 g to prepare mucinous slime. It was.

2) Preparation of Millennial Rings

The residues of the cheonnyeoncho stem, root and fruit alcohol extract of step 1) and cheonnyeoncho flowers were dried at 55 ° C. for 6 hours, and then pulverized with a hammer mill to obtain an average particle size of 300 μm.

After mixing 100 parts by weight of the residue powder of each cheonnyeoncho stem, root and fruit alcohol extract, 10 parts by weight of cheonnyeoncho flower powder, 25 parts by weight of cheonnyeoncho mucus of step 1) was mixed to prepare a cheonnyeoncho ring.

Example 2

In the same manner as in Example 1, after preparing the cheonnyeoncho mucus, cheonnyeoncho stem, root and fruit alcohol extract residue powder, cheonnyeoncho flower powder, 100 parts by weight of the residue powder of each cheonnyeoncho stem, root and fruit alcohol extract, flower powder 10 weight The parts were mixed, and 15 parts by weight of mucin herb and 15 parts by weight of wheat dough were mixed to prepare a cheonnyeoncho ring.

The wheat dough was prepared by putting 400 g of water and 2 g of lactic acid bacteria (based on 1 × 10 ⁷ CFU / g) in 1 kg of flour and then kneading at 35 ° C. for 3 days.

Comparative example  One

The cheonnyeoncho stem was dried for 24 hours at 55 ℃, but the outer part was hardened and the mucous of the inner part was not able to dry, so using it to mix with other millennial powder, for example, cheonnyeoncho flower powder to prepare a ring It was impossible.

Comparative Example 2

100 parts by weight of cheonnyeoncho stem, 20 parts by weight of fruit, 5 parts by weight of root, 10 parts by weight of flowers were mixed, and then rapidly frozen at -20 ℃, lyophilized and then ground. A mill was prepared by mixing 20 parts by weight of wheat dough with 100 parts by weight of lyophilized powder of stem, fruit, root and flower. Wheat dough was prepared by kneading 400 g of water in 1 kg of wheat flour and immediately using the dough.

Experimental Example 1: sensory test

The cheonnyeoncho prepared by the above Examples and Comparative Examples was carried out by a five-point method by 20 sensory test personnel of 25 to 50 years of random subjects, the average of the results of three iterations are shown in Table 1 below.

Item Example 1 Example 2 Comparative Example 2 zest 4.1 4.2 3.8 Odor 1.2 1.4 2.3 Texture affinity 4.6 3.9 3.7 Overall rating 4.6 4.2 3.1 1) 1: Very disliked, 3: Normal, 5: Very good

As shown in Table 1, the difference between the flavor of the Example and the comparative example in the present invention was not large, but there was an opinion that the deep taste of the cheonnyeoncho and the complex polysaccharide in the Example was felt, in Examples 1 and 2 Compared to off-flavor.

In addition, in Example 2 and Comparative Example 2, there was no significant difference in texture, but there was an opinion that it was chewed softly and moistly in Example 1, and in Example 2 and Comparative Example 2, there was an opinion that it was strong and brittle.

Overall, Example was preferred to Comparative Example 1, and Example 1 was particularly preferred.

Experimental Example 2: Effect as a feed additive

In order to confirm the effect of the millennial pill of Example 1 of the present invention on the productivity of broiler, 1 weight of millennial pill to the group (control group) and degreasing steel to which the degreasing steel whose water content was adjusted to 40 wt% was added instead of the feed additive. % Addition and the addition of the feed additive with the water content adjusted to 40% by weight (Example 1) was used by adding 0.2% by weight to each broiler feed.

50 broiler chickens of the same size were stocked in the control and the feed of Example 1, respectively. After breeding broilers for 35 days, mortality and growth rate were measured, and the start weight, end weight, and weight gain were measured.

Item Comparative Example 1 Example 1 Starting weight (g) 42.5 42 End weight (g) 1,760 1,980 Daily gain (g / d) 49.1 55.4 Feed Intake (kg) 2.88 3.02 Dead shooter 4 One Growth rate (%) 92% 98%

As a result of the breeding test, when the millennial pill of the present invention was added, the weight gain per day was 12.8% higher, and the mortality was reduced to 1/4, and the growth rate was 6% higher. By feeding the feed additives of the millennial hwan of the present invention to broilers, it is thought that the reduction of mortality and the increase in the daily weight gain are caused by the increase of immunity by microorganisms and the mortality caused by disease is reduced.

The present invention described above is not limited to the above-described embodiments and the like, and various substitutions, modifications, and changes can be made without departing from the technical spirit of the present invention. It will be obvious to him.

Claims (5)

Extracting a mixture of 10-30 parts by weight of Cheonnyeoncho fruit and 1-10 parts by weight of Cheonnyeoncho root in 100 parts by weight of Cheonnyeoncho stems with an aqueous alcohol solution, and then concentrating to prepare a cheonnyeoncho mucus;
Drying and pulverizing the residue remaining after alcohol extraction from the stem, fruit and root of the cheonnyeoncho; And
Preparing a pill by mixing 3-15 parts by weight of millennial flower powder and 5-30 parts by weight of cheonnyeoncho mucus with 100 parts by weight of the cheonnyeoncho stem, fruit and root residue powder;
Method of producing a millennial ring containing a.
The method of claim 1, wherein in the step of preparing the ring, the flour and water kneading to prepare a ring by mixing 5 to 20 parts by weight of wheat dough further fermented at 25 ~ 40 ℃ for 2 to 4 days Way.
The method of claim 2, wherein the production of wheat dough comprises 100 parts by weight of wheat flour 30 to 80 parts by weight of water and lactic acid bacteria (based on 1 × 10 ⁷ CFU / g) 1 to 5 parts by weight.
Claims 1 to 3 of the health functional food in the form of a ring manufactured by the method of any one of claims.
Claims 1 to 3 ring-shaped feed prepared by the method of any one of claims.